Home
Teledyne Tekmar
Laboratory Equipment
Torch
Teledyne Tekmar Torch User Manual
177 pages
Manual
Specs
Ask a question
To Next Page
To Next Page
Loading...
T
or
ch U
ser M
anual
w
w
w
.t
eledynet
ek
mar
.c
om
User Manual •
P
ar
t # 15-0300-074
2
Table of Contents
default chapter
4
Table of Contents
4
Chapter 1: Introduction
10
Essential Instructions
11
Safety
12
Safety Symbols
12
Working Safely
13
Introduction
14
TOC Theory
14
TOC Overview
15
NDIR Pressurization Overview
15
What Is the Torch
16
Component Overview
18
Banner Display
18
Syringe Pumper and 7-Port Valve
18
IC Sparger
19
Combustion Furnace
19
Halogen Scrubber
19
Moisture Control System (MCS)
19
Non-Dispersive Infrared (NDIR) Detector
20
Flow Restrictors
20
Mass Flow Controller (MFC)
21
Acid Container
21
Autosampler
22
Chapter 2: Installation & Setup
23
Pre-Installation
24
Before You Begin
24
Utility Requirements for the Torch
24
Minimum Computer Requirements
25
Required Tools and Supplies for Installation
25
Installation
26
Bench Placement
26
Installing the Combustion Tube
26
Furnace Setup
26
Furnace Quick Disconnect Power Fitting
26
Packing the Combustion Tube
26
Electrical and Data Connections
27
Power Cord
27
I/O Cable
28
Ethernet Crossover Cable
28
Water, Reagent, and Gas Connections
29
Connecting the Torch to a DI Water Supply
30
Connecting the Torch to an Acid Supply
30
Connecting the Torch to the Waste Container
31
Using Nuts and Ferrules Supplied with the Torch
31
Connecting the Torch to a Gas Supply
32
Installing the Drain Tray and Carousel
33
Installing the Drain Tray
33
Installing the Carousel
33
Hardware Install Complete
34
Chapter 3: Materials, Reagents, and Standards
35
Preparing Reagents and Standards
36
Materials and Reagents
36
Reagent Water (H2O)
36
Nitric Acid (HNO3)
36
Laboratory Glassware Cleaning Solution
36
Potassium Hydrogen Phthalate
36
Glassware
37
Pipettors and Plastic Tip Pipettes
37
Analytical Balance
37
Procedure for Glassware Cleaning
38
Preparation of Reagent Solutions
39
Preparation of 21% Acid Reagent (Weight/Weight)
39
KHP 1000Ppmc 1 Liter
39
Formula for Preparation of Standards
40
Preparation of Working Calibration Solutions
40
20Ppmc Working Calibration Solution
40
Formula for Working Calibration Solutions
40
Chapter 4: Toc Teklink Tm Software Setup
41
Toc Teklink Tm Setup Overview
42
Toc Teklink Tm Software Installation
42
Stand-Alone Torch Configuration
42
External PC Torch Configuration
42
Installing the Microsoft .NET 2.0 Framework from the Menu
43
Instrument Communication
44
RS232 Connection
44
Computer TCP/IP Configuration
44
Starting Toc Teklink
46
First Login: External PC
46
First Login: Internal PC
46
Instrument TCP/IP Configuration
47
Editing Network Settings
49
Adding a New Instrument
49
Toc Teklink Basics
50
Using the Mouse
50
Using the Keyboard
50
Key Points of Interest for User Interface
50
Using the Menus
50
TOC Teklink TM Help
51
About Torch Teklink TM
51
User Account Management
52
User Manager
52
Add New User
52
Change Password
52
Reset Password
53
User Properties
53
General Tab
53
Permissions Tab
53
Comments Tab
53
Instrument Management
54
Main Application
54
TOC Teklink TM Buttons and Menus
55
File Menu
55
View Menu
56
Instrument Menu
56
Tools Menu
57
Maintenance Tasks Submenu
57
Windows Menu
58
Help Menu
58
Instrument Manager
59
Instrument Configuration
60
General Tab
60
Configuration Tab
61
Advanced Tab
62
Comments Tab
62
System Properties
63
General Tab
63
Archive Tab
63
Change Justification Tab
64
CSV Export Tab
64
Diagnostics
65
Valves & Flows Tab
65
Pumper Tab
66
Autosampler Tab
66
Benchmark Tab
67
Analogue Board Tab
68
Firmware Update
68
Calibration Editor
69
Method Editor
70
General Tab
70
Advanced Tab
71
Comments Tab
72
Standards Editor
72
Standards Tab
72
Options Tab
72
Schedule Editor
73
Samples Tab
74
Options Tab
74
Comments Tab
75
Sample Analysis
75
Instrument Blank
75
Report
76
Static Overview Tab
76
Interactive Tab
77
Chapter 5: Optional Total Nitrogen Module
79
Tn Analysis Overview
80
Torch with Total Nitrogen Module
80
Technical Specifications
82
Component Overview
83
Ozone Generator
83
Photomultiplier Tube
84
Ozone Scrubber
84
Analysis Process
84
Total Carbon with Total Nitrogen (TC/TN)
84
Total Organic Carbon with Total Nitrogen (TOC/TN)
85
Total Carbon Minus Inorganic Carbon with Total Nitrogen (TC-IC/TN)
85
Installation
86
Before You Begin
86
Unpack and Inspect
86
Bench Placement
86
Installation of the TN
86
Connect Oxygen Supply to Ozonator
87
Make Plumbing Alterations
88
Initial Start-Up
88
Preventative Maintenance
89
Preventative Maintenance Checklists
89
Daily Checks
89
Weekly Maintenance Checks
89
Monthly Maintenance Checks
89
Preventive Maintenance Chart
90
Replacing Parts
91
Removing the Detector Assembly
91
Chapter 6: Tutorial
92
Software Tutorial
93
Login
93
Connecting to an Instrument
93
TOC Teklink TM Main
94
Creating a New Calibration
94
Creating a New Method
95
Creating a New Standard
95
Creating a New Schedule
97
Running the Schedule
99
Review
100
Exporting a Report
101
Chapter 7: 21 Cfr 11 Compliance
102
21 CFR 11 Features and Compliance Tools
103
User Manager
103
Setting up User Accounts
104
User Permissions
104
Edit an Existing Account
105
Time-Out
105
Lockout
106
Data Versioning, History, and Archive
107
Report Data Security
107
Electronic Signatures
107
View/Print System History and Error Logs
109
Change Justification
110
Chapter 8: System Operations
111
System Operations
112
Instrument Preparation
112
General Daily Startup Routine
112
Accessing Data Offline
112
Disabling an Existing Instrument
112
Creating a New Instrument with a Dummy Address
112
Understanding the Analysis Types
113
Sample Introduction
114
Total Organic Carbon (TOC)
115
Total Carbon (TC)
115
Inorganic Carbon (IC)
116
Total Carbon Minus Inorganic Carbon (TC-IC)
116
System Clean
116
System Blank
116
Calibration
117
Calibration Overview
117
Methods
118
Selecting the Correct Methods
119
Method Variables
119
Selecting Standards
119
Selecting Check Standard Concentrations
119
Schedule Setup
120
Optimizing Results
120
Special Applications
121
Sample Preservation for TOC
121
Hydrochloric Acid (Hcl)
121
Applications
122
Low-Level Carbon
122
High Acid Content
122
High Fraction of Inorganic Carbon
122
Chapter 9: Maintenance & Troubleshooting
123
Preventive Maintenance Checklist
124
Daily Maintenance Checks
124
Weekly Maintenance Checks
124
Monthly Maintenance Checks
124
Preventive Maintenance Chart
125
Replacing Parts
126
Combustion Tube and Catalyst
127
Packing the Combustion Tube
127
Removing the Combustion Tube
127
Installing a New Combustion Tube
128
Injection Line Needle
128
Making a 1/2Ml Injection Line Needle
128
Replacing the Injection Line Needle
129
Furnace / TC Probe
130
Furnace Fans
131
Condensing Loop Fan
131
Mist Trap
132
Copper (Cu) and Tin (Sn) in Halogen Scrubber
132
Permeation Dryer
133
Autosampler Needle
134
7-Port Valve
135
3-Way Valve
137
Motor Control Printed Circuit Board (PCB)
137
DC Control PCB
138
Analog Board
138
Fuse
139
Power Entry Module (PEM)
139
5VDC Power Supply
140
12VDC Power Supply (Stand-Alone Version Only)
140
24VDC Power Supply
141
Mass Flow Controller (MFC)
142
Syringe Pumper
142
NDIR Detector
143
Pressure Regulator
144
Leak Checking the Torch
145
Isolating a Leak and Manual Leak Checking
145
Furnace Path
145
IC Flow Path
147
Troubleshooting the Torch
148
Arm Adjustment
149
Carousel Adjustment
149
Troubleshooting Chart
150
Returning the Torch
151
Unit and Parts Disposal
151
Chapter 10: Glossary
152
Acronyms
153
Terms
154
Chapter 11: Diagrams
156
Electrical Schematic - Torch
157
Electrical Schematic - Tn Module
158
Torch Flow Diagrams - Basic
159
Dispense Acid
160
Dispense Sample to IC Sparger
161
Drain Mode
162
IC Sparge
163
Pressurize Furnace
164
Pull Acid
165
Pull Sample
166
Pull Sparged Sample
167
Sample Inject
168
System Sweep
169
Torch & Tn Flow Diagrams - Basic
170
TN Sample Flow
171
Index
172
Need help?
Do you have a question about the Teledyne Tekmar Torch and is the answer not in the manual?
Ask a question
Teledyne Tekmar Torch Specifications
General
Brand
Teledyne Tekmar
Model
Torch
Category
Laboratory Equipment
Language
English
Related product manuals
Teledyne Tekmar Atomx XYZ
244 pages
Teledyne Tekmar 15-3200-074
244 pages
Need help?
General
To Next Page
