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Thermo Scientific TriPlus 500 User Manual
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Thermo Scientific
T
riPlus 500
User Guide
Headspace Sampler
P/N 31716106
Revision A
January 2019
2
Table of Contents
Default Chapter
11
Default Chapter
11
Table of Contents
11
Preface
15
About Your System
16
Power Rating
16
Contacting Us
17
Related Documentation
17
Safety Alerts and Important Information
17
Special Notices
17
Safety Symbols and Signal Words
18
Instrument Markings and Symbols
19
Safety Information and Warnings
20
General Considerations
20
Electrical Hazards
21
Other Hazards
22
Working with Toxic or Other Harmful Compounds
23
Biological Hazards
23
Maintenance
24
Disposal
25
Writing Convention Used in this Guide
25
Chapter 1 Getting Familiar with Your Triplus 500 Headspace Sampler
27
Introduction
28
Instrument Basics
29
Label Location on the Instrument
33
Incubation Group
34
Sample Vial Carousel
34
Incubation Oven
35
Sampling Path
35
Pneumatic Connections
37
Electrical Connections
38
Status Panel
39
TRACE 1310 GC User Interface
41
Vial Loader
42
Vial Loader Electronic Module
43
Sample Trays
45
Vials Sequence Syntax
47
Positioning the Vials in the Sample Tray
48
Barcode Reader
49
About a Barcode Reader
49
Barcode Reader Description
50
Barcode Label Positioning
50
Heated/Cooled Tray
54
Triplus 500 Web Interface
55
Chapter 2 Operating Principles
57
Introduction to the Headspace Technique
58
Pneumatics
59
Analytical Cycle
60
Stand-By
60
Incubation
62
Pressurization
63
Leak Check
64
Loop Filling
65
Injection
66
Purging
68
Chapter 3 Setting up through the TRACE 1310 User Interface
69
User Interface Overview
70
Menu Icons
70
Data Entry Keys
71
Shortcut Key
72
Cursor Keys
72
Configuring the Instrument
73
Editing the Instrument Method
75
Performing Samples Sequence
79
Monitoring the Instrument Status
81
Information Page
82
Chapter 4 Setting up through Chromeleon CDS
83
Configuring the Triplus 500 HS through Chromeleon CDS
84
Hardware Configuration
85
HS Configuration
85
Error Handling
86
Editing Method Parameters through Chromeleon CDS
87
Incubation
88
Pressurization
88
Loop Filling
88
Injection
89
Venting and Purging
89
Chromeleon HS Sampler Control Panel
90
Vials Sequence
94
Chapter 5 Setting up through Tracefinder CDS
97
Configuring Triplus 500 HS through Tracefinder CDS
98
Connection
99
Hardware Configuration
99
User Configuration
100
HS Configuration
100
Error Handling
100
Editing Method Parameters through Tracefinder CDS
101
Incubation
102
Pressurization
102
Loop Filling
102
Injection
103
Venting and Purging
103
Advanced
104
Tracefinder Road Map Home Page Status Tabs
105
Method Development
107
Usage Notes
107
Chapter 6 Method Development
107
Temperatures
108
Carrier Gas Optimization
108
Auxiliary Gas Pressure Optimization
108
Shaking Conditioning
109
Sample Vials
109
Sample Vial Septa
109
Vial Filling
110
Vial Closure
110
Missing and Wrong Size Vials
111
Matrix Effects
111
Principles of Multiple Headspace Extraction (MHE)
112
Processing a Sample Vial
117
User Actions
118
Instrument Actions
118
Method Developing Workflow
123
Analytical Troubleshooting General Guidelines
128
Chapter 7 Using the Triplus 500 Web Interface
131
Introduction
132
Menu Bar
133
Login Menu
134
Administration Menu
134
Status Menu
135
Installation/Tools Menu
138
Service Menu
142
Manufacturing Menu
142
Logging out of the Triplus 500 Web Interface
142
Chapter 8 Ordering Parts
143
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Thermo Scientific TriPlus 500 Specifications
General
Brand
Thermo Scientific
Model
TriPlus 500
Category
Industrial Equipment
Language
English
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