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Dynisco 4003 - User Manual

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Dynisco Polymer Test Systems
LMI 4000
Series
Melt
Indexer
Manual
Version 4.1
38 Forge Parkway
Franklin, MA 02038
Phone +1 508 541 9400
Fax +1 508 541 6206
Manual Part Number: M0704 www.dynisco.com
Original Language Version

Table of Contents

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Dynisco 4003 Specifications

General IconGeneral
BrandDynisco
Model4003
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction

Pneumatic Lift

Pneumatic lift accessory for Flow Ratio tests, safely lifting heavy weights.

Getting Started

Pneumatic lift setup

Detailed instructions for assembling and connecting the pneumatic lift system.

Safety

Use gloves, its HOT!

Warning about high temperatures and the need for protective gear like gloves.

Electrical Hazard

Caution regarding high voltage inside the instrument and proper grounding.

Calibration Thermometers use Mercury

Safe handling of mercury thermometers due to toxicity and breakage risks.

Pinch Points

Warning about crushing hazards from moving weights and lift systems.

Fumes from Materials

Advice on ventilation and handling hazardous fumes from polymers at high temperatures.

Pre-Run Check List

Checklist of essential points to address before operating the instrument for the first time.

Series 4000: A Guided Tour

Navigating the Keypad

Introduction to the keypad's role in programming, calibration, and controls.

Configuring the Instrument

Selecting CALIB (Calibration) in the SYS Mode

Outlines the calibration options available within the SYS mode.

The SETUP mode

Routine for setting user preferences, options, and instrument parameters like REJECTION, MFR/MVR, and COMM PORT.

Programming

Overview of programming parameters that define how an experiment is performed.

Method A Run Parameters

Lists required parameters for Method A tests, including METHOD, SET POINT, MELT TIME, CUT TIME, etc.

Method A;B Run Parameters

Lists required parameters for Method A/B tests, including FLG LENGTH and PROGRAM ID.

Method B Run Parameters

Lists required parameters for Method B tests, including MELT DENSITY and NO OF FLAGS.

RATIO (Flow Ratio) run parameters

Lists parameters for Flow Ratio tests, including FLG LENGTH HI and LOAD HI.

Method A Run

Programming a Method A

Steps to create or edit a Method A program, including setting parameters.

Loading the Sample

Instructions for loading material into the barrel, including tamping and handling bridging.

Weigh the Sample

Instructions for weighing the collected sample and entering the data for calculation.

Method A;B Run

Programming Method A;B

Steps to set up and program an A/B test, including method, set point, and melt time.

Machine Setup

Detailed steps for entering run parameters like METHOD, SET POINT, MELT TIME, CUT TIME, DENSITY, and FLAG LENGTH for Method A/B.

Inserting the Timing Flag

Instructions for inserting the plastic flag onto the plunger arm for timing the run.

Method B Run

Programming Method B

Steps to set up and program a Method B test using optical flags.

Timing Flag and Starting the Run

Instructions for inserting the timing flag and initiating the RUN command for Method B.

Making the Cut

Guides on making cuts on the extrudate and options for fast/slow extrusion based on flag timing.

Flow Ratio Runs

Flow Rate Ratio test and the Pneumatic Lift Option

Explains the Flow Ratio test, its purpose, and the benefit of the pneumatic lift option.

Intrinsic Viscosity Runs with PET

Calculating PET I.V. from the Melt Indexer

Explains how the Melt Indexer correlates Melt Flow Rate to Intrinsic Viscosity for PET.

A-Standard Operating Procedure

Out of Control Action List

The Digital Encoder: Use and Calibration

Method B Encoder Option

Details the digital encoder option for Method B tests, its components, and accuracy.

Encoder Advantages

Lists the benefits of using the digital encoder, such as automatic test length and multiple readings.

Digital Encoder Installation

Installation steps for the digital encoder, including parts list and initial setup.

Instrument Maintenance and Troubleshooting

Maintenance Schedules

Covers daily, weekly, and long-term maintenance tasks and schedules.

Pneumatic Lift Troubleshooting

Steps to diagnose and resolve issues with the pneumatic lift system's operation.

Questions and Answers

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