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873 Biodiesel Rancimat
Metrohm 873 Biodiesel Rancimat User Manual
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873 Biodiesel Rancimat
Manual
8.873.8003EN
2
Table of Contents
Default Chapter
5
Table of Contents
5
1 Introduction
9
Instrument Description
9
Rancimat Method
10
About the Documentation
11
Symbols and Conventions
11
Safety Instructions
12
General Notes on Safety
12
Electrical Safety
13
Flammable Solvents and Chemicals
14
Recycling and Disposal
14
2 Overview of the Instrument
15
Setting up the Instrument
18
Packaging
18
Checks
18
Location
18
Mounting Accessories
18
Mounting Accessories for the Internal Air Supply
18
Mounting Accessories for the External Air Supply
21
Equipping the Reaction and Measuring Vessels
21
Inserting Vessels / Establishing Tubing Connections
24
Mounting the Exhaust Collection Tube (Optional Accessories)
24
Mains Connection
25
Checking the Mains Voltage
25
Replacing Fuses
26
Mains Cable and Mains Connection
26
Switching the Instrument On/Off
27
Connecting a PC
27
Connecting the 873 Biodiesel Rancimat and the PC
27
Installing the Software
27
Carrying out Basic Settings
29
Fundamentals of Operation
32
Starting and Exiting the Program
32
Terms
33
Control Window
33
Results Window
35
File Types
38
Context-Sensitive Menus
39
Mouse Functions
39
Help
40
Instrument and Program Settings
41
Establishing the Instrument Communication
41
Managing Access Rights
42
Timer
45
Gas Flow Control
47
Recording the Temperature
48
Optimizing Program and Database
49
Program Information
50
Instrument Information
50
Status Overview
52
Displaying, Filtering and Deleting Event Overview
53
Calibration Functions
56
Determining Cell Constants
56
Determining Delta T
58
Methods
63
Managing Methods
63
Parameter Description
68
Determinations
83
Preparing the Instrument and the Accessories
84
Preparing the Determination
85
Starting the Determination
87
Cleaning the Instrument and Accessories
88
Adjusting the Method Parameters During the Determination
89
Stopping the Determination Manually
89
Status of the Live Curve
90
Results
91
Determination Overview
91
Determination and Method Data
107
Graph and Reevaluation
116
Extrapolation
121
Recalculating a Determination
125
Printing and Exporting Data
132
Program Settings
139
Arranging Windows
145
GLP Functions
146
General Information on GLP and Validation
146
GLP Monitoring
146
GLP Status
148
Carrying out GLP Tests
149
GLP Results
159
5 Handling and Maintenance
163
General Information
163
Care
163
Maintenance by Metrohm Service
163
Replacing the Dust Filter
163
Regenerating or Replacing the Molecular Sieve
164
Self Test When Switching on
164
Quality Management and Validation with Metrohm
165
6 Troubleshooting
167
Problems
167
7 Technical Specifications
173
General Data
173
Temperature Regulation and Measurement
173
Conductivity Measurement
174
Gas Flow Regulation
174
GLP Test Set
175
RS-232 Interface
175
Mains Connection
175
Safety Specification
176
Electromagnetic Compatibility (EMC)
176
Ambient Temperature
176
Housing
177
8 Conformity and Warranty
178
Declaration of Conformity
178
Quality Management Principles
179
Warranty (Guarantee)
180
9 Accessories
181
Scope of Delivery
181
Optional Accessories
188
Index
191
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Metrohm 873 Biodiesel Rancimat Specifications
General
Brand
Metrohm
Model
873 Biodiesel Rancimat
Category
Laboratory Equipment
Language
English
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