TABLE OF CONTENTS
Figures .......................................................................................................... iii
Tables ........................................................................................................... iii
Safety Instructions and Symbols................................................................... iv
Cleaning Instructions .................................................................................... iv
1.
Introduction ............................................................................................... 1
1.1. About This Manual ................................................................................. 1
1.2. About the Low Current Interface (LCI) ...................................................... 1
1.2.1.
LCI Interface Cable ........................................................................... 2
1.2.2.
LCI Main Body ................................................................................. 2
1.2.3.
LCI Cell Cables ................................................................................ 3
1.3. Inspecting Your New Instrument .............................................................. 4
1.4. Maintenance, Service, and Support ........................................................... 4
2.
Installation ................................................................................................. 5
2.1. Installation ........................................................................................... 5
2.1.1.
Connect Interface Cable to LCI Main Body ............................................ 5
2.1.2.
Connect Interface Cable to Potentiostat Cell Interface ............................ 5
2.1.3.
Connect Cell Cables to LCI Front Panel ................................................. 5
2.2. LCI Calibration ...................................................................................... 5
2.2.1 Calibration ......................................................................................... 5
2.3. LCI Checkout Procedure .......................................................................... 9
3.
Measurement of Small Current Signals ..................................................... 11
3.1. Faraday Shield .................................................................................... 11
3.2. Avoiding External Noise Sources ............................................................ 12
3.3. Cell Design ......................................................................................... 12
3.3.1.
Lead and Electrode Placement .......................................................... 12
3.3.2.
Cell Construction ............................................................................ 12
3.3.3.
Reference Electrode ........................................................................ 12
3.4. Experimental Properties ........................................................................ 12
3.4.1.
Auto Current Ranging ..................................................................... 12
3.4.2.
LCI Bandwidth Limits ...................................................................... 13
4.
Specifications ........................................................................................... 15
4.1. Electronic Specifications ....................................................................... 15
4.1.1 System Performance ....................................................................... 15
4.1.2. Power Amplifier .............................................................................. 15
4.1.3. Differential Electrometer .................................................................. 15
4.1.4. Current Measurement ..................................................................... 15