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NETZSCH LFA 447 Nanoflash - User Manual

NETZSCH LFA 447 Nanoflash
89 pages
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Operating Instructions
LFA 447
TM
01/09 J:\LFA447\Contents.doc
Operating Instructions LFA 447
TM
Nanoflash
Contents
Chapter I
General Information
Chapter II
Installation
Chapter III
System Components
Chapter IV
Operating the Instrument
Chapter V
Appendix
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Summary

Chapter 1: General Information

Using the Manual: Notes and Symbols

Explains symbols and conventions used within the manual for user guidance and clarity.

Basic Safety Information

Outlines fundamental safety principles and responsibilities for operating the instrument safely.

Operational Precautions

Details specific safety measures and actions required during operations and maintenance to prevent hazards.

Safe Handling of Gas Containers

Provides guidelines for the safe handling, storage, and use of gas containers, including nitrogen.

Liquid Nitrogen Storage Safety

Offers recommendations for the safe handling and storage of liquid nitrogen containers to prevent hazards.

Chapter 2: Installation

Installation: Overview and Requirements

Covers initial setup, packing, delivery checks, and optimal location requirements for the instrument.

Installation Schematics

Presents diagrams illustrating the practical arrangement and layout of the instrument components.

Connecting System Components

Details the procedures for connecting the computer system and the thermostat to the main unit.

Chapter 3: System Components

Measuring Unit Components

Describes the main measuring unit, its key components, and technical specifications.

Front and Back Panel Interfaces

Explains the operating elements on the front panel and the connections on the back panel of the measuring unit.

Sample Holder System Overview

Introduces the various sample holders, including standard and special types, for different sample geometries.

Thermostat Function and Connection

Explains the function and connection of the thermostat required for instrument operation and cooling.

Chapter 4: Operating the Instrument

Measurement Principle

Explains the fundamental principles of the Nanoflash method for thermal property measurement.

Instrument Preparation and Setup

Guides users through preparing the IR detector, opening/closing the unit, and initial sample preparation.

Sample Handling and Calibration

Covers sample mass, density, calibration materials, and the process of inserting a sample.

Running Measurements

Details how to start measurements, adjust parameters, and perform specific heat determination.

Chapter 5: Appendix

Technical Specifications

Provides a summary of key technical data and specifications for the LFA 447 instrument.

Matrix Sample Holder Setup

Details the individual parts and installation procedure for the matrix sample holder.

Measurement Start Procedures

Outlines the final steps for starting a measurement, including sample positioning and software configuration.

NETZSCH LFA 447 Nanoflash Specifications

General IconGeneral
Accuracy±3%
Repeatability±2%
Data AcquisitionHigh-speed data acquisition system
Measurement PrincipleLaser Flash Method
Light SourceLaser
DetectorInfrared Detector
AtmosphereInert gas (e.g., nitrogen, argon) or vacuum
Thermal Conductivity Range0.1 to 1000 W/(m·K)
Specific Heat Capacity Range0.1 to 5 J/gK
Thermal Diffusivity Range0.01 to 1000 mm²/s
SoftwareLFA Software
Measurement TimeA few seconds per measurement
Power Supply110-240 V, 50/60 Hz
Dimensions600 x 400 x 300 mm