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Buchi Rotavapor R-300 User Manual

Buchi Rotavapor R-300
116 pages
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Rotavapor® R-300
Operation Manual
11593738 | H en

Table of Contents

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Buchi Rotavapor R-300 Specifications

General IconGeneral
BrandBuchi
ModelRotavapor R-300
CategoryLaboratory Equipment
LanguageEnglish

Summary

About this document

Warning notices in this document

Explains danger levels and signal words used in the manual.

Symbols

Illustrates and defines warning, directive, and other symbols used in the manual.

Available languages

Information on obtaining the manual in different languages.

Trademarks

Lists trademarks used in the manual and their owners.

Safety

Intended use

Details the intended operations and applications for the Rotavapor R-300.

Use other than that intended

Outlines impermissible applications and the associated risks.

Staff qualification

Specifies requirements for users and operators for safe device operation.

Residual risks

Details various residual risks including vapors, pressure, heat, and glass breakage.

Personal protective equipment

Recommends wearing appropriate PPE based on hazards.

Modifications

Warns against unauthorized modifications and emphasizes using genuine parts.

Product description

Description of function

Explains the working principle of the Rotavapor R-300.

Options

Lists available heating bath sizes and interface options for the Rotavapor R-300.

Configuration

Identifies components of the Rotavapor R-300 from front and rear views.

Scope of delivery

Explains how the scope of delivery is determined by the purchase order.

Technical data

Provides technical specifications for the Rotavapor, heating baths, and ambient conditions.

Safety features

Details safety features like overheat cut-out, overload protection, clips, glassware, etc.

Transport and storage

Transport

Provides guidelines for safe transportation and checking for damage.

Storage

Outlines recommendations for proper storage of the device.

Installation

Installation site

Specifies requirements for the installation location and environment.

Securing against earthquakes

Details how to secure the Rotavapor against earthquakes using lashing eyes.

Fitting the vapor duct, vacuum gasket and cooling condenser

Step-by-step instructions for assembling the vapor duct, gasket, and condenser.

Fitting the glass stopcock

Guides on how to fit and use the glass stopcock for various functions.

Fitting PTFE stopcock (optional accessory)

Instructions for fitting the optional PTFE stopcock and its functions.

Fitting the Interface I-300/I-300 Pro (optional accessory)

Details on mounting the interface unit for controlling the system.

Mounting VacuBox on R-300 (optional accessory)

Instructions for mounting the VacuBox, required for interface operation.

Mounting LegacyBox on R-300 (optional accessory)

Explains how to fit the LegacyBox for using older peripherals.

Fitting the Woulff bottle (optional accessory)

Describes how to fit the Woulff bottle for particle/droplet separation.

Fitting AutoDest sensor and vapor temperature sensor (optional accessory)

Details connecting sensors for automatic distillation.

Fitting a foam sensor (optional accessory)

Instructions for fitting the foam sensor to detect and mitigate foaming.

Connecting vacuum and coolant tubing

Guides on connecting vacuum and coolant tubing to the system.

Setting up the heating bath

Explains how to set up the heating baths (B-301, B-305) on the base.

Fitting the protection shield (optional)

Details how to fit the protection shield for safety.

Fit the splash guard (optional accessory)

Instructions for fitting the splash guard for protection against splashes.

Connecting the Rotavapor to the power supply

Explains how to connect the Rotavapor and heating bath to the power supply.

Assembling the BUCHI distillation system

Recommends and describes the use of other BUCHI equipment with the Rotavapor.

Basic settings

Explains how to set the maximum temperature and lock the set temperature.

Quick check

Outlines a quick check to verify installation completion.

Operation

Preparations

Covers preparing the heating bath, fitting flasks, and adjusting the angle.

Performing distillation

Covers crucial safety warnings before performing distillation.

Operating the Rotavapor without control system (interface)

Provides a recommended procedure for manual operation.

Operating Rotavapor with Interface I-300/I-300 Pro

Explains controlling the system via the Interface I-300/I-300 Pro.

Adjusting distillation conditions

Recommends settings for optimal distillation conditions.

Optimization distillation

Discusses optimizing the distillation process based on solvent.

Adding solvent during distillation

Instructions for adding solvent while distillation is in progress.

Finishing distillation

Step-by-step guide to safely finish the distillation process.

Removing the evaporating flask

Details the procedure for safely removing the evaporating flask.

Removing the receiving flask

Instructions for safely removing the receiving flask.

Cleaning and servicing

Inspecting and cleaning the vapor duct

Guides on inspecting and cleaning the vapor duct for damage and residues.

Checking the system for leaks

Explains how to perform a leak test and identify issues.

Cleaning the splash guard (optional accessory)

Provides instructions for cleaning the optional splash guard.

Fitting GL14 cap nut with tube seal

Details on fitting GL14 cap nuts and tube seals correctly.

Checking seals

Explains when to clean or replace seals and how to inspect them.

Cleaning the glassware

Provides methods for cleaning glass components safely and effectively.

Cleaning the heating bath

Outlines when and how to clean the heating bath bowl.

Cleaning the Woulff bottle

Instructions for cleaning the glass part of the Woulff bottle.

Removing solvent accumulations

Guides on draining fluids and drying the system before storage.

Performing a firmware update

Details the process for updating the device firmware using BUCHI tools.

Help with faults

Faults, possible causes and remedies

A troubleshooting guide listing common faults, their causes, and solutions.

Resetting safety functions

Guides on resetting overheat cut-outs and replacing fuses.

Taking out of service and disposal

Taking out of service

Procedures for safely taking the device out of service.

Disposal

Guidelines for the proper disposal of the equipment.

Appendix

Solvent table

A table listing various solvents with their properties for distillation.

Spare parts and accessories

Lists spare parts, accessories, glass assemblies, and wearing parts for the device.

List of abbreviations

Provides a list of abbreviations used in the manual.

Health and safety approval

Information on health and safety approval and declaration requirements.

Health and safety

Declaration requirements for safety, hazards, and disposal of waste.

Rotavapor® induction training

Information regarding the introduction training for Rotavapor users.

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