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Nicolet 4700
Thermo Electron Nicolet 4700 User Manual
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2
Table of Contents
Table of Contents
3
Welcome
7
About this Manual
8
Questions or Concerns
9
System Requirements
10
Installing OMNIC
11
Where to Find the Information You Need
12
Wizards and Tutorials
12
On-Line Help
13
Finding Answers to Your Questions
15
Before You Collect Spectra
20
Checking the Purge
21
Smart Purge Settings
22
Checking the Desiccant
23
Turning on the System Components
24
Cooling the Detector
25
Starting OMNIC
26
Selecting an Experiment
27
Your First Experiment
29
The OMNIC Window
30
Spectral Window
30
Menu Bar
31
Experiment Drop-Down List Box
31
Bench Status Indicator
32
Toolbar
32
Collecting a Sample Spectrum
33
Installing the Standard Sample Holder
34
Collecting the Sample Spectrum
36
How Do I Know if My Spectrum Is Good
43
Saving the Spectrum
43
Converting the Spectrum's Units
44
Labeling a Peak with the Annotation Tool
46
Verifying the Composition of the Sample
49
Creating a User Library
53
Adding a Spectrum to a User Library
53
Creating and Printing a Report
54
Spectrometer Basics
57
Spectrometer Components
57
Using the Data Collection Buttons
58
What's Inside
60
What Is on the Rear Panel
61
Turning on the Spectrometer Power
62
Using a Light Source
64
Using Beamsplitters and Detectors
66
Selecting the Right Beamsplitter and Detector
66
Improving the Quality of Your Spectral Data
70
How to Collect Data in the Visible Spectral Range
76
About the Moving Mirror Velocity
77
Spectrometer Options
78
Using the Filter Wheel
78
Using the Energy Screen Wheel
81
Using the Internal Polarizer
84
Accessories
87
Smart Accessories
87
Other Sampling Accessories for Different Applications
91
System Accessories
96
How to Cable an Accessory
97
Pass-Through Connectors
97
Detector/Motors Connector
101
Quick Answers to Your Questions about Using OMNIC
103
Collecting Spectra
103
Converting Spectra to Other Units
107
Using Spectral Libraries
108
Opening, Saving and Deleting Spectra
112
Printing
115
Displaying Spectra
116
Correcting Spectra
122
Subtracting, Adding, Multiplying and Dividing Spectra
122
Customizing OMNIC
125
Other Questions
126
Quick Answers to Your Questions about Using the Spectrometer
129
Maintenance and Service
134
Running Diagnostic Tests on Spectrometer Components
135
Maintaining Your Spectrometer
136
Aligning the Spectrometer
136
Aligning an Accessory
138
Checking Spectrometer Performance
138
Servicing Your Spectrometer
140
Troubleshooting Software Problems
141
Troubleshooting Hardware Problems
143
Performing Advanced Diagnostic Tests
154
Troubleshooting Applications Problems
156
Index
161
4
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Thermo Electron Nicolet 4700 Specifications
General
Brand
Thermo Electron
Model
Nicolet 4700
Category
Measuring Instruments
Language
English
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