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Katanax K2 Prime - User Manual

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Automatic fluxer
2

Table of Contents

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Summary

Installation

Box contents

Lists essential accessories and optional items included with the fluxer.

Location

Details vent hood requirements, clearance, and table specifications for proper placement.

Connection

Specifies power requirements, voltage, and GFCI protection for connecting the instrument.

Introduction to Fusion and the K2 Prime

The fusion theory

Describes fusion as a sample prep technique for XRF, ICP, and AA analysis.

The K2 Prime fluxer

Introduces the K2 Prime as an evolution of the original K2, highlighting its sturdiness and ease of use.

Main Features and Operation

Accuracy

Highlights entirely automated, reproducible, and real-time temperature display features.

Safety

Details integrated safety shield and absence of hazardous gas emissions.

Simplicity

Mentions intuitive interface, easy installation, and low maintenance.

Precautions

High temperature

Warns about temperatures up to 1200°C and handling hot surfaces.

High voltage

Advises caution with 240 Volts AC and interlocked safety devices.

Acid spills

Advises against glass beakers due to acid spills and recommends PTFE beakers.

How the Unit Works

Heating

Explains the heating element alloy and temperature control via thermocouple.

Agitation and pouring of the melt

Describes melt homogenization via rocking and controlled pouring into molds.

Solution agitation

Describes how the optional module uses magnetic coils to agitate solutions in beakers.

Using the K2 Prime (basic)

Operation of the safety shield

Explains the function of the safety shield and its automatic/manual operation.

The main running screen

Details the graphical display, including temperature graph, status icons, and buttons.

Loading a program

Guides the user on how to select and start a fusion program using arrows and the start button.

The right ingredients

Flux blend

Discusses the use of lithium metaborate and tetraborate mixes and their ratios.

Flux-to-sample ratio

Provides a method to find the optimal ratio for homogeneous fusion disks.

Oxidizing agents

Explains the importance of sample oxidation and the use of reagents like Li2CO3 or LiNO3.

Programming the K2 Prime (advanced)

Unlocking the advanced mode

Explains the process of entering a password to enable parameter editing.

Managing fusion methods

Covers copying, renaming, deleting, and saving custom fusion methods.

Heating steps

Details the structure of heating steps and adjustable parameters like temperature and duration.

Global Parameters

Holding temperature offset

Explains how to maintain furnace temperature between fusions for quicker start-up.

Startup tolerance

Defines permissible temperature ranges for crucible entry into the furnace.

Special Parameters

Accessing the Special parameters

Instructs how to enter the Special parameters window using a padlock icon and code.

Twisting correction

Details enabling and adjusting automatic correction for holder twisting.

Offsets

Covers adjusting various mechanical motions and sensor sensitivities.

Fusion troubleshooting

Disk cracks

Lists causes for glass disk cracking, such as improper cooling or mold sticking.

Disk crystallizes

Explains crystallization causes like inappropriate flux or improper cooling.

Non-homogenous disk

Addresses issues like undissolved particles, oversaturation, or improper grinding.

Periodic inspection

Inspection schedule table

Provides a table detailing frequency, checkpoints, actions, and page references for inspections.

Holders alignment and functionality

Details procedures for verifying and adjusting holder alignment, movement, and screw tightness.

Element terminal connections

Outlines inspection of ceramic connectors and terminals for oxidation.

Service operations

Crucible holder removal

Provides step-by-step instructions for removing the crucible holder, including its middle section.

Mold holder removal

Guides on removing the mold holder, including its middle section and cantilever supports.

Adjustment of holders

Explains how to check and adjust holder positions for proper alignment and pouring.

Heating element replacement

Heating element removal

Details disconnecting power, removing panels, and detaching heating elements.

Element tube replacement

Outlines the process for installing or replacing protective clear tubes for heating elements.

Firmware and program transfers

Preset programs

Lists factory-programmed methods and their applicable sample types and descriptions.

Backup or restore by USB

Explains how to back up and restore firmware and fusion programs using a USB drive.

Technical specifications

Electrical

Lists voltage, frequency, power ratings, and breaker requirements.

Warranty

Contacting Katanax

Katanax K2 Prime Specifications

General IconGeneral
BrandKatanax
ModelK2 Prime
CategoryIndustrial Equipment
LanguageEnglish

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