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FEI Quanta FEG 250 User Manual

FEI Quanta FEG 250
228 pages
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The Quanta FEG
250 / 450 / 650
User Operation Manual
5
th
Edition
20 August, 2010
Copyright © 2010
FEI Company
All rights reserved

Table of Contents

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FEI Quanta FEG 250 Specifications

General IconGeneral
Electron SourceField Emission Gun (FEG)
Stage5-axis motorized stage
Vacuum ModesHigh Vacuum, Low Vacuum, ESEM
Stage Movement X100 mm
Stage Movement Y100 mm
Stage Movement Z50 mm
Stage Movement R360° continuous
Accelerating Voltage200 V to 30 kV
Resolution (Low Vacuum)3.0 nm
MagnificationUp to 1, 000, 000x
DetectorsBackscattered Electron Detector
Sample SizeUp to 100 mm
Vacuum SystemTurbo-molecular pump, rotary vane pump
Operating Conditions Temperature15°C to 30°C
Operating Conditions HumidityUp to 80% non-condensing
TypeField Emission Gun Scanning Electron Microscope (FEG-SEM)

Summary

System Overview

How Quanta FEG SEM Works

Explanation of the four main components of the SEM system.

Vacuum System

Details on the three main vacuum sections and operating modes.

System Operation

Quanta FEG vacuum system

Description of the three vacuum sections: Gun, Column, and Specimen Chamber.

Vacuum Statuses

Controls and indicators for vacuum states and pump/vent operations.

Vacuum Modes

Explanation of High Vacuum (HiVac), Low Vacuum (LoVac), and ESEM modes.

Quanta FEG System States

Overview of system states: Shutdown, Standby, Overnight, and Full Operation.

POWER OFF

Procedures for safely powering off the instrument and emergency shutdown.

Software Control

xT microscope Server Software

Functionality of the server application for controlling microscope functions.

xT microscope Control Software

Overview of the main window elements and user interface.

The Stage Menu

Functions for stage navigation, alignment, and user units.

PREFERENCES… DIALOGUE

Accessing and configuring system settings via the Preferences dialogue.

Operating Procedures

Specimen Preparation and Handling

Guidelines for preparing and handling specimens for SEM observation.

Obtaining an Image

Pre-check procedures and conditions for obtaining an initial SEM image.

Optimising an Image

Techniques for improving image quality through adjustments.

Detector Types and Usage

Overview of available detectors and their configuration.

Alignments

Quanta FEG System Alignments

Overview of available alignment procedures and common rules.

Stages

Stages Types and Accessories

Description of stage types and available sample holders.

EUCENTRIC POSITION

Procedure for adjusting the stage to the eucentric position for optimal use.

Maintenance and Troubleshooting

Troubleshooting

Guide to common problems and their corrective actions.

DIAGNOSTICS AUTO REPORT

Procedure for generating a system report for troubleshooting.

System Options

Optional Detectors

Information on various optional detectors like GBSD, STEM I, and vCD.

Energy Dispersive X-ray (EDX) Analysis

Technique for identifying elemental composition using X-rays.

Cooling Stage / Waterless Cooling Stage

Controlling sample temperature with cooling stages.

Heating Stage 1000 °C / Heating Stage 1500 °C

Controlling sample temperature up to 1500 °C with heating stages.

Beam Deceleration

Method for improving microscope resolution at low accelerating voltages.

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