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Optics11 Piuma Nanoindenter User Manual

Optics11 Piuma Nanoindenter
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PIUMA NANOINDENTER
USER MANUAL
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Optics11 Piuma Nanoindenter Specifications

General IconGeneral
Data Acquisition RateUp to 100 kHz
Maximum Sample Size100 mm diameter
Indenter TypesBerkovich, spherical, flat punch, custom
TechniquesDMA, scratch testing
Microscope CompatibilityCompatible with optical microscopes
SoftwareDMA

Summary

Revision History

Safety

Introduction

1. Installation

1.1 The Piuma Nanoindenter and its components

Describes the Piuma Nanoindenter and its five main components.

1.2 Connecting components

Outlines the necessary cables and connection scheme for setting up the system.

2. Preparing the Setup for Measurement

2.1 Starting the system

Details powering up the instrument and launching the Piuma software.

2.2 Mounting a probe to the Piuma Nanoindenter

Guides on selecting and installing the correct probe for measurements.

2.3 Calibrating the optical signal

Describes the process of calibrating the optical signal for accurate measurements.

2.4 Calibrating the probe geometrical factor

Explains how to determine the geometrical factor for accurate data analysis.

3. Using the Piuma Nanoindenter

3.1 Stage controls

Manual positioning of the Piuma stages in X, Y, and Z directions.

3.2 Piezo controls

Manual control of the piezo stack for precise indentation positioning.

3.3 The Find surface procedure

Steps for safely approaching the sample surface using automated functions.

3.4 Modes of operation

Overview of D-mode, P-mode, and I-mode operations.

3.5 Dynamic mechanical analysis – DMA

Enables mechanical oscillations during indentation for dynamic analysis.

3.6 Saving measurement

Instructions for setting up a dedicated folder and naming experiments.

3.7 Performing measurements

Describes the process of conducting single or series of indentations.

3.8 Data processing and analysis

Explains how load-displacement data is stored and processed.

4. Optimizing Instrument Stability and Sample Mounting

4.1 Environment stability

Discusses minimizing errors from temperature drift and vibrations.

4.2 Sample stability

Addresses sample temperature, integrity, and mechanical instability.

4.3 Probe stability

Covers factors affecting probe stability like temperature and air bubbles.

5. Working Principle of the Piuma Nanoindenter Instrument

5.1 Principle of operation

Explains how the instrument uses optical probes and interferometry.

5.2 The Measurement and Calculation of the Young's Modulus

Describes methods to measure and calculate Young's modulus.

6. Description of the Piuma Software

6.1 Front panel controls

Overview of controls for operating stages, setting experiments, and viewing status.

6.2 Results

Displays indentation results including modulus and probe suitability.

6.3 Configuration panels

Menus to configure indentation profile, probe, and advanced settings.

7. The OP1550 Interferometer

7.1 Using the OP1550 Interferometer

Guides on navigating menus and using the interferometer's functions.

8. FAQ & Troubleshoot

Flowchart - Calibration

A flowchart to guide through calibration issues and solutions.

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