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870 KF Titrino plus
Metrohm 870 KF Titrino plus User Manual
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870 KF Titrino plus
Manual
8.870.8003EN
2
Table of Contents
Default Chapter
5
Table of Contents
5
1 Introduction
11
Instrument Description
11
Titration and Measuring Modes
11
Connectors
11
Intended Use
11
About the Documentation
12
Symbols and Conventions
12
Safety Instructions
13
General Notes on Safety
13
Electrical Safety
13
Tubing and Capillary Connections
14
Flammable Solvents and Chemicals
14
Recycling and Disposal
14
2 Overview of the Instrument
16
Figure 1 Front 870 KF Titrino Plus
16
Figure 2 Rear 870 KF Titrino Plus
17
3 Water Determination According to Karl Fischer (KFT)
18
Figure 3 Reagent Dosing for KFT
18
4 Installation
19
Setting up the Instrument
19
Packaging
19
Checks
19
Location
19
Connecting a Sensor
19
Figure 4 Connecting a Polarizable Electrode
19
Connecting a Stirrer
20
Connecting a Balance
20
Figure 5 Connecting a Stirrer
20
Connecting Keyboard, Printer and Other USB Devices
21
Figure 6 Connecting a Balance
21
Figure 7 Connecting USB Devices
21
Figure 8 Connecting the USB Stick
23
Figure 9 Connecting the 6.2147.000 USB Keyboard with USB Stick and Printer
23
RS-232/USB Box (for Connecting Balances)
23
Connecting Instruments to the Remote Connector
24
Attaching the Exchange Unit
24
Figure 11 Connecting a Remote Cable
24
Figure 12 Attaching the Exchange Unit
24
5 Operation
26
Switching the Instrument on and off
26
Fundamentals of Operation
27
The Keypad
27
Structure of the Dialog Windows
27
Figure 13 Keypad 870 KF Titrino Plus
27
Navigating in the Dialog
28
Entering Text and Numbers
28
Selecting from a Selection List
29
Methods
30
Method Templates
30
Loading a Method
30
Saving a Method
31
Exporting a Method
31
Sample Data
32
Entering Sample Data in the Main Dialog
32
Requesting Sample Data at the Time of Determination Start
33
Carrying out a Determination
34
Live Modifications
37
Editing the Sample Data of the Running Determination
37
Live Parameters
38
Results
39
Statistics
40
Printing a Report Manually
41
Manual Control
43
Dosing
43
Stirring
47
6 System Settings
49
Basic Settings
49
Managing Solutions
52
General
52
Editing the Solution Data
53
File Management
54
Figure 14 Directory Structure on the USB Stick
55
Configuring External Devices
56
Instrument Diagnosis
58
Loading Program Versions and Language Files
58
Diagnosis Functions
60
7 Parameters
61
Karl Fischer Titrations (KFT)
61
Conditioning
61
Start Conditions
62
Control Parameters
63
Titration Parameters
66
Stop Conditions
68
Calculations - Methods "Blank Ipol/Upol
69
Calculations - Methods "Titer Ipol/Upol
70
Calculations - Methods "KFT Ipol/Upol", "KFT Ipol/Upol-Blank
71
Statistics
73
Reports
73
8 Handling and Maintenance
75
Quality Management and Validation with Metrohm
75
9 Troubleshooting
76
Karl Fischer Titration
76
Miscellaneous
77
10 Appendix
79
Exchange Unit
79
Maximum Dosing and Filling Rate
79
Parameters for the Preparing (PREP)
79
Stirring Rate
79
Balance
80
Figure 15 Rotational Speed Depending on Stirring Rate
80
USB Devices
81
Numerical USB Keypad 6.2147.000
81
Key Assignment of a USB Keyboard
81
PC Mouse
82
Printer
83
System Initialization
83
Remote Interface
84
Pin Assignment of the Remote Interface
84
Figure 16 Pin Assignment of Remote Socket and Plug
84
Status Diagram of the Remote Interface
85
Figure 17 Remote Status Diagram
85
Remote Control Via an RS-232 Connection
86
Figure 18 Connecting the RS-232/USB Box to the PC
86
Commands and Variables
87
11 Technical Specifications
89
Measuring Inputs
89
Polarizer
89
Dosing Drive
90
Interfaces
90
Mains Connection
90
Safety Specification
90
Electromagnetic Compatibility (EMC)
91
Ambient Temperature
91
Reference Conditions
91
Dimensions
92
12 Conformity and Warranty
93
Declaration of Conformity
93
Quality Management Principles
94
Warranty (Guarantee)
95
13 Accessories
96
Scope of Delivery
96
Optional Accessories
101
Index
103
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Installation And Tutorial
44 pages
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Metrohm 870 KF Titrino plus Specifications
General
Brand
Metrohm
Model
870 KF Titrino plus
Category
Laboratory Equipment
Language
English
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