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Parr Instrument 4703 - User Manual

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239M
4600 & 4700
General Purpose Pressure Vessels
Operating Instruction Manual
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Summary

Preface and Introduction

Scope and Intended Use

Manual scope, intended use as high-pressure reactor, and user responsibilities.

Safety Information

Provides essential safety precautions for electrical shock and personal injury.

Symbols, Conditions, and Handling

Symbols and Environmental Conditions

Defines symbols and specifies operating/storage conditions for the instrument.

Unpacking and Safe Handling

Instructions for unpacking, checking parts, and safe lifting/carrying of equipment.

User Responsibilities and Limits

Users Safety Responsibility

Outlines the user's fundamental role in safe operation, selection, and installation.

Pressure and Temperature Limits

Details how working pressure and temperature depend on vessel design and materials.

Vessel Closures

Split Ring Closure System

Explains the split ring cover clamp mechanism for securing vessel heads.

Screw Cap Closure System

Describes the threaded sleeve and screw cap closure used on smaller Parr vessels.

Closure Operation Procedures

Step-by-step instructions for opening/closing split ring and screw cap vessels.

Pressure Vessel Seals

Seal Types and Temperature Limits

Describes flat and O-ring seals, and their temperature limits up to 350°C.

High-Temperature Sealing

Discusses flexible graphite and metal gaskets for temperatures above 350°C.

Vessel Sealing Methods

Instructions on tightening compression bolts for sealing and O-ring self-sealing.

Gasket Sealing and Specifics

PTFE;Graphite Gasket Tightening

Bolt tightening for PTFE/graphite gaskets, including torque and pattern.

Metal Gasket Requirements

Details uniform loading and specific instructions for metal gasket applications.

Sealing 4740 High Pressure Vessels

Closing operations for Series 4740 vessels using screw caps and compression screws.

Vessel Head Fittings

Gage Block Assemblies

Describes assemblies combining inlet valve, pressure gage, and rupture disc.

Pressure Gages and Safety Discs

Information on pressure gages, rupture discs, limits, and safety precautions.

Coned Pressure Fittings

Explains coned fittings for connecting parts and forming rigid, leak-proof joints.

Fitting and Thread Specifications

Coned Fitting Details

Illustrates and details the components and use of coned pressure fittings.

Tapered Pipe Thread Information

Discusses tapered pipe threads, maintenance, and port enlargement for fittings.

Maintenance and Testing

General Maintenance Guidelines

General guidelines for inspecting connections, using wrenches, and applying lubricants.

Periodic Hydrostatic Testing

Procedures for hydrostatic testing of cylinders and criteria for discarding.

Assembly Guide and Material Data

Head Assembly Guide Reference

Table referencing head styles and their corresponding gage block assembly uses.

Material Designation Codes

Codes for alternative materials and gasket material designations with suffixes.

Series 4700 Working Limits and Parts

Series 4703-4714 Specifications

Working limits and parts list for Series 4703-4714 pressure vessels.

Series 4740 Vessel Details

Series 4740 Working Limits and Parts

Working limits, parts, and diagrams for Series 4740 pressure vessels.

Series 4750 Vessel Details

Series 4750 Working Limits and Parts

Working limits, parts, and diagrams for Series 4750 pressure vessels.

Series 4760-4777 Vessel Details

Series 4760-4777 Working Limits and Parts

Working limits, parts, and diagrams for Series 4760-4777 pressure vessels.

Series 4760 Q-47770 Vessel Details

Series 4760 Q-47770 Working Limits and Parts

Working limits, parts, and diagrams for Series 4760Q-47770 pressure vessels.

Series 4790 Vessel Configurations

4790 Flat Gasket & Split Ring

Working limits and parts for 4790 vessels with flat gaskets and split ring closures.

4790 O-ring Seal Variants

Working limits and parts for 4790 vessels with O-ring seals (screw cap or split ring).

Series 4600-4620 Working Limits and Parts

Series 4600-4620 Specifications

Working limits and parts list for Series 4600-4620 pressure vessels.

Series 4600 Q-46200 Vessel Details

Series 4600 Q-46200 Working Limits and Parts

Working limits and parts list for Series 4600Q-46200 pressure vessels.

Series 4605-4626 Vessel Details

Series 4605-4626 Working Limits and Parts

Working limits and parts list for Series 4605-4626 pressure vessels.

Series 4650 Vessel Details

Series 4650 Working Limits and Parts

Working limits and parts list for Series 4650 pressure vessels.

Series 4660 Vessel Details

Series 4660 Working Limits and Parts

Working limits and parts list for Series 4660 pressure vessels.

Series 46600 Vessel Details

Series 46600 Working Limits and Parts

Working limits and parts list for Series 46600 pressure vessels.

Series 4670-4674 Vessel Details

Series 4670-4674 Working Limits and Parts

Working limits and parts list for Series 4670-4674 pressure vessels.

Series 4676-4677 Vessel Details

Series 4676-4677 Working Limits and Parts

Working limits and parts list for Series 4676-4677 pressure vessels.

Series 4678-4679 Vessel Details

Series 4678-4679 Working Limits and Parts

Working limits and parts list for Series 4678-4679 pressure vessels.

Series 4680 Vessel Details

Series 4680 Working Limits and Parts

Working limits and parts list for Series 4680 pressure vessels.

Gage Block Assemblies

Gage Block Parts List

Lists all part numbers and descriptions for gage block assemblies.

Pressure Gage Specifications

Series 56 HC and 593 HC Gages

Lists part numbers and pressure ranges for 56HC and 593HC series pressure gages.

Gage Block Assembly Diagram

Gage Block Assembly Drawing

Illustrates the assembly of gage blocks with notes on anti-seize and torque.

Summary

Preface and Introduction

Scope and Intended Use

Manual scope, intended use as high-pressure reactor, and user responsibilities.

Safety Information

Provides essential safety precautions for electrical shock and personal injury.

Symbols, Conditions, and Handling

Symbols and Environmental Conditions

Defines symbols and specifies operating/storage conditions for the instrument.

Unpacking and Safe Handling

Instructions for unpacking, checking parts, and safe lifting/carrying of equipment.

User Responsibilities and Limits

Users Safety Responsibility

Outlines the user's fundamental role in safe operation, selection, and installation.

Pressure and Temperature Limits

Details how working pressure and temperature depend on vessel design and materials.

Vessel Closures

Split Ring Closure System

Explains the split ring cover clamp mechanism for securing vessel heads.

Screw Cap Closure System

Describes the threaded sleeve and screw cap closure used on smaller Parr vessels.

Closure Operation Procedures

Step-by-step instructions for opening/closing split ring and screw cap vessels.

Pressure Vessel Seals

Seal Types and Temperature Limits

Describes flat and O-ring seals, and their temperature limits up to 350°C.

High-Temperature Sealing

Discusses flexible graphite and metal gaskets for temperatures above 350°C.

Vessel Sealing Methods

Instructions on tightening compression bolts for sealing and O-ring self-sealing.

Gasket Sealing and Specifics

PTFE;Graphite Gasket Tightening

Bolt tightening for PTFE/graphite gaskets, including torque and pattern.

Metal Gasket Requirements

Details uniform loading and specific instructions for metal gasket applications.

Sealing 4740 High Pressure Vessels

Closing operations for Series 4740 vessels using screw caps and compression screws.

Vessel Head Fittings

Gage Block Assemblies

Describes assemblies combining inlet valve, pressure gage, and rupture disc.

Pressure Gages and Safety Discs

Information on pressure gages, rupture discs, limits, and safety precautions.

Coned Pressure Fittings

Explains coned fittings for connecting parts and forming rigid, leak-proof joints.

Fitting and Thread Specifications

Coned Fitting Details

Illustrates and details the components and use of coned pressure fittings.

Tapered Pipe Thread Information

Discusses tapered pipe threads, maintenance, and port enlargement for fittings.

Maintenance and Testing

General Maintenance Guidelines

General guidelines for inspecting connections, using wrenches, and applying lubricants.

Periodic Hydrostatic Testing

Procedures for hydrostatic testing of cylinders and criteria for discarding.

Assembly Guide and Material Data

Head Assembly Guide Reference

Table referencing head styles and their corresponding gage block assembly uses.

Material Designation Codes

Codes for alternative materials and gasket material designations with suffixes.

Series 4700 Working Limits and Parts

Series 4703-4714 Specifications

Working limits and parts list for Series 4703-4714 pressure vessels.

Series 4740 Vessel Details

Series 4740 Working Limits and Parts

Working limits, parts, and diagrams for Series 4740 pressure vessels.

Series 4750 Vessel Details

Series 4750 Working Limits and Parts

Working limits, parts, and diagrams for Series 4750 pressure vessels.

Series 4760-4777 Vessel Details

Series 4760-4777 Working Limits and Parts

Working limits, parts, and diagrams for Series 4760-4777 pressure vessels.

Series 4760 Q-47770 Vessel Details

Series 4760 Q-47770 Working Limits and Parts

Working limits, parts, and diagrams for Series 4760Q-47770 pressure vessels.

Series 4790 Vessel Configurations

4790 Flat Gasket & Split Ring

Working limits and parts for 4790 vessels with flat gaskets and split ring closures.

4790 O-ring Seal Variants

Working limits and parts for 4790 vessels with O-ring seals (screw cap or split ring).

Series 4600-4620 Working Limits and Parts

Series 4600-4620 Specifications

Working limits and parts list for Series 4600-4620 pressure vessels.

Series 4600 Q-46200 Vessel Details

Series 4600 Q-46200 Working Limits and Parts

Working limits and parts list for Series 4600Q-46200 pressure vessels.

Series 4605-4626 Vessel Details

Series 4605-4626 Working Limits and Parts

Working limits and parts list for Series 4605-4626 pressure vessels.

Series 4650 Vessel Details

Series 4650 Working Limits and Parts

Working limits and parts list for Series 4650 pressure vessels.

Series 4660 Vessel Details

Series 4660 Working Limits and Parts

Working limits and parts list for Series 4660 pressure vessels.

Series 46600 Vessel Details

Series 46600 Working Limits and Parts

Working limits and parts list for Series 46600 pressure vessels.

Series 4670-4674 Vessel Details

Series 4670-4674 Working Limits and Parts

Working limits and parts list for Series 4670-4674 pressure vessels.

Series 4676-4677 Vessel Details

Series 4676-4677 Working Limits and Parts

Working limits and parts list for Series 4676-4677 pressure vessels.

Series 4678-4679 Vessel Details

Series 4678-4679 Working Limits and Parts

Working limits and parts list for Series 4678-4679 pressure vessels.

Series 4680 Vessel Details

Series 4680 Working Limits and Parts

Working limits and parts list for Series 4680 pressure vessels.

Gage Block Assemblies

Gage Block Parts List

Lists all part numbers and descriptions for gage block assemblies.

Pressure Gage Specifications

Series 56 HC and 593 HC Gages

Lists part numbers and pressure ranges for 56HC and 593HC series pressure gages.

Gage Block Assembly Diagram

Gage Block Assembly Drawing

Illustrates the assembly of gage blocks with notes on anti-seize and torque.

Parr Instrument 4703 Specifications

General IconGeneral
BrandParr Instrument
Model4703
CategoryLaboratory Equipment
LanguageEnglish

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