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Rotavapor R-220 SE
Buchi Rotavapor R-220 SE User Manual
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Rotav
apor
® R-
2
2
0 SE
Operation Manua
l
1
1
5
933
56H en
2
Table of Contents
Default Chapter
3
Table of Contents
3
1 About this Manual
7
2 Safety
8
User Qualification
8
Proper Use
8
Improper Use
8
Safety Warnings and Safety Signals Used in this Manual
9
Product Safety
12
General Hazards
12
Warning Labels on Housing
13
Personal Safety Measures
14
Built-In Safety Elements and Measures
14
General Safety Rules
15
3 Technical Data
16
Available System Configurations and Dimensions
16
Application Areas
17
Typical Example Applications and Accessories
17
Technical Data
18
Materials Used
20
4 Description of Function
21
Functional Principle of a Rotavapor Evaporation
21
Rotavapor Front-Side
23
Tubing Scheme
24
Cooling Water Routing
26
Vaccum Routing
27
User Interface Front-Side
29
Connection Field at the Rear-Side
30
5 Putting into Operation
33
Installation Site
33
Electrical Connections
34
Sensor Setup and Adjustments
35
Level Sensors
36
Cooling Water Flow Sensor
37
Foam Sensor
38
Vapor Temperature Sensor
40
Cooling Water Temperature Sensor
41
Battery Driven Lift Function at Power Failure
41
Setting up the Support Rod(S)
42
Condenser Clamps
43
Easyclamps
44
Inlet Valve
45
Glassware and Configurations
46
Additional Cleaning Measures for Food, Pharma and Cosmetic Applications
46
Primary Cleaning
46
Example for a Disinfection Via an Evaporation Cycle
47
Verification of the Disinfection Process
47
Controlled Contamination and Distillation
48
Disinfection
48
Sampling for Determination of the Germ Count
48
Final Cleaning and Drying
48
General Installation Instructions for Glassware
49
Single Receiver
51
Heating Bath Filling Level
55
Heating Bath Setup for 2×1800 W Heating Element
56
Water as Heating Transfer Medium
58
Heating Transfer Media with High Boiling Point
59
Heating Bath Setup for 4.2 and 6.3 Kw Heating Element
60
Attaching and Removing Evaporating Flasks
62
Adjusting the Snap Flange
64
Installation and Usage of a Shut-Off Tap
65
Vacuum Controller Installation / Removal
66
Controller Upgrade
67
Final Installation Check
67
6 Operation
68
Evaporation in Three Steps
68
Optimal Distillation Conditions
69
Solvent Table
70
7 Maintenance and Repairs
71
Customer Service
71
Regular Service and Checks
72
System Tightness
72
Sealings and Hoses
72
Glassware and Clamps
72
Housing, Heating Bath, Cables and Accessories
72
Snap Flange Coupling, Flask Seal and Vapor Duct
74
Distribution Head Seal and Vacuum Seal
77
8 Troubleshooting
79
Resetting the Over-Temperature Protection
79
Error Messages and Their Remedy
80
Resettable Automatic System Fuses
84
9 Shutdown, Storage, Transport and Disposal
85
Storage and Transport
85
Disposal
86
Lead-Acid Battery
86
10 Spare Parts
88
Reflux Glass Configurations
89
R' Configuration
90
RB' Configuration
91
C' Configuration
92
BASIC' Configuration
93
Decending Glass Configurations
94
D' Configuration
95
D2 HP' Configuration
96
D2' Configuration
97
DB' Configuration
98
DB2' Configuration
99
Receiving Vessel Parts
100
Optional Equipment and Upgrade Parts
105
Declarations and Requirements
106
4
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Buchi Rotavapor R-220 SE Specifications
General
Brand
Buchi
Model
Rotavapor R-220 SE
Category
Laboratory Equipment
Language
English
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