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Buchi Rotavapor R-300 User Manual
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Rotavapor® R-300
Operation Manual
11593738 | H en
2
Table of Contents
Default Chapter
3
Table of Contents
3
1 About this Document
6
Warning Notices in this Document
6
Symbols
6
Warning Symbols
6
Mandatory Directive Symbols
7
Other Symbols
7
Available Languages
7
Trademarks
7
2 Safety
8
Intended Use
8
Use Other than that Intended
8
Staff Qualification
9
Residual Risks
9
Dangerous Vapors
9
High Internal Pressure
10
Hot Surfaces and Liquids
10
Rotating Parts
10
Faults During Operation
10
Glass Breakage
10
Personal Protective Equipment
10
Modifications
11
3 Product Description
12
Description of Function
12
Options
13
Configuration
14
Front View
14
Rear View
15
Heating Bath User Interface
16
Type Plate
17
Warning Symbols on the Device
18
Cover for Heating Bath B-305 (Optional)
18
Scope of Delivery
19
Technical Data
19
Heating Bath Base, B-300
19
Heating Bath
20
Ambient Conditions
20
Materials
20
Safety Features
21
Overheat Cut-Out
21
Protection against Electrical Overload
21
Clips and Holders
21
Glassware
21
Optional Accessories
21
Earthquake Safety
21
4 Transport and Storage
22
Transport
22
Storage
22
5 Installation
23
Installation Site
23
Securing against Earthquakes
23
Fitting the Vapor Duct, Vacuum Gasket and Cooling Condenser
24
Fitting the Glass Stopcock
25
Fitting PTFE Stopcock (Optional Accessory)
26
Fitting the Interface I-300/I-300 Pro (Optional Accessory)
26
Mounting Vacubox on R-300 (Optional Accessory)
27
Mounting Legacybox on R-300 (Optional Accessory)
28
Fitting the Woulff Bottle (Optional Accessory)
29
Fitting Autodest Sensor and Vapor Temperature Sensor (Optional Accessory)
31
Fitting a Foam Sensor (Optional Accessory)
32
Connecting Vacuum and Coolant Tubing
34
Overview: Vacuum and Coolant Tubing
35
Setting up the Heating Bath
36
Fitting the Protection Shield (Optional)
37
Fit the Splash Guard (Optional Accessory)
38
Connecting the Rotavapor to the Power Supply
40
Assembling the BUCHI Distillation System
42
Overview: Setting up Communication Connections
43
Connecting Communication Cables to the Rotavapor
44
Overview: Setting up Coolant Tubing Connections
45
Overview: Setting up Vacuum Tubing Connections
46
Basic Settings
47
Quick Check
47
6 Operation
49
Preparations
49
Preparing the Heating Bath
49
Fitting the Evaporating Flask
50
Adjusting Immersion Angle of Evaporating Flask
51
Fitting the Receiving Flask
52
Raising and Lowering Rotary Drive Unit
53
Performing Distillation
57
Operating the Rotavapor Without Control System (Interface)
58
Operating Rotavapor with Interface I-300/I-300 Pro
59
Adjusting Distillation Conditions
60
Optimization Distillation
60
Adding Solvent During Distillation
62
Finishing Distillation
63
Removing the Evaporating Flask
63
Removing the Receiving Flask
64
7 Cleaning and Servicing
65
Inspecting and Cleaning the Vapor Duct
65
Checking the System for Leaks
66
Cleaning the Splash Guard (Optional Accessory)
66
Fitting GL14 Cap Nut with Tube Seal
67
Checking Seals
68
Cleaning the Glassware
70
Cleaning the Heating Bath
70
Cleaning the Woulff Bottle
70
Removing Solvent Accumulations
71
Performing a Firmware Update
71
8 Help with Faults
74
Faults, Possible Causes and Remedies
74
Resetting Safety Functions
76
Resetting Overheat Safety Cut-Out on Heating Bath
76
Replacing Fuse in Heating Bath Base
77
9 Taking out of Service and Disposal
78
Taking out of Service
78
Disposal
78
10 Appendix
79
Solvent Table
79
Spare Parts and Accessories
80
Glass Assembly a
80
Glass Assembly V
81
Glass Assembly C
82
Glass Assembly S
83
Glass Assembly CR
84
Glass Assembly E
85
Glass Assembly by
86
Glass Apparatus HP
87
Accessories
87
Wearing Parts
102
List of Abbreviations
111
Health and Safety Approval
111
Health and Safety
112
Rotavapor® Induction Training
113
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Buchi Rotavapor R-300 Specifications
General
Brand
Buchi
Model
Rotavapor R-300
Category
Laboratory Equipment
Language
English
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