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UNITY-xr
Markes International UNITY-xr - User Manual
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QUI
-1117
Version 1.3 Janu
ary 2018
Markes Internationa
l Ltd
T:
+44 (0)144
3 230935
F:
+44 (0)144
3 231531
E:
enquiries@mark
es.com
www.markes.com
Installation manual
UNITY-
xr
2
Table of Contents
Main Page
Table of Contents
2
Preface
4
Notices
4
Warranty
4
Regulatory Compliance
4
Important Safety Warnings
5
Labels/Symbols
5
Mains Voltages
5
High Temperatures
6
Cleaning and Decontamination
6
Environment Operating Conditions
6
Temperature
6
Humidity
6
Altitude
6
Technical Specifications
7
Physical Properties
7
Electrical Properties
7
Technical Support Contact Details
7
UNITY-Air Server-Xr Pre-Installation Check List
8
Minimum Computer Specification for UNITY-Air Server-Xr Control
8
GC Equipment Requirements
8
Access into the GC Oven
8
GC Configuration/Parameter Selection
8
Laboratory Location
9
Space Requirements
9
Quality of the Laboratory Air
9
Quality of the Laboratory Gas Lines
9
Services
9
Power
9
Pressure Controlled Supply of Dry Air or Nitrogen (Purge Gas)
9
Pressure Controlled Carrier Gas Supply
10
Filters
10
Installing UNITY-Air Server-Xr
11
Unpacking UNITY-Air Server-Xr
11
Connections to UNITY-Air Server-Xr
11
Gas Connections
12
UNITY-Air Server-Xr with Electronic Carrier Control (ECC)
12
UNITY-Air Server-Xr Without Electronic Carrier Control (ECC) / T'D Option
13
Cable Connections
14
Installing the Transfer Line
14
Installing the Transfer Line Onto the GC
14
Installing the Fused Silica Transfer Line Insert
16
Connecting the Transfer Line to UNITY-Air Server-Xr
17
Installing the Cold Trap
20
Connecting the Air Server-Xr to the UNITY-Xr
23
Sample Line Connection
24
Configuring the Dryer (Optional)
24
Check for Gas Leaks
27
Installing Markes Instrument Control (MIC) Software
28
System Configuration
28
Running the Software
28
Configuring the Software
28
Detecting the UNITY-Air Server-Xr
31
Installation Qualification
32
Leak Testing
32
Conditioning the Cold Trap
32
System Checkout
34
Configuration of UNITY-Air Server-Xr Electronic Gas Control - Instrument Specific Guides
35
UNITY-Air Server-Xr Electronic Gas Control with the Agilent 6890GC
35
Procedure
35
6890 Inlet Settings
36
UNITY-Air Server-Xr Electronic Gas Control with the Agilent 7890GC
37
Procedure
37
7890 Inlet Setup
38
7890 Inlet Settings
38
UNITY-Air Server-Xr Electronic Gas Control with the Shimadzu QP 2010 (Plus) GCMS Fitted with AFC
39
Gas Connections between UNITY-Air Server-Xr and the Shimadzu AFC
39
Configuring the Shimadzu GC Software
40
Flow Stability
41
Ready / Start Connections between UNITY-Air Server-Xr and Shimadzu GC
42
UNITY-Air Server-Xr Electronic Gas Control with the Thermo DPFC
43
Procedure
43
Configuring the Thermo GC Software
43
UNITY-Air Server-Xr Electronic Gas Control with the Thermo 1300 Series GC
44
Installing the Markes TD to the Thermo Scientific TRACE Series 1300 GC
44
Testing the ECC Setup
47
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Markes International UNITY-xr Specifications
General
Sample Type
Air, gas
Technology
Thermal desorption
Temperature Range
-30 to 450°C
Cooling
Peltier
Heating Rate
Up to 100°C/min
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