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15-3200-074
Teledyne Tekmar 15-3200-074 User Manual
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Atomx XYZ
User Manual
Part Number: 15-3200-074
Rev
: B, June - 2018
2
Table of Contents
default chapter
3
Table of Contents
3
Essential Instructions
13
Teledyne Tekmar Customer Support Center
13
Warranty
13
Notations and Hazard Severity Levels
14
Atomx XYZ Safety Symbols Defined
15
Atomx XYZ Safety Labels
17
Working Safely
20
CE Mark
21
Explanation of Regulatory Marks
21
Unit Disposal
21
Chapter 1: Introduction
23
Atomx XYZ with Methanol Extractions Overview
23
Purge and Trap Background
23
Purge and Trap Fundamentals
23
Brief History
24
Purge and Trap Operation Overview
24
Headspace Equilibrium Diagram
25
Trapping, Adsorption and Desorption
26
Atomx XYZ Specifications
27
General Specifications
27
Performance Specifications
28
Sample Needle
29
Liquid Samples
29
Low-Level Solid Samples
29
High-Level Solid Samples
29
Internal Standard Injection
30
Sample Gas Handling and Requirements
30
Electrical Requirements
31
Atomx XYZ Component Overview
33
Sample Mount and Sparger
35
Vials
35
Internal Standard Pressure Regulator
36
Internal Standard Vessels
36
Syringe Drive with Sweepable 25 Ml Syringe
37
Sample Needle
37
XYZ Autosampler Pick and Place Assembly
38
Elevator
38
Elevator and Sample Vial Cup
38
Vial Mixer Assembly
39
Status Light
39
Vial Mixer
39
Unit Status Light
39
Sample Purge Gas Inlet
40
Mass Flow Controller (MFC)
40
Sample Pathway
40
Analytical Trap
41
Moisture Control System (MCS)
41
Carrier Gas Inlet Line/Heated Sample Transfer Line
42
Carrier Gas Inlet Line and Heated Sample Transfer Line
42
Valving
43
Heated 6-Port Valve
44
Soil Valve
44
Optional Accessories
45
Sparge Vessel Heater
45
6-Port Syringe Valve
45
Vial Chiller Plate
46
Guardian Foam Sensor and Eliminator
46
Chapter 2: Installation and Setup
47
Pre-Installation
47
Overview
47
Operating Environment
47
Work Surface Requirements
48
Electrical Requirements
48
Gas Supply Requirements
49
Minimum Computer Requirements
50
Required Tools and Supplies for Installation and Operation
50
Unpacking the Atomx XYZ
51
Installation Kit Box
51
Installation Kit Box Label
51
Atomx XYZ System Overview
52
Back of Atomx XYZ
53
Electrical and Data Connections
54
AC Power Cord
54
Atomx XYZ Power Entry Module
54
GC I/O (Input/Output) Connection
55
GC I/O Cable Connection
55
Gas Connections
56
Connecting the Atomx XYZ Sample Purge Gas Supply
56
Sample Purge Gas Tubing
56
Atomx XYZ Carrier Gas Supply and Heated Sample Transfer Line Connection to the Gas Chromatograph (GC)
57
Atomx Carrier Gas Line, Heated Sample
57
Transfer Line and Purge Gas Tubing Connections
57
Liquid Connections
59
Drain Tubing
59
DI Water Reservoir Connection
59
Optional Methanol Reservoir Connection
60
Optional Vial Chiller Plate Tubing Connections
61
Methanol Supply Tubing
61
Install Atomx XYZ Teklink Software
62
Release Notes
63
License Agreement
63
Connect the USB Interface Cable
68
Create an Instrument Profile
68
Options Tab
69
Leak Check Tab
70
Guardian Foam Sensor and Foam Eliminator (Optional)
71
Connected and Default Profile
71
Atomx XYZ with Guardian Foam Sensor
72
Atomx XYZ with Guardian Foam Sensor and Foam Eliminator
72
Configuring the Guardian Foam Sensor & Eliminator
72
Preparing DI Water
73
Methanol Supply Grade
73
Preparing Working Standards
74
Working Standard Sample Calculation
74
Chapter 3: Atomx XYZ Teklink Software Overview
75
About Atomx XYZ Teklink Software
75
The Atomx XYZ Teklink Software Environment
75
Touchscreen Capability
75
Pinnable" Screens
76
Title Bar
76
Schedules Screen Title Bar
76
Open, Save, Load, and Print Buttons
77
Instrument Control Buttons
77
Control Buttons
77
Delete at Next Archive Check-Box
78
Delete at Next Archive Check-Box - Schedule Screen
78
Open Schedule Dialog Source Drop-Down Menu
78
Primary Screens
79
The Home Screen
79
Home Screen
79
Instrument Status Panel
80
Methods Screen
81
Standby Tab
81
Purge Tab
82
Soil Methods Screen - Purge Tab
84
Methanol Extraction Methods Screen - Purge Tab
85
Desorb Tab
86
Bake Tab
87
Water Methods Screen - Bake Tab
87
Schedules Screen
88
Methanol Methods Screen - Bake Tab
88
Tools Screen
90
Prime Menu
91
Commands Menu
91
System Menu
94
Leak Check Dialog
96
System Properties Dialog
97
System Properties - Data Tab
98
About Dialog
101
Diagnostics
102
Arm/Elevator
103
Pumper Diagnostics
104
Upgrade Firmware Dialog
104
Benchmark Test
105
Upgrade Firmware Dialog
105
Add, Connect and Deactivate an Instrument Profile
106
Add an Instrument Profile and Connect
106
Options Tab
107
Deactivate an Instrument Profile
108
Leak Check Tab
108
Using the Methods Screen
109
Methods Types
109
Default Methods
109
Configuration Dialog Showing Current Instrument Profile
109
Open a Method
110
Creating a Custom Method
110
Choose Method Type
110
Load the Method
113
Print a Method
113
Using the Schedule Screen
113
Open Schedule
113
Create a Schedule
113
Schedules Screen - Blank Schedule
113
Schedules Screen Right-Click Options
114
Select Method Dialog
115
Sample ID Column
115
Save Schedule
116
Select Standard Drop-Down
116
Print Schedule
117
Load (Run) the Schedule
117
Step Schedule
118
Hold Schedule
118
Schedule Hold - Instrument Status Panel
118
Abort a Sample or Schedule
119
Completion of the Schedule
119
Data Storage Location and Archiving Data
120
System Properties - Data Tab
120
Chapter 4: Instrument Operations
121
Atomx XYZ Mode Descriptions
121
Atomx XYZ Valve Output/Mechanism Chart
123
Waters
123
Soils
125
Methanol Extraction
126
Optimization/Method Development
128
Purge Mode
130
Dry Purge Mode
130
Desorb Ready Mode
130
Desorb Pre-Heat Mode
130
Desorb Mode
131
Bake Mode
131
Method Parameters
132
Water
132
Soil
133
Methanol Extraction
134
Analytical Trap Recommended Operating Conditions
135
Chapter 5: Maintenance and Troubleshooting
137
Maintenance Safety
137
Replacing Parts
137
Preventative Maintenance Checks
138
Daily Maintenance Checks
138
Weekly Maintenance Checks
138
Monthly Maintenance Checks
139
Quarterly Maintenance Checks
139
Preventative Maintenance Chart
140
GC In/Out (I/O) Cable and GC Type Reference
141
Instrument Access Panels
142
Front of the Atomx XYZ
142
Right Side of Atomx XYZ
143
Analytical Trap Compartment and Sparger Panel Open
143
Plumbing Overview
144
Plumbing Components
144
Electrical Overview
146
Printed Circuit Boards
146
Printed Circuit Board Locations - Atomx XYZ Concentrator
147
Printed Circuit Board Locations - Autosampler
147
CPU Communication Board (Master Board)
148
Multi-Channel Temperature Control Board
149
DC Valve Control Board
150
Internal Standard Valve Control Board
151
Banner Board/Status Light
152
XYZ Interface Board (XYZ) (Sidekick Board)
152
XYZ Control Board (Incrediboard)
153
XYZ Input/Output Board (Generic Aux IO Board)
153
Elevator Drive Board (ASX 7200 W-Axis Driver Board)
154
Power Supplies
154
System Leak Check
155
System Leak Check Flow Diagram
157
Leak Check Failed - Check Sub-System a
158
Sub-System a Leak Check Flow Diagram
159
Leak Check Failed - Check Sub-System B
160
Sub-System B Leak Check Flow Diagram
161
Leak Check Failed - Check Sub-System C
162
Sub-System C Leak Check Flow Diagram
163
Leak Check Failed - All Sub-Systems Checked and Passed
164
Glassware Good Practices Cleaning Procedures
164
Sparger Cleaning
164
Verifying/Setting Internal Standard Vessel Pressure
165
Verify the Internal Standard Vessel Pressure
165
Setting the Internal Standard Vessel Pressure
166
Sample Needle Replacement
167
Tools and Supplies
167
Procedure
167
Sparger Replacement
169
Analytical Trap Replacement
171
Analytical Trap Conditioning
173
Analytical Trap Recommended Conditioning Settings
173
Procedure
173
Elevator Lubrication
174
Tools and Supplies
174
Procedure
174
XYZ Autosampler Cleaning Procedure
175
Monthly Autosampler External Cleaning
176
Quarterly Autosampler Cleaning
176
XYZ Autosampler Alignment
176
When Is Alignment Needed
177
Alignment Overview
177
Tools and Supplies
178
Procedure
178
Syringe Initialization
190
Syringe Replacement
190
Power Entry Module (PEM) Fuse Replacement
190
Multi-Channel Temperature Control Board Fuse Replacement
193
Main Fuse
193
Multi-Channel Temperature Control Board
193
Heater Output Fuses
195
Diagram - Heater Output Fuses
196
Upgrade Concentrator Firmware
197
Download Firmware
197
Upgrade Board Firmware
198
Upgrade Autosampler Firmware
198
File Selected
200
Upgrade Atomx XYZ Teklink Software
201
Troubleshooting
202
Benchmark Test
202
Benchmark Test
203
No Power Flow Chart
204
No Response Flow Chart
205
Low Response Flow Chart
206
Carryover Contamination Flow Chart
207
Returning the Atomx XYZ
208
Prepare for Shipment Function
208
Unit and Parts Disposal
208
Technical Assistance
208
Teledyne Tekmar Customer Support
208
Appendix A: Diagrams
209
Atomx XYZ Concentrator Electrical Schematic
209
Atomx XYZ Autosampler Electrical Schematic
210
Atomx XYZ Plumbing Diagram
211
Atomx XYZ Flow Diagrams
213
Atomx XYZ - Basic Flow Diagram
213
Atomx XYZ - Waters Flow Diagram - Standby/Purge Ready
214
Atomx XYZ - Waters Flow Diagram - Standby Purge Ready
214
Atomx XYZ - Waters Flow Diagram - Sample Fill
215
Atomx XYZ Waters Flow Diagram - Sample Transfer
216
Atomx XYZ - Waters Flow Diagram - Sample Transfer
216
Atomx XYZ Waters Flow Diagram - Purge
217
Atomx XYZ - Waters Flow Diagram - Purge
217
Atomx XYZ Waters Flow Diagram - Dry Purge
218
Atomx XYZ - Waters Flow Diagram - Dry Purge
218
Atomx XYZ Waters Flow Diagram - Desorb
219
Atomx XYZ - Waters Flow Diagram - Desorb
219
Atomx XYZ Waters Flow Diagram - Bake Rinse Fill
220
Atomx XYZ - Waters Flow Diagram - Bake Rinse Fill
220
Atomx XYZ Waters Flow Diagram - Bake Rinse Transfer
221
Atomx XYZ - Waters Flow Diagram - Bake Rinse Transfer
221
Atomx XYZ Waters Flow Diagram - Bake Rinse Drain
222
Atomx XYZ - Waters Flow Diagram - Bake Rinse Drain
222
Atomx XYZ Waters Flow Diagram - Bake
223
Atomx XYZ - Waters Flow Diagram - Bake
223
Atomx XYZ Soils Flow Diagram - Standby/Purge Ready
224
Atomx XYZ - Soils Flow Diagram - Standby/Purge Ready
224
Atomx XYZ Soils Flow Diagram - DI Transfer to Vial
225
Atomx XYZ - Soils Flow Diagram - DI Transfer to Vial
225
Atomx XYZ Soils Flow Diagram - Purge
226
Atomx XYZ - Soils Flow Diagram - Purge
226
Atomx XYZ Soils Flow Diagram - Dry Purge
227
Atomx XYZ - Soils Flow Diagram - Dry Purge
227
Atomx XYZ Soils Flow Diagram - Bake
228
Atomx XYZ - Soils Flow Diagram - Bake
228
Atomx XYZ Methanol Flow Diagram - Fill
229
Atomx XYZ - Methanol Flow Diagram - Fill
229
Atomx XYZ Methanol Flow Diagram - Dispense to Vial
230
Atomx XYZ - Methanol Flow Diagram - Dispense to Vial
230
Atomx XYZ Methanol Flow Diagram - Extract Fill
231
Atomx XYZ - Methanol Flow Diagram - Extract Fill
231
Atomx XYZ Methanol Flow Diagram - Dispense Extract to Glassware
232
Atomx XYZ - Methanol Flow Diagram - Dispense Extract to Glassware
232
Atomx XYZ - Eliminator Flow Diagram - Basic
233
Atomx XYZ - Eliminator - Ready
234
Atomx XYZ - Eliminator Flow Diagram - Ready
234
Atomx XYZ - Eliminator Flow Diagram - Add Defoamer
235
Atomx XYZ - Eliminator Flow Diagram - Rinse
236
Sample Mount and Sparger
237
Mass Flow Controller
237
Moisture Control System
237
Syringe
242
No Response Flow Chart
242
Low Response Flow Chart
242
Liquid Handling
242
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Teledyne Tekmar 15-3200-074 Specifications
General
Brand
Teledyne Tekmar
Model
15-3200-074
Category
Laboratory Equipment
Language
English
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