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CIANFLONE X Series - User Manual

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Portaspec X Series
Multi Element Bench Top
X-ray Spectrograph
Model 2501XBT
Operations & Safety Manual
Zn
30
41.81°
Zinc
Cu
29
45.03°
Copper
Y
39
23.81°
Yttrium
Br
35
29.96°
Bromine
Sr
38
25.15°
Strontium
Cr
24
69.35°
Chromium
V
23
76.92°
Vanadium
Ni
28
48.67°
Nickel
Co
27
52.81°
Cobalt
Mn
25
62.97°
Manganese
Fe
26
57.52°
Iron
Portaspec
®
XRF
Analysis / Control
SCIENTIFIC
CIANFLONE
U
92
26.14°
Uranium
W
74
43.01°
Tungsten
Ti
22
86.14°
Titanium
Au
79
36.97°
Gold
Pb
82
33.92°
Lead
Pt
78
38.05°
Platinum
Mo
42
20.33°
Molybdenum
Ru
44
18.37°
Ruthenium
Hf
72
45.85°
Hafnium
Ag
47
16.01°
Silver
Nb
41
21.40°
Niobium
Zr
40
22.56°
Zirconium
Ba
56
87.17°
Barium
X-Ray Tube
Detector
Collimator
Receiving
Specimen
Crystal
Source
Collimator
NOTE: This Manual contains the older Portaspec Operating Control Software Version
and is in the process of being revised and updated with the new “PCS” Portaspec Control
Software. Your Portaspec instrument may differ as well. However, this Manual will
continue to be a valuable resource in the operation and safety of the Model 2501XBT
Portaspec and all Operators should be familiar with its contents.
2021
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Summary

Important Notices

X-Ray Monitoring & Reports

Procedures and recommendations for monitoring radiation exposure.

Portaspec Manufacturers Notice

Manufacturer's warranty and user responsibilities regarding regulations.

Medical Notice

Precautions for individuals with radioactive medical dyes.

Introduction and Description

Model 2501 X Series Portaspec

Overview of the wavelength dispersive XRF analyzer.

Model 2501 XBT Portaspec

Details configuration, sample holder, and capabilities.

Quality in the Manufacturing Process

Component verification, assembly, and quality checks.

Certificates

Information on calibration and radiation compliance certificates.

X-Ray Safety

The X-ray Tube

Description of the X-ray tube, its function, and alignment.

Caution and Warning Labels

Identifies and explains safety labels on the device.

X-Ray Safety

Caution Radiation

Details the "CAUTION RADIATION" label placement and visibility.

Information Labels

Location and content of serial number and fuse labels.

Audible Alerts

Explains system test alerts and failure indications.

X-Ray Safety

X-ray On Alert

Describes the audible alert accompanying the X-ray on indicator.

Visual Indicators

Explains the fail-safe warning light and software indicators.

X-ray Interlock Switches

Explains the crucial role of interlocks in preventing radiation exposure.

X-Ray Safety

X-Ray On Interlock Key Switch

Details the operation of the X-ray on/off key switch.

Rear Panel Safety Interlock Switch

Describes the interlock switch on the rear panel.

X-Ray Safety

Model 2501 XBT Two-Position Sample Holder Interlock Switches

Explains sample holder interlocks for safety.

Portaspec Shielding

Details the shielding materials and design for radiation containment.

X-Ray Safety

Personal Dosimetry and Area-Monitoring

Discusses requirements for personal and area radiation monitoring.

Portaspec Radiation Leakage Test or Radiation Survey

Outlines procedures for leakage testing and survey specifications.

X-Ray Safety

Portaspec Service

Recommends certified technicians for maintenance and annual certification.

Portaspec Initial Setup

Power Requirements

Details voltage, frequency, grounding, and dedicated power source needs.

Portaspec Location and Operating Environment

Guidance on ideal placement and environmental conditions.

Portaspec Initial Setup

Model 2501 XBT Portaspec Assembly

Step-by-step instructions for assembling the instrument.

Portaspec Initial Setup

Power Down and Disassembly

Procedure for safely powering down and disassembling the unit.

Transporting

Guidelines for safely moving the Portaspec unit.

Portaspec Initial Setup

Shipping Cases

Information on optional premium cases for shipping and storage.

Principle of Operation

Radiation Path Explanation

Describes the path of radiation from source to detector.

Operating the Portaspec

The Operator

Operator qualifications, training, and familiarity with manual.

The Operating Environment

Ideal temperature, humidity, and handling conditions.

Operating the Portaspec

Operators Tutorial

Step-by-step guide for initial setup and connection.

Operating the Portaspec

Analyzing for the First Time

Guide for performing the first analysis with calibration sample.

Operating the Portaspec

Sample Preparation and Presentation

Techniques for preparing and presenting samples for analysis.

Operating the Portaspec

Qualitative and Quantitative Analysis

Methods for identifying and quantifying elements in samples.

Operating the Portaspec

Water Cooling

Details on water cooling requirements and precautions.

Component Description

Model 2501 XBT Portaspec Front View

Identification of components on the front of the Portaspec.

Component Description

Model 2501 XBT Portaspec Rear View

Identification of components on the rear of the Portaspec.

Component Description

Model 2501 XBT Portaspec Rear Panel Internal View

Identification of internal components on the rear panel.

Component Description

Model 2501 XBT Portaspec Interior View

Identification of main internal assemblies.

Component Description

Model 2501 XBT Portaspec X-Ray Optical Path

Description of the optical path components.

Accessory Description and Assembly

Catalog No. 2522 X Coolant Circulator

Details of the coolant circulator accessory.

Filling the Coolant Circulator

Instructions for filling and preparing the coolant circulator.

Accessory Description and Assembly

Catalog 2545 X Constant Output Voltage Regulator

Details of the constant voltage regulator accessory.

Maintenance and Troubleshooting

Troubleshooting Chart

Common problems, their causes, and solutions.

Maintenance and Troubleshooting

Element Stop Adjustment Model 2501 XBT

Procedure for adjusting element stops for accurate settings.

Maintenance and Troubleshooting

Setting the Stop

Detailed steps for setting element stops using the software.

Maintenance and Troubleshooting

Portaspec Preventative Maintenance Schedule

Schedule of daily, monthly, and yearly maintenance tasks.

Maintenance and Troubleshooting

Recommended Spare Parts

List of recommended spare parts for inventory.

X Series Technical Data

Portaspec Model 2501 XBT Technical Data

Comprehensive technical specifications of the instrument.

Appendix

X-Ray Emission Line Wavelengths and Two Theta Tables

Data table of X-ray emission lines and angles.

Appendix

X-Ray Periodic Chart

Periodic table indicating analyzable elements.

Appendix

Interference and Resolution Chart

Chart showing spectral interferences and resolution.

Appendix

Counting Statistics for a Gaussian Distribution

Table related to counting statistics and confidence levels.

Appendix

Model 2501 XBT Schematic Diagram

Electrical schematic of the Portaspec system.

Portaspec Warranty

Separate Warranty With Respect to X-Ray Tubes

Specific warranty terms for the X-ray tube component.

CIANFLONE X Series Specifications

General IconGeneral
BrandCIANFLONE
ModelX Series
CategoryLaboratory Equipment
LanguageEnglish