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Labconco FreeZone 76700 Series User Manual

Labconco FreeZone 76700 Series
65 pages
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FreeZone
®
2.5 Liter Freeze Dry Systems
Models
74200 Series
76700 Series
76705 Series
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User’s Manual
Please read the User’s Manual before operating the equipment.
Labconco Corporation
8811 Prospect Avenue
Kansas City, MO 64132-2696
800-821-5525, 816-333-8811
FAX 816-363-0130
E-MAIL labconco@labconco.com
HOME PAGE www.labconco.com

Table of Contents

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Labconco FreeZone 76700 Series Specifications

General IconGeneral
Model76700 Series
TypeFreeze Dryer
Collector Capacity6 liters
Temperature-50 °C
Condenser TypeStainless steel
Voltage115V
Electrical115 V, 60 Hz
Capacity6 L

Summary

Chapter 1: Introduction

Freeze Dry Process

Overview of the freeze-drying process, including sublimation and vacuum.

Freeze Dry Rates

Factors affecting freeze-drying speed like surface area, thickness, and temperature.

Freeze Dry Capacity

Determining how much sample can be freeze-dried based on system and sample properties.

Samples Containing Volatile Substances

Handling samples with volatile components and their effect on freeze drying.

About This Manual

Explains the manual's purpose, structure, and conventions for user guidance.

Typographical Conventions

Explains formatting like italics, bold text, and icons used in the manual.

Your Next Step

Guidance on which chapters to read next based on the user's installation status.

Chapter 2: Prerequisites

Electrical Requirements

Details on dedicated outlets, circuit breakers, and specific plug types for the freeze dryer.

Location Requirements

Guidelines for placing the unit, ensuring proper airflow and stability.

Vacuum Pump Requirements

Specifications for the required vacuum pump, including displacement and pressure.

Chamber or Manifold Requirements

Information on the necessity of separate purchase for chambers and manifolds.

Chapter 3: Getting Started

Unpacking Your Freeze Dryer

Instructions for carefully unpacking and inspecting the freeze dryer for transit damage.

Freeze Dryer Components

Guidance on locating and verifying all received freeze dryer components.

Setting Up Your Freeze Dryer

Steps for positioning and preparing the freeze dryer after unpacking.

Component Orientation

Proper positioning of the unit for optimal airflow and stability.

Vacuum Pump Connection

How to correctly connect the vacuum pump to the freeze dryer.

Electrical Connection

Steps for connecting the freeze dryer's power cord to the electrical supply.

Drying Chamber or Drying Manifold Installation

How to attach chambers or manifolds to the collector chamber lid.

Chemical Resistance of Freeze Dryer Components

Information on material compatibility with various chemicals used in processes.

Solvent Safety Precautions

Warnings and guidelines for safely handling flammable or hazardous solvents.

Chapter 4: Using Your Freeze Dryer

Freeze Dryer Controls

Detailed explanation of the function of each button and indicator on the control panel.

Operation Checklist

Pre-use checklist to ensure the freeze dryer is ready for operation.

Vacuum Pump Ballast Setting

Recommendation on setting the gas ballast for optimal vacuum performance.

System Setup and Configuration

Configuring units, start-up modes, vacuum levels, and hours monitoring.

Sample Handling and Processing

Procedures for preparing, adding, and processing samples in the freeze dryer.

Shutdown and Defrosting

Steps for safely turning off the unit and removing ice from the collector.

System Alarms and Error Handling

Understanding and responding to various system alarms like power failure and voltage errors.

Chapter 5: Maintaining Your Freeze Dryer

Front Access Panel Removal (Console Models)

Instructions for removing the front panel for maintenance access on console units.

Chapter 6: Using the RS232 Receptacle

Computer Connection for Interface

How to connect a computer to the freeze dryer for data monitoring.

Chapter 7: Troubleshooting

Vacuum Pump Issues

Steps to diagnose and resolve problems related to the vacuum pump's performance.

Gasket, Tubing, and Valve Issues

Troubleshooting leaks and problems with seals, hoses, and sample valves.

System Component and Chamber Isolation

Tests to determine if leaks originate from the drying chamber or collection system.

Refrigeration Module Operation

Diagnosing issues with collector temperature and refrigeration system performance.

Chapter 8: Modifying Your Freeze Dryer Display

Temperature and Vacuum Display Adjustment

How to add offsets to calibrate temperature and vacuum readings.

Line Voltage Alarm Point Configuration

Adjusting voltage alarm limits to prevent nuisance alarms.

Moisture Sensor Alarm Management

Instructions on how to enable or disable the moisture sensor alarm.

Display Modification and Reset Procedures

Steps to adjust display settings and perform master resets.

Appendix A: Freeze Dryer Components

Appendix B: Freeze Dryer Dimensions

Appendix C: Freeze Dryer Specifications

Electrical Specifications

Detailed electrical requirements, voltage ranges, frequency, and amperage ratings.

Environmental Conditions

Specifies operating conditions like altitude, temperature, and humidity limits.

Appendix D: Freeze Dryer Accessories

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