EasyManua.ls Logo

VWR International sympHony User Manual

Default Icon
126 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
Cotter Corporation (N.S.L.)
Cañon City Milling Facility
Cañon City, Colorado
Procedure
Sampling Equipment
Decontamination
Number: SOP-E-044
Page 1 of 5
Revision: 1
Date: --/--/--
APPROVAL PAGE
SAMPLING EQUIPMENT DECONTAMINATION
APPROVALS
Environmental Coordinator:
Date:
Program Manager:
Date:
QA Manager:
Date:
Question and Answer IconNeed help?

Do you have a question about the VWR International sympHony and is the answer not in the manual?

VWR International sympHony Specifications

General IconGeneral
pH Range0.00 to 14.00 pH
pH Resolution0.01 pH
pH Accuracy±0.01 pH
mV Resolution1 mV
Temperature Resolution0.1 °C
Temperature Accuracy±0.5 °C
Calibration PointsUp to 5
Resolution0.01 pH, 1 mV, 0.1 °C
Temperature CompensationAutomatic (0 to 100 °C)
mV Range±1999 mV

Summary

Sampling Equipment Decontamination

1.0 Purpose

Describes the methods for decontamination of non-dedicated sampling equipment for water quality, soil, sediment, or vegetation sampling.

2.0 Scope

Applies to decontamination of all sampling equipment used during water, soil, sediment, or vegetation sampling by Cotter Corp.

3.0 References

Lists relevant documents including the Colorado Radioactive Materials License and QAPP.

4.0 Definitions

Provides definitions for terms like Reagent Grade Water, EDTA, and Field Staff.

5.0 Equipment and Materials

Details the necessary equipment and materials for sampling equipment decontamination.

6.0 Health and Safety

Outlines health and safety precautions, especially regarding acids and protective gear.

7.0 Responsibility

Defines responsibilities for the Environmental Coordinator and Field Staff.

8.0 Instructions

Provides step-by-step guidance for equipment decontamination for different sample types.

9.0 Records

Specifies the records to be maintained, such as field logbooks and conductivity values.

Oxidation Reduction Potential Measurements

1.0 Purpose

Describes activities for measuring Oxidation-reduction potential (ORP) in unfiltered water samples.

2.0 Scope

Applies to ORP measurements within a millivolt range for water quality samples.

3.0 References

Lists relevant documents including QAPP and Colorado Radioactive Materials License.

4.0 Definitions

Defines Oxidation-reduction potential (ORP) and its measurement correlation.

5.0 Appendices

Lists appendices containing offset correction factors and meter manuals.

6.0 Equipment and Materials

Details the required equipment and materials for ORP measurements.

7.0 Health and Safety

Provides health and safety precautions for handling ORP standards and reagents.

8.0 Responsibility

Assigns responsibility for following the ORP measurement procedure.

9.0 Equipment Inspection

Outlines procedures for inspecting the ORP meter and probes.

10.0 Equipment Calibration and Frequency

Details the calibration process, frequency, and recording requirements for ORP meters.

11.0 Measurement Instructions

Provides direct measurement instructions for ORP, including sample handling and calculations.

Chapter I Introduction

Convenient Meter Features

Highlights key features of the sympHony meter for electrochemistry measurements.

Chapter II Display

General Description

Describes the meter display, including icons for temperature, calibration, and measurement parameters.

Chapter III Keypad

General Description

Details the keypad layout for portable and benchtop sympHony meters.

Key Definitions

Explains the function of each key on the meter's keypad.

Chapter IV Preparation

Installing the Power Adapter

Instructions for connecting the universal power adapter to the meter.

Installing the Batteries

Guidance on installing AA alkaline batteries in the meter.

Connecting the Electrodes

Diagrams and instructions for connecting various electrodes and probes to the meter.

Turning on the Instrument

Steps for powering on the meter and toggling the display backlight.

Meter Maintenance

Routine maintenance procedures for cleaning and caring for the meter.

Chapter V Meter Setup

Setup Menu

Instructions on how to navigate and use the meter's setup menu.

Setup Menu Table

A comprehensive table listing all available setup menu options and descriptions.

Enabling or Disabling the Setup Menu Password

Procedure for setting up or disabling a password for the setup menu.

General Menu Settings

Configuration options for manual temperature, stirrer speed, and automatic shutoff.

Time and Date Settings

Instructions for setting the meter's current time and date format.

AUTO-READ™, Continuous or Timed Measurement Settings

Configuration for different measurement read types and timing modes.

Selecting the Measurement Parameter

Guide on choosing and displaying different measurement parameters on the meter.

Method Setup

Functionality for saving and managing up to 10 methods for calibration and measurement.

Chapter VI pH Technique

pH Setup Menu

Details on configuring pH measurement settings like resolution and buffer recognition.

pH Calibration

Step-by-step instructions for calibrating the pH electrode.

pH Measurement

Procedure for performing pH measurements using different modes.

mV, Relative mV and ORP Technique

Explanation of measuring and calibrating millivolt, relative mV, and ORP values.

Chapter VII Dissolved Oxygen Technique

Dissolved Oxygen Setup Menu

Configuration settings for dissolved oxygen measurements.

Dissolved Oxygen Calibration

Instructions for calibrating the dissolved oxygen probe using various modes.

Dissolved Oxygen Measurement

Procedure for taking dissolved oxygen measurements using different modes.

Chapter VIII Conductivity Technique

Conductivity Setup Menu

Settings for conductivity measurements, including temperature compensation and cell constant.

Conductivity Calibration

Steps for performing manual and automatic conductivity calibration.

Conductivity Measurement

Procedure for taking conductivity measurements using different modes.

Chapter IX ISE Technique

ISE Setup Menu

Configuration options for Ion Selective Electrode (ISE) measurements.

Preparation of Standards

Guidance on preparing calibration standards for ISE measurements.

Serial Dilutions

Method for preparing serial dilutions for calibration standards.

ISE Calibration

Procedure for calibrating the Ion Selective Electrode (ISE).

ISE Measurement

Procedure for taking Ion Selective Electrode (ISE) measurements.

Chapter X Data Archiving and Retrieval

Datalog and Calibration Log

Information on the meter's datalog capacity and calibration log.

Viewing and Downloading the Datalog and Calibration Log

Instructions for viewing, downloading, and sending data to printers or computers.

Chapter XI Declaration of Conformity

Chapter XII Troubleshooting

Meter Self Test

Procedure for running the meter's built-in self-test function.

Meter Error Codes

List of error codes, their descriptions, and troubleshooting steps.

General Troubleshooting

Common problems and solutions for meter operation and features.

pH Troubleshooting

Specific troubleshooting tips for pH calibration and measurement issues.

ISE Troubleshooting

Troubleshooting guide for Ion Selective Electrode (ISE) calibration and readings.

Conductivity Troubleshooting

Solutions for common problems encountered with conductivity measurements.

Dissolved Oxygen Troubleshooting

Troubleshooting steps for dissolved oxygen measurement and calibration issues.

Chapter XIII Meter Specifications

Meter Specifications

Environmental operating conditions and general specifications for the meters.

pH

Specifications for pH measurement range, resolution, accuracy, and calibration points.

Millivolts, Relative Millivolts, ORP

Specifications for mV, relative mV, and ORP measurement range, resolution, and accuracy.

ISE

Specifications for Ion Selective Electrode (ISE) measurement range, resolution, and accuracy.

Dissolved Oxygen

Specifications for dissolved oxygen measurement range, resolution, and accuracy.

Conductivity

Specifications for conductivity measurement range, resolution, and accuracy.

Temperature

Specifications for temperature measurement range, resolution, and accuracy.

Ordering Information

List of product codes and descriptions for meters and accessories.

Appendix A Special Meter Setup Menu Features

pH Setup Menu Features

Details on automatic buffer recognition for pH calibration.

Dissolved Oxygen Setup Menu Features

Features for barometric pressure compensation and salinity correction.

Conductivity Setup Menu Features

Information on temperature compensation and reference temperature settings.

ISE Setup Menu Features

Explanation of concentration range settings and automatic blank correction.

Vegetation Sampling

1.0 Purpose

Provides methods for collection, analysis, and reporting of vegetation samples.

2.0 Scope

Applies to vegetation samples collected during the growing season near air monitoring locations.

3.0 References

Lists relevant documents such as QAPP, SOP-E-044, and SOP-E-160.

4.0 Definitions

Defines terms like SSTF, LIMS, and Field Staff.

5.0 Equipment and Materials

Lists necessary equipment and materials for vegetation sampling.

6.0 Health and Safety

Outlines precautions for chemical hazards and plant contact hazards.

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Staff.

8.0 Instructions

Step-by-step guide for collecting vegetation samples, including labeling and QA procedures.

9.0 Records

Specifies records to be maintained, such as field logbooks and analysis reports.

Environmental Thermoluminescent Dosimetry

1.0 Purpose

Provides methods for collection, analysis, and reporting of environmental exposure rates.

2.0 Scope

Applies to environmental Thermoluminescent Dosimeters (TLDs) for exposure evaluation.

3.0 References

Lists relevant documents including QAPP and Colorado Radioactive Materials License.

4.0 Definitions

Defines TLD and Field Staff.

5.0 Equipment and Materials

Lists necessary equipment and materials for TLD deployment and collection.

6.0 Health and Safety

Outlines PPE requirements and awareness of local hazards like snakes and insects.

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Staff Sample Technician.

8.0 Instructions

Provides instructions for TLD frequency and procedures for deployment and collection.

8.1 Frequency

Specifies the quarterly frequency for replacing exposed TLDs.

8.2 Procedure

Details the process for EC receiving TLDs, providing them to staff, and deployment.

9.0 Records

Specifies the TLD dosimetry analysis report as the primary record.

Arkansas River Water Sample Collection

1.0 Purpose

Procedure for taking water quality samples from the Arkansas River.

2.0 Scope

Applies to water samples taken from the Arkansas River at specific locations.

3.0 References

Lists relevant documents including QAPP, SOP-E-044, and SOP-E-160.

4.0 Definitions

Defines Field Staff.

5.0 Equipment and Materials

Lists necessary equipment and materials for water sampling.

6.0 Health and Safety

Highlights safety precautions for equipment, river banks, and roadways.

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Sample Technician.

8.0 Instructions

Provides guidance on sampling frequency, locations, methods, and labeling.

9.0 Records

Specifies records to be maintained, such as field logbooks and tablets.

Soil Sampling

1.0 Purpose

Provides methods for collection, analysis, and reporting of soil samples.

2.0 Scope

Applies only to annual routine soil samples for public dose assessment.

3.0 References

Lists relevant documents including QAPP, SOP-E-044, and SOP-E-160.

4.0 Definitions

Defines SSTF and Field Staff.

5.0 Equipment and Materials

Lists necessary equipment and materials for soil sampling.

6.0 Health and Safety

Outlines standard worker safety and handling of equipment.

7.0 Responsibility

Defines responsibilities for EC, Field Staff, and QA Manager.

8.0 Instructions

Step-by-step guide for collecting soil samples, including depth, labeling, and QA procedures.

9.0 Records

Specifies records to be maintained, such as field logbooks and data sheets.

Radon Flux Measurement

1.0 Purpose

Standardizes methodology for measuring tailings impoundment Radon-222 emanation rates.

2.0 Scope

Applies to collecting radon flux samples and measuring emanation rates from the tailings impoundment.

3.0 References

Lists relevant documents including QAPP and EPA Method 115.

4.0 Definitions

Defines LACC (Large area charcoal canister) and Field Staff.

5.0 Equipment and Materials

Lists necessary equipment and materials for radon flux measurement.

6.0 Health and Safety

Outlines PPE requirements and cautions regarding pinch points in monitoring equipment.

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Sampling Staff.

8.0 Instructions

Provides instructions for canister deployment, retrieval, and decontamination.

8.1 Canister Deployment

Details the process for deploying radon flux canisters, including site criteria and labeling.

8.2 Canister Retrieval

Procedures for retrieving canisters, recording data, and preparing them for shipment.

8.3 Canister and Equipment Decontamination

Instructions for decontaminating canisters and associated equipment after testing.

9.0 Records

Specifies field data sheets or tablets as the required records.

Weather Monitoring

1.0 Purpose

Describes the meteorological monitoring program utilized by Cotter Corporation.

2.0 Scope

Applies to Cotter personnel inspecting, calibrating, and summarizing weather station data.

3.0 References

Lists relevant documents including QAPP and MET ONE sensor specifications.

4.0 Definitions

Defines Field Staff.

5.0 Equipment and Materials

Lists meteorological monitoring station equipment and materials.

6.0 Health and Safety

Outlines the use of appropriate personal protective equipment (PPE).

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Staff.

8.0 Instructions

Provides instructions for frequency of inspections, calibrations, and data handling.

8.1 Frequency

Specifies weekly, monthly, quarterly, and semiannual inspection and calibration frequencies.

8.3 Semiannually, calibrate the following sensors

Procedure for semiannual calibration of wind speed, direction, temperature, sigma, and rainfall sensors.

8.4 Monthly, download and reformat the meteorological data

Process for downloading, reformatting, and summarizing meteorological data for annual reports.

9.0 Records

Lists inspection and calibration reports, and summary reports as required records.

Field Global Positioning System Surveying

1.0 Purpose

Describes required standards, procedures, and performance criteria for GPS surveys.

2.0 Scope

Applies to global positioning system surveying activities conducted by Cotter Corporation.

3.0 References

Lists relevant geospatial positioning accuracy standards and data policies.

4.0 Definitions

Defines terms such as Field Staff, Vertical Accuracy, Horizontal Accuracy, and PDOP.

5.0 Equipment and Materials

Lists necessary equipment and materials for GPS surveying.

6.0 Health and Safety

Outlines safety precautions for equipment use, traffic, and weather conditions.

7.0 Responsibility

Defines responsibilities for QA Manager, EC, and Field Sample Technician.

8.0 Equipment Setup Instructions

Step-by-step guide for setting up GPS receivers and data collectors.

9.0 Survey Instructions

Procedure for conducting GPS surveys, including point measurement and data saving.

10.0 Accuracy Standards

Defines horizontal and vertical positional accuracy standards for GPS surveys.

11.0 Metadata

Specifies information that needs to be documented in the geospatial data metadata.

12.0 Records

Specifies field sampling logbooks, field data sheets, or tablets as records.

Related product manuals