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Anton Paar DHS 1100 - User Manual

Anton Paar DHS 1100
38 pages
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Measure
what is measurable
and make measurable
that which is not.
Galileo Galilei (1564-1642)
Instruction Manual and Safety Information
DHS 1100
Domed Hot Stage with
CCU 100 Control Unit
(Original Instruction)
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Summary

1 Safety Instructions

1.1 General Safety Instructions

Covers liability, installation, use, maintenance, disposal, and precautions for flammable materials.

1.2 Conventions for safety messages

Explains the meaning of WARNING, CAUTION, NOTICE, and symbols used in the manual.

1.3 Safety Signs on the Instrument

Shows warning symbols on the instrument and advises to keep them legible.

2 Overview

2.1 Description of the Instrument

Details the DHS 1100 Domed Hot Stage, its design, applications, and required accessories.

2.2 Design of the Instrument

Describes the components of the DHS 1100, including housing, cooling ring, and domes.

2.2.1 Dome

Explains the graphite and PEEK dome materials, their properties, and applications.

2.2.2 Dome Cooling Nozzle for PEEK Dome

Provides information on the cooling nozzle for PEEK dome operation.

2.2.3 Housing and Internal Parts

Details the housing material, cooling fins, heating plate, springs, and internal components.

2.2.4 Connection Device

Describes the connection device for gas/vacuum and temperature control.

2.3 CCU 100 Combined Control Unit

Explains the function and operation of the CCU 100 for sample plate temperature control.

2.3.1 CCU 100 Front Panel

Details the control buttons, status LEDs, and display on the CCU 100 front panel.

2.3.2 CCU 100 Rear Panel

Lists and describes the connectors found on the CCU 100 rear panel.

2.3.3 Control of the Compressed-Air Cooling

Explains how the CCU 100 controls the compressed-air cooling system.

2.3.4 Overheat Protection

Describes the protective thermoswitch and overheat protection mechanism.

2.4 Compressed-Air Cooling Equipment

Recommends the Air Service Unit for compressed air requirements.

3 Installation

3.1 Installation Requirements

Lists requirements for X-ray diffractometer, electrical, compressed-air, and vacuum equipment.

3.2 Unpacking the Instrument

Provides instructions and warnings for carefully unpacking the instrument.

3.3 Mounting the DHS 1100 on the Goniometer

Details how to mount the DHS 1100 to the goniometer using bore holes and quick coupling.

3.4 Installing the Compressed Air Cooling

Explains installing compressed air cooling, connecting it to CCU 100 and Air Service Unit.

3.5 Connecting the Gas Supply;Vacuum Equipment

Describes connecting gas/vacuum hoses for operation under vacuum or inert gas.

3.6 Installing the CCU 100 Combined Control Unit

Guides on rack mounting the CCU 100 and ensuring adequate space and ventilation.

3.7 Connecting CCU 100 with a Computer

Explains connecting the CCU 100 to a computer via RS 232 for remote control.

3.8 Installing the Cooling Nozzle

Details specifications for PEEK dome operation, including cooling nozzles.

4 Putting DHS 1100 into Operation

4.1 Alignment

Describes standard alignment at room temperature and potential adjustments for accurate measurements.

4.2 Starting CCU 100

Provides step-by-step instructions for powering on and initializing the CCU 100.

5 Operating CCU 100

5.1 Front Panel of the Instrument

Details the CCU 100's front panel layout: keypad, LEDs, and display.

5.2 Keypad

Details the CCU 100 keypad functions and status LEDs.

5.3 Display

Explains the CCU 100 display elements and its navigation diagram.

Parameter Page

Lists and describes CCU 100 parameters like heating/cooling rate and dome configuration.

Config Parameters

Details configurable CCU 100 parameters like heating rate activation and set point range.

5.4 Turning the Heater On and OFF

Explains how to turn the CCU 100 heater on and off.

5.5 Controlling the Compressed-Air Cooling

Describes the two modes (cOFF, CON) for controlling compressed-air cooling.

5.6 Manual Control of CCU 100

Guides on manual operation for setting sample temperature and heating/cooling rate.

5.7 Remote Control of CCU 100

Discusses remote control options via diffractometer software or NAMBICON software.

6 Operation

6.1 Preparing the Instrument

Outlines safety requirements and conditions for operating the DHS 1100.

6.2 Mounting the Sample

Details the process of mounting flat samples onto the heating plate.

6.3 Mounting and Removing the Dome

Provides step-by-step instructions for mounting and removing the dome.

6.4 Operation of DHS 1100 with PEEK Dome

Details specific requirements for operating with a PEEK dome, including cooling nozzles.

6.5 Performing a Measurement

Guides on starting measurements after sample mounting and alignment.

7 Troubleshooting

7.1 Error Messages

Lists and describes alarm messages (E01-E13, E98-E99) and their causes.

7.2 General Messages on Display

Explains general messages like '8888' and '9999' shown on the CCU 100 display.

7.3 Error Analysis

Refers to the reference manual for detailed error analysis.

8 Upkeep and Cleaning

8.1 Checking the Dome

Outlines regular checks for the dome, including cracks and coatings.

8.2 Replacing the O-rings

Describes replacing O-rings, emphasizing careful handling of sealing surfaces.

8.3 Changing the Hot Plate

Details the procedure for removing and replacing the hot plate.

8.4 Exchanging Electronic Components

Covers switching off the instrument and checking/replacing main fuses.

9 Maintenance and Repair

9.1 Warranty

Lists parts excluded from warranty and additional exclusions for damage.

9.2 Repair Performed by an Authorized Anton Paar Representative

Explains how to contact representatives for repairs and required documentation.

Appendix A: Technical Data

Temperature range

Lists temperature ranges for Graphite Dome and PEEK Dome under various atmospheres.

Atmospheres

Specifies permitted gases and pressure limits for the dome.

Temperature measurement & control

Details the temperature control unit, sensor type, and heater type.

Dimensions;Weight

Provides physical dimensions and weight of the DHS 1100.

Sample plate

Lists sample plate diameter, thickness, height, and fixing method.

Dome

Details dome diameter, wall thickness, X-ray transmission, and angular range.

Cooling requirements

Specifies cooling air pressure and flow rate for different dome configurations.

List of materials

Enumerates materials used for sample plate, springs, thermocouple, heater, dome, housing, etc.

CCU 100 Dimensions

Provides dimensions and weight of the CCU 100.

CCU 100 Electrical Data (for use with DHS 1100)

Details voltage, frequency, power consumption, fuses, and output parameters for CCU 100.

Ambient conditions

Specifies ambient temperature, humidity, pollution degree, and operating altitude.

Disposal

General advice on instrument disposal.

The DHS 1100 with CCU 100 Combined Control Unit Unit is CE-compliant according to:

Lists CE compliance directives and applied standards for EMC and Low Voltage.

Appendix B: Declaration of Conformity

EU Declaration of Conformity

Official declaration by Anton Paar GmbH regarding product conformity to EU legislation.

Anton Paar DHS 1100 Specifications

General IconGeneral
Control SystemDigital PID controller
Temperature stability±0.1 °C
Power Supply50/60 Hz
Cooling TechnologyNot applicable
CoolingNot applicable
DisplayLCD
InterfaceRS-232