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Dynisco LMI 4000 Series - User Manual

Dynisco LMI 4000 Series
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Dynisco Polymer Test Systems
LMI 4000
Series
Melt
Indexer
Manual
Version 4.1
38 Forge Parkway
Franklin, MA 02038
Phone +1 508 541 9400
Fax +1 508 541 6206
Manual Part Number: M0704 www.dynisco.com
Original Language Version

Table of Contents

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Dynisco LMI 4000 Series Specifications

General IconGeneral
StandardsASTM D1238, ISO 1133
Die Bore Diameter2.095 mm (0.0825 in)
Die Length8.000 mm (0.315 in)
Cylinder Diameter9.550 mm (0.376 in)
Piston Diameter9.474 mm (0.373 in)
Test MethodsProcedure A
Accuracy±0.5%
Repeatability±0.5%
Power Supply50/60 Hz
DescriptionMelt Flow Indexer

Summary

Introduction

Pneumatic Lift

Accessory for Flow Ratio tests, enabling safe weight handling.

Getting Started

Bench Requirements and Placement

Guidelines for optimal laboratory bench setup and placement.

Pneumatic lift setup

Step-by-step guide for installing the pneumatic lift system.

Installing the Digital Encoder

Instructions for installing the digital encoder module.

Installation Steps (See Figure 1)

Detailed steps for attaching encoder components and plates.

Safety

Use gloves, its HOT!

Warning about high temperatures and the risk of burns.

Electrical Hazard

Precautions regarding electrical safety and high voltage components.

Calibration Thermometers use Mercury

Safe handling and precautions for mercury thermometers.

Pinch Points

Warning about potential pinch hazards from moving parts or weights.

Fumes from Materials

Precautions and recommendations for materials emitting hazardous fumes.

Pre-Run Check List

Essential checks to perform before operating the instrument.

Series 4000: A Guided Tour

Setup

Navigating instrument configuration and system parameters.

Edit

Procedure for editing test programs and parameters.

Run

Executing configured test programs.

Navigating the Keypad

Guide to using the instrument's keypad for operation.

Configuring the Instrument

Selecting CALIB (Calibration) in the SYS Mode

Accessing various calibration options within the SYS mode.

Selecting TEST in the SYS Mode

Accessing instrument test functions within the SYS mode.

The SETUP mode

Configuring system settings and instrument options.

Programming

Procedures for creating, recalling, and saving test programs.

Method A Run Parameters

Defining and entering parameters specific to Method A tests.

Method A;B Run Parameters

Defining and entering parameters for Method A/B tests.

Method B Run Parameters

Defining and entering parameters for Method B tests.

RATIO (Flow Ratio) run parameters

Defining and entering parameters for Flow Ratio tests.

Run a Program

Initiating and executing a configured test program.

Method A Run

Calculations: Method A

Formula for calculating Melt Flow Rate (MFR) in Method A.

Enter Run Parameters

Inputting specific parameters for the Method A experiment.

Loading the Sample

Step-by-step guide for loading the sample into the barrel.

RUN

Initiating the test run after sample loading.

Weigh the Sample

Weighing the collected sample for accurate MFR calculation.

Method A;B Run

Calculations: Method A;B

Formulas used for calculating apparent melt density in Method A/B.

Programming Method A;B

Setting up a Method A/B test program.

Machine Setup

Configuring the instrument for a Method A/B test.

Inserting the Timing Flag

Steps for inserting the timing flag for measurement.

Making the Cut

Procedure for cutting the extrudate sample.

Method B Run

Calculations: Method B

Formulas for calculating Melt Volumetric Flow Rate (MVR) in Method B.

Method B Flags Setup

Setting up timing flags for Method B testing.

Programming Method B

Setting up a Method B test program.

The Actual Run

Executing the Method B test procedure.

How to do it: Step by Step

Step-by-step guide for performing the actual test.

Instrument Prep

Preparing the instrument and verifying settings before the run.

Loading the Barrel

Procedure for loading the barrel with the sample material.

Cleaning Up

Cleaning procedures after completing the Method B test.

Flow Ratio Runs

Flow Rate Ratio - How to Do It

Step-by-step guide to performing the Flow Rate Ratio test.

Intrinsic Viscosity Runs with PET

How to do it

Procedures for performing Intrinsic Viscosity calculations on the indexer.

Charge Weight

A-Standard Operating Procedure

Instrument Preparation

Steps for preparing the instrument for standard operating procedures.

Conducting the Test

Detailed steps for conducting the standard operating procedure test.

Clean Up

Procedures for cleaning the instrument after tests.

Out of Control Action List

The Digital Encoder: Use and Calibration

Method B Encoder Option

Details specific to the digital encoder option for Method B.

Digital Encoder Installation

Step-by-step guide for installing the digital encoder.

Programming for use with the Digital Encoder

Setting up and programming the digital encoder for use.

Complete Digital Encoder Calibration

Full calibration procedure for the digital encoder.

Instrument Calibration

Digital Encoder Calibration

Calibrating the digital encoder.

Instrument Maintenance and Troubleshooting

Maintenance

Routine maintenance procedures for the instrument.

Troubleshooting

General troubleshooting guide for common issues.

Pneumatic Lift Troubleshooting

Troubleshooting the pneumatic lift system.

Questions and Answers

Typical Problems

Common problems encountered and their solutions.

USB Setup

PC and Daisy Instructions

Setting up USB communication with Daisy software.

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