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Dionex UltiMate 3000 Series - User Manual

Dionex UltiMate 3000 Series
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UltiMate 3000 Series
SD, RS, and BM Pumps
Operating Instructions
(Original Operating Instructions)
Revision: 1.4
Date: September 2010
© 2010 Dionex
Doc. No. 4820.4001

Table of Contents

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Summary

Declaration of Conformity

Introduction

How to Use This Manual

Explains the manual's layout and structure for user reference.

Safety Information

Details safety warnings, symbols, and general precautions.

Intended Use

Describes the pump's design purpose and applications.

Federal Communications Commission (FCC) Note

Provides FCC compliance information for Class A digital devices.

Overview

Unit Description

Describes the pump as the heart of the UltiMate 3000 system and its key features.

Pump Configurations

Lists and describes the different UltiMate 3000 pump models available.

Operating Principle

Explains the serial dual-piston pump's operation with compressibility compensation.

Front Panel Elements

Identifies and describes the components on the pump's front panel.

Rear Panel

Details the connectors and ports located on the rear panel of the pump.

Installation

Facility Requirements

Outlines necessary environmental and power specifications for installation.

Unpacking

Provides instructions for unpacking the pump and inspecting for damage.

Positioning the Pump in the UltiMate 3000 System

Guides on stacking and interconnecting system modules for optimal setup.

Connecting the Pump

Details how to connect the pump to the computer and system components.

Preparation for Operation (Startup)

Overview of Actions

Lists the sequence of steps required to prepare the pump for operation.

General Precautions for Connecting Capillaries

Provides general guidelines and precautions for connecting capillaries.

Solvent Reservoirs

Details how to connect solvent reservoirs and related components.

Setting Up the Rear Seal Wash System

Guides on setting up the rear seal wash system for pump maintenance.

Connecting Drain Tubing

Explains how to connect the drain tubing for liquid discharge.

Purging the Pump

Describes the process of rinsing the pump system with solvent.

Equilibrating the System

Guides on equilibrating the HPLC system before starting sample analysis.

Operation and Maintenance

Power-Up

Describes the sequence of events when the pump is powered on.

Status Screens

Explains the information displayed on the pump's status screen.

Operation with Chromeleon

Details how to operate the pump using the Chromeleon software.

Function Keys and Menus on the Pump Display

Explains how to use function keys and menus for direct pump operation.

Information for Operating the Pump

Provides specific information on settings and functions for pump operation.

Special Chromeleon Functions

Overviews special functions Chromeleon supports for pump operation.

Shutting Down the Pump

Lists precautions and procedures for shutting down the pump.

Routine and Preventive Maintenance

Outlines recommended routine and preventive maintenance schedules.

Troubleshooting

Overview

Introduces features to help identify and eliminate operational problems.

Pump Block Status Indicator

Explains the operational status indicated by the pump block LED.

Messages on the Pump Display

Describes pump display messages and how to navigate them.

Chromeleon Diagnostics Messages

Details messages from Chromeleon diagnostic tests and their causes.

Operating Problems

Lists common operating problems, probable causes, and remedial actions.

Checking the Compression Values

Service

General Notes

Covers general precautions before performing maintenance or repair work.

Eliminating Leakage

Provides steps to identify, eliminate, and dry leaks detected by the sensor.

Rear Seal Wash System

Details inspection and maintenance procedures for the rear seal wash system.

Replacing the Check Valve Cartridges

Step-by-step guide for replacing the pump's check valve cartridges.

Pistons and Piston Seals

Information on pistons and piston seals, including disassembly and replacement.

Pistons and Piston Seals

Visually Inspecting the Pump for Piston Seal Leakage

Guides on visually inspecting the pump for leaks from piston seals.

Pump Head and Pistons

Details procedures for removing and installing the pump head and pistons.

Replacing the Piston Seals

Step-by-step guide for replacing the pump's piston seals.

Mixing System

Capillary Mixer

Details the replacement procedure for the capillary mixer.

Static Mixer

Guides on replacing the static mixer component.

Inline Filter

Replacing the Inline Filter (ISO-3100)

Steps for replacing the inline filter in ISO-3100 models.

Inline Filter (LPG-3400 BM, DGP-3600 BM)

Guides on replacing the inline filter in specific BM pump models.

Checking the Inline Filter for Permeability

Describes how to check the permeability of the inline filter.

Replacing the Purge Valve Knob

Testing the Pump for Leakage

Vacuum Degasser (Rinsing the Degassing Channels)

Replacing the Main Power Fuses

Updating the Pump Firmware

Pump-Specific Information

ISO-3100

Provides information on interior components, flow path, and operating principle for ISO-3100.

LPG-3400

Details interior components, flow path, and operating principle for LPG-3400.

DGP-3600

Covers interior components, flow path, and operating principle for DGP-3600.

HPG-3200

Provides details on interior components, flow path, and operating principle for HPG-3200.

HPG-3400

Covers interior components, flow path, and operating principle for HPG-3400.

Optimizing the Pump for Specific Applications

Technical Information

Accessories, Consumables, and Spare Parts

Standard Accessories

Lists the standard accessories shipped with the pump.

Optional Accessories

Lists optional accessories available for the pump.

Consumables and Spare Parts

Details consumables and spare parts for the pump, including part numbers.

Appendix

Digital I;O (Pin Assignment)

Details the pin assignments for the digital I/O ports.

Solvent Rack (Pin Assignment)

Provides pin assignment details for the Solvent Rack port.

Index

Dionex UltiMate 3000 Series Specifications

General IconGeneral
Flow Rate Range0.001 to 10 mL/min
Flow Rate Accuracy±1%
Flow Rate Precision< ±0.1% RSD
Pressure Range0 to 9000 psi (0 to 62 MPa)
Flow Accuracy±1%
Flow Precision<0.07% RSD
Gradient MixingHigh-pressure or low-pressure mixing
Compatible SolventsWater, methanol, acetonitrile, and other common HPLC solvents
Operating Temperature4°C to 40°C (39°F to 104°F)
Power Requirements100-240 V, 50/60 Hz

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