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Thermo Scientific HAAKE RotoVisco 1 User Manual

Thermo Scientific HAAKE RotoVisco 1
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Instruction Manual
HAAKE RotoViscoHAAKE RotoVisco
HAAKE RotoViscoHAAKE RotoVisco
HAAKE RotoVisco
®®
®®
®
1 1
1 1
1
HAAKE RheoStressHAAKE RheoStress
HAAKE RheoStressHAAKE RheoStress
HAAKE RheoStress
®®
®®
®
1 1
1 1
1
version 2.3
“Translation of the original instruction manual“

Table of Contents

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Thermo Scientific HAAKE RotoVisco 1 Specifications

General IconGeneral
BrandThermo Scientific
ModelHAAKE RotoVisco 1
CategoryMeasuring Instruments
LanguageEnglish

Summary

Declaration of Conformity

Key to Symbols

Symbols Used in Manual

Explains symbols used in the instruction manual for user guidance and warnings.

Symbols Used on Unit

Describes symbols found directly on the unit for operational and safety information.

CE and WEEE Compliance

CE Sign Information

Details the meaning and implications of the CE marking on the product.

WEEE Compliance

Explains compliance with the Waste Electrical & Electronic Equipment Directive.

Quality Assurance and Contacts

Quality Assurance

Outlines the company's commitment to ISO 9001:2008 quality management standards.

Thermo Fisher Scientific Contacts

Provides contact information for inquiries and support in Germany and internationally.

Warranty Information

Warranty Details

Specifies maintenance intervals required to maintain warranty validity and recommended service procedures.

Safety Notes and Warnings

General Safety Instructions

Provides critical safety instructions and warnings for proper and safe operation of the rheometer.

Unpacking and Ambient Conditions

Transportation Damage and Delivery Contents

Details procedures for handling transportation damage and lists standard accessories included in the delivery.

Sensor Systems Overview

Describes various sensor systems available for rheometers and their suitability.

Temperature Control Unit Accessories

Lists accessories like hoses and nozzles required for temperature control units.

Application Software

Mentions the HAAKE RheoWin software for instrument control and data analysis.

Installation Space and Mains Supply

Specifies recommended space, layout, mains connection, and fuse insertion for installation.

Cooling Air and Air Supply Requirements

Explains cooling air needs for measuring heads and specifications for air supply.

Air Compressors and Ambient Conditions

Recommends oil-free compressors and specifies environmental conditions for testing.

Unit Description

Introduction to Rheometer Operation

Explains basic rheological measurement principles (CR vs. CS modes) and CS mode benefits.

HAAKE RotoVisco1 Features

Details measurement modes like Thixotropy, Time Curve, Temp. Programs, and Yield Point.

HAAKE RheoStress1 Features

Describes measurement capabilities including Flow Curves, Time Curves, Temp. Programs, Viscoelasticity.

Temperature Control Options

Lists and describes various temperature control units and their temperature ranges.

Main Features of HAAKE Rheometers

Highlights key features like quick-fitting sensors, controlled lift, and software capabilities.

Installation Procedures

Setting Up the Rheometer

Guides on unpacking, placing, and leveling the rheometer using its adjustable feet and spirit level.

Connecting System Components

Explains how to connect the instrument, control unit, PC, and printer via RS232 and other interfaces.

PT100 Sensor Connections

Details the PT100 sensor connections (input and output) for specific temperature control units.

Hose Connections for Liquid Temperature Control

Provides instructions on connecting hoses for liquid temperature control units, including flow direction.

Air Bearing Cooling Connection

Specifies the connection for cooling air required for the air bearings of RheoStress1 models.

Functional Elements

Temperature Control Units Overview

Presents a table showing the compatibility of temperature control units with HAAKE RotoVisco1 and RheoStress1.

External Filter Installation and Function

Describes the purpose and installation of the external filter for protecting temperature control units.

Measuring Instrument (No Temperature Control)

Identifies front-panel components of the measuring instrument without a temperature control unit.

Rear Panel Connections Overview

Identifies rear-panel connections like power, RS232, printer, cooling air, and PT100.

Measuring Instrument with TCL/Z Unit

Identifies front-panel components of the measuring instrument with a TCL/Z temperature control unit.

Rear Panel Connections (TCL/Z Unit)

Identifies rear-panel connections for the instrument with TCL/Z unit.

Measuring Instrument with TCL/P, TCE/P, TCP/P, TCP/PE Units

Identifies front-panel components for instruments with specific temperature control units.

Rear Panel Connections (TCL/P Units)

Identifies rear-panel connections for instruments with TCL/P, TCE/P, TCP/P, TCP/PE units.

Measuring Unit with TCE/PC and Cone Heater TC1

Identifies front-panel components of the unit with TCE/PC stabilization and cone heater TC1.

Rear Panel Connections (TCE/PC + TC1)

Identifies rear-panel connections for the unit with TCE/PC stabilization and cone heater TC1.

Measuring Instrument with SHRP Unit

Identifies front-panel components of the instrument with SHRP temperature control unit.

Rear Panel Connections (SHRP Unit)

Identifies rear-panel connections for the instrument with SHRP temperature control unit.

Display Unit Operation

Explains the functions of the display unit, including header, keys, and general screen layout.

Diagnosis and Date/Time Settings

Describes diagnostic functions and how to set the date and time via the display unit.

Display Settings and Unit Selection

Covers display contrast, unit switching, country settings, and online value/graph configuration.

Data Memory Management

Explains how to access and manage stored measurement data.

Menu Navigation and Lift Control

Guides on navigating display unit menus and controlling the instrument's lift mechanism.

Operator, Sample Name, and Batch ID Setup

Describes defining and selecting operator, sample names, and batch IDs within the interface.

Configuring and Executing Measurement Sequences

Guides on setting up measurement sequences, defining jobs, and initiating tests.

Operating the Rheometer

Switching On the Instrument

Provides step-by-step instructions for powering on the rheometer and initial device checks.

Working with the Display Unit Menu

Guides on navigating the display unit menus, starting with the Configuration submenu.

Starting the Software (RheoWin)

Provides instructions for launching the RheoWin software and connecting to the measuring device.

Upload Mode for Display Unit

Explains the "Upload Mode" for operating the device independently of the PC for programming or data transfer.

Torque Compensation and Inertia Correction

Explains torque compensation and inertia correction for accurate measurement results.

Data Upload and Management

Details data upload, communication records, and managing user/sample/sensor data.

Creating and Uploading JOBS

Describes creating measurement procedures (JOBS) and uploading them to the device.

Measuring Results and Data Import

Describes viewing, printing, and importing measurement results into RheoWin.

Quick Cut-off Function

Describes the quick cut-off switch and its function to interrupt measuring jobs, drive, and heating.

Temperature Control Units

Temperature Control Unit TCO

Explains the function of the TCO unit, measurement of torque, and temperature calculation.

Temperature Control Unit TCL/Z

Details the TCL/Z unit, beaker insertion, hose connections, and circulator placement.

Temperature Control Unit TCL/P

Describes the TCL/P unit, its plate, temperature ranges, and high-temperature measurement recommendations.

Temperature Control Unit TCE/P

Explains the TCE/P unit, its plate, temperature ranges, and the role of the solenoid valve in cooling control.

Temperature Control Unit TCP/P and TCP/PE

Describes TCP/P and TCP/PE units using Peltier elements for temperature control.

Peltier Module Operation and Cooling/Heating

Explains the Peltier process, cooling coil operation, recommended liquids, and heating/cooling rates.

Temperature Stabilisation Unit TCE/P with Cone Heater TC1

Details the TCE/P unit with TC1 for high-temperature measurements up to 350°C.

Cone Heater TC1 Operation

Explains the PID controller, independent heating elements, and use of ceramic shafts with TC1.

Compressed Air Distributor for TC1

Describes the compressed air distributor setup, depending on building supply or HAAKE compressor.

Temperature Control Unit SHRP

Focuses on the SHRP unit for bitumen and asphalt testing, dynamic modes, and temperature ranges.

Sensor Systems Overview

Cylinder Sensor Systems

Introduces various cylinder sensor systems, including immersion discs, coaxial cylinders, and their standards.

Calculation Factors and Measuring Ranges

Explains calculation factors, shear stress (τ) range, and shear rate (γ) range.

Viscosity (η) Range Calculation

Details how to calculate the viscosity measuring range based on shear stress and shear rate ranges.

Cylinder Sensor Systems Z-DIN

Describes Z-DIN cylinder systems for polymer dispersions, ease of cleaning, and suitability for temperature programs.

Geometry and Calculation Equations (Z-DIN)

Provides geometric definitions and calculation equations for Z-DIN systems.

Cylinder Sensor System Z-DIN Specifications

Lists detailed specifications and calculation factors for Z10DIN, Z20DIN, and Z34DIN sensors.

Calculation Equations to DIN 53019/ISO 3219

Presents shear stress, shear rate, and deformation calculation equations according to DIN 53019/ISO 3219.

Cylinder Sensor System Z Specifications

Lists detailed specifications and calculation factors for Z31, Z38, and Z41 sensors.

Geometry and Calculation Equations (Cylinder System Z)

Provides geometric definitions and calculation equations for Cylinder System Z sensors.

Double Gap Cylinder Sensor DG43

Describes the DG43 sensor for low viscous liquids and small volumes, noting its double shearing surfaces.

Geometry and Calculation Equations (DG43)

Details the geometry and calculation equations for the DG43 double gap cylinder sensor.

Double Gap Cylinder Sensor DG43 Specifications

Lists detailed specifications and calculation factors for the DG43 sensor.

Solvent Trap for Z10-Z41 and DG43

Shows the solvent trap accessory for specific cylinder sensor systems.

Solvent Trap for Z43

Shows the solvent trap accessory for the Z43 cylinder sensor.

Cone-Plate and Plate-Plate Sensor Systems Application

Discusses the application of cone-plate and plate-plate sensors for viscous liquids and precision measurements.

Cone-Plate Sensor Systems Characteristics

Highlights cone radius and cone angle as key characteristics of cone-plate sensor systems.

Cone-Plate Calculation Equations

Presents shear stress and shear rate calculation equations for cone-plate sensors.

Cone/Plate Measuring Errors

Discusses common errors in cone/plate measurements, such as incorrect gap or filling.

Cone-Plate Sensor System (0.5° Angle) Specifications

Lists specifications and calculation factors for C20/0.5, C35/0.5, and C60/0.5 cone-plate sensors.

Cone-Plate Sensor System (1° Angle) Specifications

Lists specifications and calculation factors for C20/1, C35/1, and C60/1 cone-plate sensors.

Cone-Plate Sensor System (2° Angle) Specifications

Lists specifications and calculation factors for C20/2, C35/2, and C60/2 cone-plate sensors.

Cone-Plate Sensor System (4° Angle) Specifications

Lists specifications and calculation factors for C20/4, C35/4, and C60/4 cone-plate sensors.

Plate-Plate Sensor Systems

Explains plate-plate sensor systems, determined by plate radius and variable distance.

Plate-Plate Calculation Equations

Presents shear stress, shear rate, and deformation calculation equations for plate-plate sensors.

Plate-Plate Measuring Errors

Discusses errors related to incorrect gap or filling in plate-plate sensor systems.

Graphical Determination of Structural Exponent 'n'

Explains graphical methods for determining the 'n' exponent in non-Newtonian flow behavior.

Plate-Plate Sensor System with Variable Distance Specifications

Lists specifications and calculation factors for PP20, PP35, and PP60 plate-plate sensors.

Platter-Platter Measuring Equipment with Profiled Surface

Describes specialized platter-platter geometries for tests with wall slip, and necessary software adjustments.

High Shear Cylinder Sensor System HS Application

Explains the application of the HS system for high shear rate viscosity measurements and shear stability.

High Shear Cylinder Sensor System HS Specifications

Lists specifications and calculation factors for HS25, HS100, and HS400 sensors.

SHRP Plate-Platte Sensor System PP 1 mm Specifications

Lists specifications and calculation factors for SHRP PP 1 mm plate-plate sensors.

Immersion Sensor System FL Application

Describes the FL system for measuring thixotropic substances like cremes and gels, preserving sample structure.

Optional Sensor Systems

Optional Sensor Systems Compatibility

Provides a compatibility table for optional sensors with HAAKE RotoVisco1 and RheoStress1.

Hints on Measurement

Temperature Programs with Series 1 Units

Warns about thermal expansion and its effect on measurements, suggesting solutions.

Range Limits in Oscillation (RheoStress 1)

Illustrates the operational range limits for oscillation measurements with RheoStress 1.

Correction of Dynamic Measurement (RheoStress 1)

Explains mechanical and electromagnetic influences on dynamic measurements and the need for corrections.

Determination of Mass Moment of Inertia

Details methods for accurately determining the mass moment of inertia of the sensor system.

Maintenance and Care

General Maintenance Guidelines

Provides essential care instructions, including avoiding impacts, cable care, and cleaning precautions.

Maintenance Instructions for HAAKE RheoStress1

Outlines the annual system check and recommended maintenance tasks for the RheoStress1.

Maintenance Instructions for HAAKE Rotovisco1

Lists the annual system check and recommended maintenance tasks for the Rotovisco1.

Filter Unit Maintenance

Explains the filter unit's connection to the air supply and the procedure for filter replacement.

Flat Sieve Maintenance

Details the procedure for changing or cleaning the flat sieve in the tempering unit.

Instrument Repairs and Service

Advises against opening the unit and directs users to the Thermo Fisher Scientific service department.

Pin Wiring and Connections

RS232 Interface Connection

Describes the pin assignments for connecting the rheometer to a computer via RS232.

Centronics Connection

Details the pin assignments for the Centronics printer connection.

Display Unit Connection

Lists pin assignments for connecting the optional display unit.

PT100 Sensor Connections (Input/Output)

Explains PT100 sensor connections for TCO, TCL/P, and TCL/Z units.

External Connections

Shielded Cables and PT100 Sensor

Emphasizes using shielded cables and proper shielding contact for EMC requirements and PT100 sensor wiring.

Technical Specifications

HAAKE RV1 and RS1 Model Specifications

Lists key technical specifications like torque, speed, frequency, and bearing type for RV1 and RS1 models.

Dimensions, Weight, and Power Requirements

Provides physical dimensions, weight, mains voltage, frequency, and fuse ratings for various configurations.

Rheological Measurement Terms

Rheometrical Measuring Modes

Categorizes measurement modes (CD, CR, CS) and describes their application in rheological testing.

Signal Forms in Steady Rotation

Classifies steady rotation measurements into Creep/Recovery, Stress Growth/Decay, and Ramps.

Oscillating Movement (OSC)

Explains oscillation measurements for determining elastic and viscous properties, including moduli.

Flow Properties and Viscosity Behaviors

Defines common viscosity behaviors like Newtonian, Pseudoplastic, Dilatant, Thixotropic, Rheopectic, and Plastic.

Quantities in Rheometry and Rheology

Lists typical instrument, measuring, rheometrical, and rheological quantities and parameters.

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