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Dynisco 4002 - User Manual

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Dynisco Polymer Test Systems
LMI 4000
Series
Melt
Indexer
Manual
Version 4.1
38 Forge Parkway
Franklin, MA 02038
Phone +1 508 541 9400
Fax +1 508 541 6206
Manual Part Number: M0704 www.dynisco.com
Original Language Version

Table of Contents

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Dynisco 4002 Specifications

General IconGeneral
BrandDynisco
Model4002
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction

Method B Encoder Option

Pneumatic Lift

Getting Started

Pneumatic lift setup

Installing the Digital Encoder

Safety

Use gloves, its HOT!

Warning about high temperatures and burn prevention.

Electrical Hazard

Caution regarding high voltage inside the instrument housing.

Pinch Points

Fumes from Materials

Series 4000: A Guided Tour

Edit

Inputting parameters for experiments and subsequent calculations.

Run

Procedure for programming, loading, and starting experiments.

Navigating the Keypad

Keypad Definitions

Configuring the Instrument

Selecting CALIB (Calibration) in the SYS Mode

Selecting TEST in the SYS Mode

The SETUP mode

Programming

Method A Run Parameters

Method A;B Run Parameters

Method B Run Parameters

RATIO (Flow Ratio) run parameters

Method A Run

Programming a Method A

Steps to create or edit a Method A program.

Machine Setup

Loading the Sample

Making the Cut

Weigh the Sample

Cleaning Up

Method A;B Run

Programming Method A;B

Machine Setup

Entering run parameters for Method A/B.

The Actual Run

Instrument Prep

Preparing the instrument and verifying program data for Method B.

Loading the Barrel

Instructions for loading the sample into the barrel for Method B.

Inserting the Timing Flag

Method B Run

Method B Flags Setup

Choosing a Timing Flag

Timing Flag and Starting the Run

Flow Ratio Runs

Flow Rate Ratio test and the Pneumatic Lift Option

Details on Flow Rate Ratio tests and using the pneumatic lift.

Flow Rate Ratio - How to Do It

Step-by-step guide for performing a Flow Ratio test.

Intrinsic Viscosity Runs with PET

Calculating PET I.V. from the Melt Indexer

How the Melt Indexer correlates MFR to Intrinsic Viscosity.

How to do it

Charge Weight

A-Standard Operating Procedure

Instrument Preparation

Steps for preparing the instrument before testing.

Conducting the Test

Clean Up

Out of Control Action List

Model 4004 and Computer Control

The Digital Encoder: Use and Calibration

Method B Encoder Option

How the encoder option enhances Method B tests.

Digital Encoder Installation

Programming for use with the Digital Encoder

Enable the Digital Encoder

Steps to enable the digital encoder in the setup menu.

Encoder Homing and Maintenance

Complete Digital Encoder Calibration

Pneumatic Lift Options

Pneumatic Lift

Accessory for Flow Ratio tests, automatically lifts weights.

Mini-Lift

Small pneumatic lift for piston rod support.

Instrument Calibration

RTD Sensor

Steps for calibrating RTD sensors using thermometers.

Digital Encoder Calibration

Instrument Maintenance and Troubleshooting

Maintenance

Routine maintenance tasks for the instrument.

Troubleshooting

Pneumatic Lift Troubleshooting

Questions and Answers

Typical Questions

USB Setup

PC and Daisy Instructions

Steps for configuring COM port assignment for Daisy software.

PC and MI Works Instructions

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