Name: Parr Instrument 6400
Brand: Parr Instrument
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587M

6400

Automatic Isoperibol Calorimeter

Operating Instruction Manual

For models produced after October 2010

Figure3
- Table of Contents3
Figure5
Preface6
- Purpose6
- Related Instructions6
- Scope6
- Explanation of Symbols7
- Intended Usage7
- Safety Information7
- Cleaning & Maintenance8
- Environmental Conditions8
- General Specifications8
- Provisions for Lifting and Carrying8
Table8
Chapter10
- Environmental Conditions10
Installation10
- Swagelok Tube Fittings10
Table10
- Electrical Connection11
- Front Panel Meter11
- Required Consumables, Utilities and Power Requirements11
- 6400 Calorimeter Back Panel12
- Figure 1-212
- 6400 External Plumbing13
- Figure 1-313
- Water Connection13
- Bomb Exhaust Connections14
- Gas Connection14
- Balance Connections15
- Communication Connections15
- Printer Connections15
- 6400 Calorimeter Peripherals16
- Figure 1-516
- Figure16
- Figure 1-416
- Multiple Alternate Configurations16
Table17
Chapter18
- Initial Fill18
Quick Start18
Chapter20
- Control Keys20
- Menu Keys20
- Menu System20
Operation20
- Default Settings21
- Programming21
- Sample Preparation21
  - Figure 3-123
  - Bucket Fill Flow Diagram25
- Volatile Sample Technique23
- Cotton Thread Assembly24
  - Fill Cycle25
- Test Process24
  - Closing the Bomb24
Figure 3-6 Drain Flow Diagram29
Chapter30
- Calorimeter Operation Menu30
  - Temperature Vs. Time Plot31
  - Temperature Plot Setup Menu31
- Main Menu30
Menu Descriptions30
- Operating Controls Menu32
  - Spiking Controls32
  - Bomb Rinse Tank Controls33
- Program Information and Control Menu34
  - Software & Hardware Info34
  - User/Factory Settings35
- Calibration Data and Controls Menu36
  - Bomb 137
  - Control Plot Chart Plot37
- Thermochemical Corrections Menu38
  - Calculation Factors Menu39
  - Net Heat/Dry Heat Factors40
- Data Entry Controls Menu40
- Reporting Controls Menu42
- Communication Controls Menu43
  - Balance Port Communications43
  - Balance Port Settings44
- Diagnostics Menu45
- File Management Menu45
  - Run Data File Manager45
Chapter48
Reports48
Chapter50
- Automatic Statistical Calculations50
- Standard Materials50
Standardizations50
- Standardizing the Calorimeter50
- Calorimeter Control Limit Values in J/G When Benzoic Acid Is Used as a Test Sample51
- Calorimeter Control Limit Values in Cal/G When Benzoic Acid Is Used as a Test Sample52
- Calorimeter Control Limit Values in Btu/Lb When Benzoic Acid Is Used as a Test Sample53
- Table 6-353
Chapter54
Calculations54
- General Calculations54
- Thermochemical Corrections54
- ASTM and ISO Methods Differ55
- Acid and Sulfur Corrections56
- Thermochemical Calculation Details56
- ASTM Treatment for Acid and Sulfur58
- ISO Calculations58
- Conversion to Net Heat of Combustion59
- Conversion to Other Moisture Bases59
- Spiking Samples59
Calculating the Heat of Combustion54
Chapter60
Computer Communications60
- Computer Connections60
- Samba Server Feature (Optional)61
- 6400 Data File Naming Convention68
- Bar Code Port68
- 6400 Calorimeter Run Data Template69
- Table 8-269
Chapter70
- Clearing Memory70
Memory Management70
- Removable SD Memory70
5 Chapter72
- Bomb Removal72
- Inspection of Critical Sealing Surfaces72
Maintenance72
- 50 To 100 Test Maintenance73
- 500 Test Maintenance73
- Daily Maintenance73
- Fuses73
- Quarterly Maintenance73
- 5000 Test Maintenance74
- 6400 Maintenance Checklist75
Bomb Exhaust Troubleshooting76
- Troubleshooting76
Troubleshooting 7477
- Jacket Temperature Troubleshooting77
- Error List78
Chapter80
- Return for Repair80
Technical Service80
Chapter82
- A1250DD2 Controller Assembly82
- A1265DD Bucket and Stirrer Tube Assembly82
Parts Lists82
- Principal Assemblies in Calorimeter82
- A1255DD Bucket Stirrer Assembly83
- A1266DD Cover Assembly83
- A1457DD Accessory/Installation Kit83
Chapter84
- Figure 14-1 1138 Parts Diagram84
- 1138 Parts Diagram Key85
Drawings84
- Figure 14-2 6400 Cutaway Right86
  - Figure87
    - Figure88
    - A1250DD2 Control Schematic89
  - 6400 Cover Open88
- 6400 Cutaway Left87
- A1251DD Oxygen Solenoid Assembly90
- A1447DD Water Solenoid Assembly90
Tables106
- Factory Default Settings106
Table106
Table107
- Settings for ISO & BSI Methods108

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Parr Instrument 6400 Specifications

General

Brand	Parr Instrument
Model	6400
Category	Measuring Instruments
Language	English

Parr Instrument 6400 User Manual

Table of Contents

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Parr Instrument 6400 Specifications