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Spectroquant Prove 300
Merck Spectroquant Prove 300 Operating Manual
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Table of Contents
Contents
3
Photometry
8
Photometric Test Kits
10
Cell Tests
10
Additional Reagents
10
Reagent Tests
11
Notes for Practical Use
12
Measuring Range
12
Influence of Ph
13
Influence of Temperature
13
Time Stability
14
Influence of Foreign Substances
14
Suitability for Use in Seawater
14
Dosing the Reagents
15
Shelf-Life of the Reagents
15
Sample Preparation
16
Taking Samples
16
Preliminary Tests
16
Dilution
16
Filtration
17
Homogenization
18
Decomposition
18
Pipetting System
20
Analytical Quality Assurance (AQA)
22
Quality Control at the Manufacturer
22
Quality Control for the User
24
Checking the Spectrometer
25
Checking the Overall System
26
Checking the Pipettes
27
Checking Thermoreactors
27
Determination of Sample Influences (Matrix Effects)
28
Definition of Errors
28
Testing for Handling Errors
28
Overview
30
Scope of Delivery
30
Product View
30
Display and User Interface
31
Main Menu Navigation
32
Screen Layout Concentration Measurement Overview
33
Screen Layout Method List Overview
33
Screen Layout Results Overview
34
Main Menu Buttons
35
Safety
40
Intended Use
40
Function and Operational Safety
41
Target Group and User Qualification
41
Handling Hazardous Substances
41
General Notes on Handling
42
Initial Setup
42
Connecting the Power Supply
42
Connecting the Power Adapter
42
First Power-On
43
Language Setup
43
Date, Time and Country-Specific Settings
43
Self-Test
44
Connecting Optional Peripheral Devices
45
Communication Ports
45
Printer
45
USB Memory Device/Barcode Reader
45
Operation
46
Switching the Spectrometer on or off
46
Energy-Saving Mode - Display
47
Switching off
47
System Setup
48
Information
49
Interface (Setup 1)
49
Region (Setup 2)
50
Country Zone EU/US, Decimal Separator
51
Quality (Setup 3)
52
Automation (Setup 4)
53
User Management
54
Edit User, E.g. Change Password
54
Create User
54
Delete User
54
Service
55
Backup/Restore
55
Exporting Log And/Or System Files
55
Importing User-Defined Methods
55
Updates
56
Firmware and Method Update Spectrophotometer
56
Measurements
57
Performing a Measurement
58
Measuring with a Round Cell with a Round Cell with Closed Lid
58
Measuring with Rectangular Cells with Open Lid
58
Zero Adjustment
60
When to Repeat the Zero Adjustment
61
Zero Adjustment for User-Defined Concentration Methods
62
Zero Adjustment Procedure for Pre-Programmed Concentration Methods
62
Zero Adjustment for Ad Hoc Absorbance/Transmission Measurements
63
Zero Adjustment for Ad Hoc Kinetic Measurements
64
Zero Adjustment for Ad Hoc Spectra
65
Zero Adjustment (Baseline) Procedure for Ad Hoc Spectrum Measurement
65
Zero Adjustment for User-Defined Kinetic Methods
66
Zero Adjustment for User-Defined Spectrum Methods
67
Method List
68
Selecting a Method Manually
68
Searching and Filtering the Method List
68
Programmng a User-Defined Method
69
User-Defined Concentration Methods
70
Calibration Data/Calibration Function for Single-Wavelength Methods
70
Programming/Mofifying User-Defined Methods (Single Wavelength)
71
Enter Value Pairs
72
Measure Value Pairs
72
Enter a Function
73
Calculated Calibration Function
73
Entering Coefficients
73
Calibration Data and Calibration Function of Multi-Wavelength Methods
74
Programming/Modifying User-Defined Methods (Multi-Wavelength)
74
Programming a User-Defined Spectrum Method
78
Programming a User-Defined Kinetic Method
80
Copying/Duplicating a User-Defined Method
82
Modifying a User-Defined Method from the Method List
83
Deleting a User-Defined Method from the Method List
84
Export User-Defined Method to a USB Memory Device
85
Measuring in Concentration Mode
86
Measuring Cell Tests with a Barcode
86
Measuring Reagent Tests with Autoselector
88
Measuring Reagent-Free Tests and User-Defined Methods
88
Exceeding the Upper or Lower Limits of the Measuring Range
89
Method-Specific Settings for Concentration Mode
90
Measuring Diluted Samples
91
Sample Blank Value
92
Reagent Blank Value
93
Automatic Turbidity Correction
95
User Recalibration (Standard Adjustment)
96
Calibration of Value Pairs for User-Defined Methods
96
Value Pair Calibration
97
Matrixcheck
99
If Spiking Is Active
101
If Diluting Is Active
101
Ad Hoc Measurement
102
Ad Hoc ABS/TRANS Measurement
103
Ad Hoc Spectrum Measurement
104
Ad Hoc Kinetic Measurement
105
Spectrum - General Information
106
Recording the Spectrum
106
Baseline
106
Content of the Information Bar in Spectrum Measurements
107
Evaluating a Spectrum
108
Kinetics
110
Recording Kinetics
110
Evaluating a Kinetic
111
AQA (Analytical Quality Assurance)
112
Spectrophotometer Monitoring (AQA1)
112
Photometric Accuracy
112
Total System Monitoring (AQA2)
113
Wavelength Accuracy
113
Stray Light Test
113
Spectral Resolution
113
AQA Overview
114
Perform AQA1 Status Check
115
Perform AQA2 Status Check
116
AQA1 Selection List
117
Activating and Deactivating an AQA1 Test
118
Editing an AQA1 Test
118
Performing an AQA1 Test
120
Creating a User-Defined AQA1 Test
122
AQA2 Selection List
123
Activating and Deactivating an AQA2 Test
124
Editing an AQA2 Test
124
Performing an AQA2 Test
126
Perform Pipecheck
128
Timer
130
Results and Measurement Datasets
131
Displaying the Results
132
Show Details of One Result
133
Filtering Results to Further Process Measurement Datasets
134
Panorama - Value Control Card
135
Print Results and Measurement Datasets
136
Export Results and Measurement Datasets
137
User Groups
138
User Rights in Detail
138
Activating/Deactivating the User Management Function
139
Create an Administrator/User Account
140
Edit or Delete a User
141
Login/Logout
142
Change Password with User Rights Only
143
To Logout as User or Administrator
143
Maintenance and Cleaning
144
Exchanging the Buffer Battery
144
Exchanging the Halogen Lamp (Prove 100)
144
Disposal of Batteries
144
Cleaning the Housing and Display
146
Cleaning the Cell Compartment
146
Cleaning the Cell Compartment Cover and the Rear Cavity
148
Cleaning the Detector Lens
149
Error Causes and Troubleshooting
150
Technical Data
152
Accessories and Test Media
158
Glossary
160
List of Smart Icons on Display
162
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Merck Spectroquant Prove 300 Specifications
General
Brand
Merck
Model
Spectroquant Prove 300
Category
Measuring Instruments
Language
English
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