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Parr Instrument 6400 User Manual

Parr Instrument 6400
110 pages
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587M
6400
Automatic Isoperibol Calorimeter
Operating Instruction Manual
For models produced after October 2010

Table of Contents

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Parr Instrument 6400 Specifications

General IconGeneral
BrandParr Instrument
Model6400
CategoryMeasuring Instruments
LanguageEnglish

Summary

Preface

Scope

Outlines the manual's purpose for installing and operating the Parr 6400 Calorimeter.

Purpose

Explains how combustion heat is measured using the calorimeter and the substitution procedure.

Customer Service

Provides contact information for the Parr Customer Service Department for assistance.

Explanation of Symbols

Safety Information

Intended Usage

Specifies the intended use of the instrument and potential consequences of misuse.

General Specifications

Environmental Conditions

Details the operating and storage environmental conditions, including temperature, humidity, and altitude.

Cleaning & Maintenance

Outlines procedures for routine cleaning and notes user-serviceable parts.

CHAPTER 1 Installation

Environmental Conditions

Describes the laboratory requirements for installing and operating the calorimeter.

Swagelok Tube Fittings

Explains the procedure for installing and tightening Swagelok tube fittings for secure connections.

Required Consumables, Utilities and Power Requirements

Electrical Connection

Details how to properly connect the calorimeter to a grounded electrical outlet for safety and performance.

Water Connection

Gas Connection

Bomb Exhaust Connections

Explains how to connect the bomb exhaust to a collection system or optional container.

Communication Connections

Printer Connections

Explains printer settings and default configuration for the Parr 1758 Printer.

Balance Connections

Details how to connect various types of balances and configure communication parameters.

CHAPTER 2 Quick Start

Initial Fill

Step-by-step instructions for filling the calorimeter with water and checking systems.

Quick Start

Provides a concise procedure for performing the first test or pretest.

CHAPTER 3 Operation

Menu System

Explains the menu-driven interface and organization of settings and controls.

Menu Keys

Describes different types of keys used for data entry and navigation within the menus.

Control Keys

Details the function of the five primary control keys (Escape, Main Menu, Start, Abort, Report, Help).

Programming

Default Settings

Describes the pre-programmed default settings and how to reload them.

Sample Preparation

Covers sample size, sulfur/chlorine content, and particle size considerations for accurate testing.

Combustion Capsules

Test Process

Closing the bomb

Instructions on how to correctly close the bomb head into the calorimeter cylinder.

Fill Cycle

Pre-Period

Bomb Firing

Post-Period

Details the post-period phase where the temperature rise is monitored and recorded.

Cool/Rinse

Drain

CHAPTER 4 Menu Descriptions

Main Menu

Shows the primary screen layout and explains the function of main menu keys.

Calorimeter Operation Menu

Describes the main menu for operating the calorimeter, including mode, temperature plots, and test initiation.

Temperature vs. Time Plot

Temperature Plot Setup Menu

Details the various settings available for configuring the temperature plot display.

Operating Controls Menu

Spiking Controls

Explains how to use spiking materials to aid combustion and compensate for their heat.

Bomb Rinse Tank Controls

Program Information and Control Menu

Software and Hardware Info

Displays system information like software version, CPU, and IP address.

User/Factory Settings

Calibration Data and Controls Menu

Control Chart Parameters

Explains the use of control charts for process monitoring and setting limits.

Bomb 1

Manual EE Entry

Describes how to manually enter the Energy Equivalent (EE) value for a bomb.

Print Standardization Runs

Option to print all tests used for EE value calculation.

Thermochemical Corrections Menu

Calculation Factors

Nitric Acid Factor

Sets the factor for nitric acid correction calculations.

Sulfur Value is Percent

Toggles sulfur value entry between weight percent and other units.

Net Heat/Dry Factors

Data Entry Controls Menu

Net Heat Data Entry Controls

Specifies how hydrogen, oxygen, and nitrogen content are entered for net heat calculations.

Auto Sample ID Controls

Moisture Data Entry Controls

Preweigh Sample ID Controls

Reporting Controls Menu

Communication Controls Menu

Printer Type

Selects the type of printer connected to the calorimeter.

Balance Port

Accesses settings for balance port communication.

File Management Menu

Diagnostics Menu

Pretesting Cycle

Initiates a pretest cycle to condition the calorimeter before testing.

Data Logger Controls

Data Log Items

User Defined Buttons

I/O Diagnostics

CHAPTER 5 Reports

Preliminary Reports

Explains preliminary reports generated at test conclusion for quick confirmation.

Final reports

Describes final reports generated after all thermochemical corrections are entered.

CHAPTER 6 Standardizations

Standardizing the Calorimeter

Explains the purpose and procedure for standardizing the calorimeter.

Standard Materials

Lists the standard materials, like benzoic acid pellets, used for standardization.

Automatic Statistical Calculations

CHAPTER 7 Calculations

Calculating the Heat of Combustion

Details the formula and process for calculating the gross heat of combustion.

General Calculations

Presents the main formula for heat of combustion and defines its variables.

Temperature Rise

Explains how the calorimeter corrects temperature rise readings.

Energy Equivalent

Thermochemical Corrections

Nitric Acid Correction

Explains the correction for heat generated by nitric acid formation during combustion.

Sulfur Correction

Details the correction for heat from sulfuric acid formation due to sulfur in the sample.

Fuse Correction

Describes the correction for heat liberated by the fuse wire used to ignite the sample.

Thermochemical Calculation Details

Acid and Sulfur Corrections

Explains how acid and sulfur corrections are calculated, including related factors.

ASTM and ISO Methods Differ

ASTM Treatment for Acid and Sulfur

ISO Calculations

Spiking Samples

Conversion to Other Moisture Bases

Conversion to Net Heat of Combustion

CHAPTER 8 Computer Communications

Computer Connections

Explains how to connect the calorimeter to a computer using Ethernet and FTP.

Samba Server Feature (Optional)

Web Server Service

Configuration Page

Run Data Page

System Info Page

LCD Snap Shot Page

Documentation Page

Bar Code Port

CHAPTER 9 Memory Management

Clearing Memory

Details procedures for deleting single files or series of files from memory.

Removable SD Memory

Explains the use of SD memory cards for data transfer, backup, and system updates.

CHAPTER 10 Maintenance

Inspection of Critical Sealing Surfaces

Describes how to inspect and maintain sealing surfaces for leaks and wear.

Bomb Removal

Provides steps for removing the bomb cylinder from the bucket assembly for servicing.

Fuses

Daily Maintenance

Quarterly Maintenance

50 to 100 Test Maintenance

500 Test Maintenance

5000 Test Maintenance

6400 Maintenance Checklist

CHAPTER 11 Troubleshooting

Bomb Exhaust Troubleshooting

Covers troubleshooting issues related to the bomb exhaust system and piston movement.

Jacket Temperature Troubleshooting

Error List

Start and Pretest buttons dim.

Explains why the start/pretest buttons may be dim and how to resolve it.

A Misfire Condition Has Been Detected.

Lists causes for a misfire error, such as fuse issues or poor stirring.

A Preperiod Timeout Has Occurred.

Details potential causes for a pre-period timeout, like bomb leaks or lid issues.

A Postperiod Timeout has Occurred

There Is A Problem With The Bucket Thermistor.

There Is A Problem With The Jacket Thermistor.

A/D Initialization Failed.

Bomb ID – Has Been Fired – Times Which Exceeds the Bomb Service Interval.

You Have Exceeded the Run Data File Limit (1000 Files).

Bomb EE Standard Deviation Warning.

Sample Weight Warning.

The Lid has Failed to Lock or is not Closed Properly.

The heater loop break limit has been detected.

Could Not Cool the Bomb Successfully.

Rinse Tank Level May Be Low.

CHAPTER 12 Technical Service

Return for Repair

Outlines the procedure and requirements for returning the calorimeter for repair services.

CHAPTER 13 Parts Lists

Principal Assemblies in Calorimeter

Lists the main assemblies of the 6400 Calorimeter.

A1250DD2 Controller Assembly

Details the components of the A1250DD2 Controller Assembly.

A1265DD Bucket and Stirrer Tube Assembly

Lists parts for the A1265DD Bucket and Stirrer Tube Assembly.

A1255DD Bucket Stirrer Assembly

A1266DD Cover Assembly

A1457DD Accessory/Installation Kit

CHAPTER 14 Drawings

Figure 14-1 1138 Parts Diagram

Shows a parts diagram for the 1138 Oxygen Combustion Vessel.

1138 Parts Diagram Key

Figure 14-2 6400 Cutaway Right

Figure 14-3 6400 Cutaway Left

Figure 14-4 6400 Cover Open

Figure 14-5 A1250DD2 Control Schematic

Figure 14-6 A1251DD Oxygen Solenoid Assembly

Figure 14-7 A1447DD Water Solenoid Assembly

Figure 14-8 A1456DD Rinse Valve Assembly

Figure 14-9 6400 Internal Plumbing Diagram

Figure 14-10 6400 Water Tank and Jacket Cooling Solenoid

Figure 14-11 A1455DD Propeller Assembly

Figure 14-12 A1448DD Temperature Control Assembly

Figure 14-13 A1268DD Stirrer Motor and Mount

Figure 14-14 6400 Bucket Assembly

Figure 14-15 6400 Air Can Assembly, Cutaway Left

Figure 14-16 6400 Air Can Assembly, Cutaway Front

Figure 14-17 A1450DD Bomb Head Assembly, View 1

Figure 14-18 A1450DD Bomb Head Assembly, View 2

Figure 14-19 A1050DD Rinse Collection Assembly

Figure 14-20 Wiring Diagram

Figure 14-21 Wiring Diagram

Figure 14-22 Fuse Diagram

CHAPTER 15 Tables

Table 15-1 Factory Default Settings

Lists the factory default settings for calorimeter operations, controls, and settings.

Table 15-2 Settings for ISO & BSI Methods