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Thermo Electron Nicolet 4700 User Manual

Thermo Electron Nicolet 4700
170 pages
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Table of Contents

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Thermo Electron Nicolet 4700 Specifications

General IconGeneral
BrandThermo Electron
ModelNicolet 4700
CategoryMeasuring Instruments
LanguageEnglish

Summary

Welcome

About this manual

Explains how to use the system, OMNIC software, and spectrometer operation, maintenance, and service.

System requirements

Details the hardware and software specifications needed for the computer system.

Installing OMNIC

Provides instructions for installing the OMNIC software on your computer.

Before You Collect Spectra

Checking the purge

Details how to check and set the spectrometer's purge gas flow rate and pressure.

Turning on the system components

Step-by-step guide for powering on the spectrometer and associated accessories.

Starting OMNIC

Instructions on how to launch and access the OMNIC software.

Selecting an experiment

Explains how to load parameter settings for data collection experiments.

Your First Experiment

The OMNIC window

Describes the main OMNIC interface elements: spectral window, menu bar, and toolbar.

Collecting a sample spectrum

Guides users through the process of collecting a background and sample spectrum.

Installing the standard sample holder

Provides instructions and illustrations for installing the sample holder.

Spectrum Processing and Analysis

Saving the spectrum

Explains the procedures for saving collected spectral data using File menu options.

Labeling a peak with the annotation tool

Details how to use the annotation tool to add labels to spectral peaks.

Verifying the composition of the sample

Describes how to compare a collected spectrum with library spectra for identification.

Creating and printing a report

Guides users on creating and printing reports with spectral data and analysis results.

Spectrometer Basics

Spectrometer components

Identifies the main external components of the Nicolet 4700/6700 spectrometer.

Turning on the spectrometer power

Step-by-step instructions for powering on the spectrometer and system components.

Spectrometer Options

Using the filter wheel

Explains the function and use of the optional automated filter wheel accessory.

Using the energy screen wheel

Details how to use energy screens to prevent detector saturation and signal distortion.

Using the internal polarizer

Describes the optional automated polarizer for controlling IR beam polarization.

Accessories

Smart Accessories

Introduces Smart Accessories that integrate with the spectrometer and OMNIC software.

System accessories

Lists system accessories like power conditioners, air dryers, and purge gas generators.

How to cable an accessory

Provides guidance on connecting cables for accessories and peripherals.

Quick Answers to Your Questions

Using OMNIC

Answers common questions about collecting spectra, converting units, and using spectral libraries.

Using the Spectrometer

Addresses questions about energy screens, opening the spectrometer cover, and alignment.

Maintenance and Service

Running diagnostic tests on spectrometer components

Explains how to use diagnostic tests to check spectrometer component performance.

Maintaining your spectrometer

Covers procedures for spectrometer alignment and performance checks.

Troubleshooting

Software Problems

Lists common software issues with OMNIC and their solutions.

Hardware Problems

Addresses common hardware issues with the spectrometer and their resolutions.

Applications Problems

Provides troubleshooting steps for specific data collection and spectral analysis issues.

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