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FISCHER FISCHERSCOPE X-RAY 4000 Series User Manual

FISCHER FISCHERSCOPE X-RAY 4000 Series
170 pages
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OPERATOR’S MANUAL
Coating Thickness Material Analysis Microhardness Material Testing
FISCHERSCOPE
®
X-RAY 4000 Series

Table of Contents

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FISCHER FISCHERSCOPE X-RAY 4000 Series Specifications

General IconGeneral
Element DetectionFrom Sodium (Na) to Uranium (U)
DetectorSilicon Drift Detector (SDD)
Power Supply100-240 V AC, 50/60 Hz
TypeX-ray spectrometer
ApplicationMaterial analysis, coating thickness measurement
Measurement PrincipleX-ray fluorescence (XRF)
Detection LimitsTypically in the ppm range, depending on the element and matrix
Sample typesSolids, powders, liquids, coatings
X-ray TubeMicrofocus X-ray tube
Analysis ChamberVacuum or air atmosphere
SoftwareWinFTM software for data acquisition and analysis

Summary

Safety Information

Intended Use

Specifies the intended applications of the FISCHERSCOPE X-RAY for coating thickness and material analysis.

Safety of the Electrical Equipment

Details safety requirements for the instrument's electrical components according to IEC/VDE standards.

Maintenance and Repair

Outlines that maintenance and repair must be performed by authorized FISCHER service personnel.

X-Radiation Safety

Describes protective measures against X-radiation and operational safety guidelines.

Requirements for the Operating Personnel

Specifies the necessary training and knowledge for operators and trained specialists.

X-Radiation Safety Details

Provides detailed technical information and diagrams related to X-radiation safety.

Instrument Overview

Areas of Application

Lists the measurement applications for which the instrument is suited.

X-Ray Fluorescence

Explains the fundamental principle of X-ray fluorescence excitation and emission.

Functional Principle of the Instrument

Details the operational principle and key components of the FISCHERSCOPE X-RAY instrument.

Components

Describes the main hardware components of the instrument, like aperture, shutter, and lighting.

Switching the Instrument on and off

Switching on the Instrument

Provides step-by-step instructions for powering on the instrument and the PC.

Switching off the Instrument

Outlines the correct procedure for powering down the instrument and associated PC.

Communication between Instrument and WinFTM

Explains how to establish and manage communication between the instrument and the WinFTM software.

Manual Measurements

Deleting Measurement Readings

Describes how to delete individual or all measurement readings and the consequences.

WinFTM File Structure

Def.MA

Defines the Def.MA file as containing measurement settings for the application.

Measurement Application

Explains the measurement application file's role in measurement accuracy and content.

Product

Describes the product file's function in data organization and measurement control.

User Interface of the WinFTM Software

WinFTM Main Window

Provides an overview of the main window and its various components.

Video Image

Details the functions and controls for viewing and adjusting the specimen's video image.

Statistics Field

Explains the statistical results displayed for the last block of measurements.

Measurement Value Field

Describes how measurement readings are displayed in different modes.

Product Administration

Product

Explains the necessity of product files for instrument measurements.

Setting up a new product

Provides step-by-step instructions for creating a new product file in WinFTM.

Importing a product

Guides users on how to import product files received from FISCHER.

Modifying a product

Explains how to modify product-specific settings using the "Modify product" dialog.

Deleting a product

Describes the process for deleting product files that are no longer needed.

Assigning a new measurement application to a product

Details how to link a measurement application to an existing product.

Modifying a measurement application

Explains the steps to change parameters within a measurement application.

Copying a measurement application

Describes the procedure for duplicating an existing measurement application.

Deleting a measurement application

Outlines how to remove a measurement application.

Viewing the Def.MA

Explains how to view the Def.MA file for suitability checks.

Importing a Def.MA

Guides users on importing a new Def.MA file from FISCHER.

Backing up product or Def.MA files

Details procedures for backing up product and Def.MA files.

Reference samples

Explains the purpose and characteristics of reference samples for monitoring.

Base material in Def.MA

Discusses how to define the base material in Def.MA for accurate analysis.

Monitoring the measurement devices

Explains the necessity and process of monitoring measurement devices for accuracy.

Handling of Measurement Data and Statistical Evaluations

Saving / not saving measurement data

Describes how to enable/disable automatic saving of measurement readings.

Overwriting Measurement Data

Explains how to overwrite existing measurement readings with new ones.

Closing a Block (Order no. / Operator)

Details the process of closing a block and associating it with order numbers or operators.

Block evaluation (statistics)

Explains how to view and print statistical results for a block.

Variable and fixed block size

Discusses the options for setting variable or fixed block sizes for measurements.

Deleting a block

Outlines the procedure for deleting a block of measurements.

Setting Up the Print Form Using PDM

Statistical Evaluation and Documentation Using the Supplementary Software PDM

Introduces the PDM software for enhanced data evaluation and documentation.

Editing Print Form Templates Using PDM

Guides users on creating and modifying print form templates using the PDM editor.

Inserting Variables for Print Form Templates

Explains how to insert variables into print form templates for dynamic reporting.

Variables Available for Block Evaluation

Lists and describes variables used in print form templates for block evaluation.

Variables Available for the final Evaluation

Lists and describes variables used in print form templates for final evaluation.

Measurement Uncertainty and Measuring Ranges

To estimate the Measuring range

Provides instructions on how to estimate the measuring range and required precision.

Meaning of the measurement uncertainty

Explains the concept of measurement uncertainty and its influencing factors.

Random Error

Discusses random errors in measurements and their theoretical calculation.

Systematic Error

Details how systematic errors are identified and characterized by comparison with standards.

Display of the measurement uncertainty

Explains how to configure the display of measurement uncertainty components.

Task programming

Starting a Task

Describes how to start and interrupt tasks for automating measurement procedures.

Programming Tool

Introduces the tool for creating and managing measurement tasks.

Getting started with task programming

Offers guidance on starting task programming with predefined examples.

Syntax of Task Commands

Explains the syntax rules for writing task commands.

List of Task Commands

Provides a comprehensive list of available task commands categorized by function.

Example Specification Limit Commands

Illustrates the use of specification limit commands with a practical example.

Data back-up

Extent of the data back-up

Allows selection of the scope for data backup (partial or complete).

Target path for data back-up

Specifies how to set the destination path for data backups.

Back-up cycle

Describes how to configure the frequency and initiation of data backups.

Mass per unit area and geometric coating thickness

Correlation between mass per unit area and coating thickness

Explains the relationship between mass per unit area and geometric coating thickness.

Calibration standards from FISCHER

Discusses calibration standards provided by FISCHER and their properties.

Setting the density in the Def.MA

Details how to manually set element densities within the Def.MA file.

Measurement device monitoring for the Fischerscope X-RAY

Calibration of X-ray fluorescence measuring instruments

Explains the process and importance of calibrating XRF measuring instruments.

Why monitor measurement devices?

Details the necessity and benefits of regularly monitoring measurement devices for stability.

Variation of measurement readings

Discusses how measurement readings vary due to repeatability conditions and instrument influences.

Trueness of measurement readings

Defines trueness and how it's determined by comparing measured values to known correct values.

Random and systematic deviations

Differentiates between random and systematic deviations in measurement results.

Trueness and precision

Clarifies the distinct concepts of trueness and precision in measurement technology.

Practical monitoring of the measurement devices

Provides practical steps and recommendations for monitoring measurement devices.

When and how to carry out corrections?

Outlines the procedures and triggers for performing corrective actions on measurement applications.

Wouldn’t it be better to re-calibrate?

Discusses when re-calibration is necessary versus other corrective measures.

Pre-run for determining the control limits

Explains the pre-run process for establishing control limits in quality charts.

Long-term monitoring

Describes continuous monitoring strategies for maintaining instrument stability.

Calibration

Purpose of the Calibration

Explains the situations requiring calibration and its core function.

Performing the Calibration

Details the prerequisites and steps for performing instrument calibration.

Measurement Data Export

Starting the Measurement Data Export

Guides users on initiating data export and setting up templates.

Export Settings

Explains how to configure export settings specific to products.

Setting up an Export Template

Details the process of creating and customizing export templates for data output.

Addendum

Description of the Characteristic Statistical Parameters

Provides definitions and equations for key statistical parameters used in analysis.

Final Result – Fixed Block Definition

Defines statistical parameters for results with fixed block definitions.

Final Result – Variable Block Definition

Defines statistical parameters for results with variable block definitions.

Periodic Table of the Elements with X-Ray Properties

Presents a periodic table with relevant X-ray properties for element identification.

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