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6400
Parr Instrument 6400 User Manual
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1
Installation
Parr Instrument Company
14
Figure 1-4
6400 Calorimeter P
eripherals
Figure 1-5
Multiple Alternate Configurations
15
17
Table of Contents
Figure
3
Table of Contents
3
Figure
5
Preface
6
Purpose
6
Related Instructions
6
Scope
6
Explanation of Symbols
7
Intended Usage
7
Safety Information
7
Cleaning & Maintenance
8
Environmental Conditions
8
General Specifications
8
Provisions for Lifting and Carrying
8
Table
8
Chapter
10
Environmental Conditions
10
Installation
10
Swagelok Tube Fittings
10
Table
10
Electrical Connection
11
Front Panel Meter
11
Required Consumables, Utilities and Power Requirements
11
6400 Calorimeter Back Panel
12
Figure 1-2
12
6400 External Plumbing
13
Figure 1-3
13
Water Connection
13
Bomb Exhaust Connections
14
Gas Connection
14
Balance Connections
15
Communication Connections
15
Printer Connections
15
6400 Calorimeter Peripherals
16
Figure 1-5
16
Figure
16
Figure 1-4
16
Multiple Alternate Configurations
16
Table
17
Chapter
18
Initial Fill
18
Quick Start
18
Chapter
20
Control Keys
20
Menu Keys
20
Menu System
20
Operation
20
Default Settings
21
Programming
21
Sample Preparation
21
Figure 3-1
23
Bucket Fill Flow Diagram
25
Figure 3-3
25
Figure 3-4
26
Pre-Period
26
Pre-Period/Post-Period Flow Diagram
26
Bomb Firing
27
Post-Period
27
Cool/Rinse
28
Figure 3-5
28
Rinse & Cool Flow Diagram
28
Volatile Sample Technique
23
Cotton Thread Assembly
24
Fill Cycle
25
Test Process
24
Closing the Bomb
24
Figure 3-6 Drain Flow Diagram
29
Chapter
30
Calorimeter Operation Menu
30
Temperature Vs. Time Plot
31
Temperature Plot Setup Menu
31
Main Menu
30
Menu Descriptions
30
Operating Controls Menu
32
Spiking Controls
32
Bomb Rinse Tank Controls
33
Program Information and Control Menu
34
Software & Hardware Info
34
User/Factory Settings
35
Calibration Data and Controls Menu
36
Bomb 1
37
Control Plot Chart Plot
37
Thermochemical Corrections Menu
38
Calculation Factors Menu
39
Net Heat/Dry Heat Factors
40
Data Entry Controls Menu
40
Net Heat Data Entry Controls
41
Auto Sample ID Controls
41
Moisture Data Entry Controls
42
Preweigh Sample ID Controls
42
Reporting Controls Menu
42
Communication Controls Menu
43
Balance Port Communications
43
Balance Port Settings
44
Diagnostics Menu
45
Data Logger Controls
46
Data Log Items
47
User Defined Buttons
47
I/O Diagnostics
47
File Management Menu
45
Run Data File Manager
45
Chapter
48
Reports
48
Chapter
50
Automatic Statistical Calculations
50
Standard Materials
50
Standardizations
50
Standardizing the Calorimeter
50
Calorimeter Control Limit Values in J/G When Benzoic Acid Is Used as a Test Sample
51
Calorimeter Control Limit Values in Cal/G When Benzoic Acid Is Used as a Test Sample
52
Calorimeter Control Limit Values in Btu/Lb When Benzoic Acid Is Used as a Test Sample
53
Table 6-3
53
Chapter
54
Calculations
54
General Calculations
54
Thermochemical Corrections
54
ASTM and ISO Methods Differ
55
Acid and Sulfur Corrections
56
Thermochemical Calculation Details
56
ASTM Treatment for Acid and Sulfur
58
ISO Calculations
58
Conversion to Net Heat of Combustion
59
Conversion to Other Moisture Bases
59
Spiking Samples
59
Calculating the Heat of Combustion
54
Chapter
60
Computer Communications
60
Computer Connections
60
Samba Server Feature (Optional)
61
6400 Data File Naming Convention
68
Bar Code Port
68
6400 Calorimeter Run Data Template
69
Table 8-2
69
Chapter
70
Clearing Memory
70
Memory Management
70
Removable SD Memory
70
5 Chapter
72
Bomb Removal
72
Inspection of Critical Sealing Surfaces
72
Maintenance
72
50 To 100 Test Maintenance
73
500 Test Maintenance
73
Daily Maintenance
73
Fuses
73
Quarterly Maintenance
73
5000 Test Maintenance
74
6400 Maintenance Checklist
75
Bomb Exhaust Troubleshooting
76
Troubleshooting
76
Troubleshooting 74
77
Jacket Temperature Troubleshooting
77
Error List
78
Chapter
80
Return for Repair
80
Technical Service
80
Chapter
82
A1250DD2 Controller Assembly
82
A1265DD Bucket and Stirrer Tube Assembly
82
Parts Lists
82
Principal Assemblies in Calorimeter
82
A1255DD Bucket Stirrer Assembly
83
A1266DD Cover Assembly
83
A1457DD Accessory/Installation Kit
83
Chapter
84
Figure 14-1 1138 Parts Diagram
84
1138 Parts Diagram Key
85
Drawings
84
Figure 14-2 6400 Cutaway Right
86
Figure
87
Figure
88
A1250DD2 Control Schematic
89
6400 Cover Open
88
6400 Cutaway Left
87
Figure
89
A1448DD Temperature Control Assembly
94
A1455DD Propeller Assembly
94
Figure 14-11
94
A1268DD Stirrer Motor and Mount
95
Figure 14-13
95
6400 Bucket Assembly
96
Figure 14-14
96
6400 Air Can Assembly, Cutaway Left
97
Figure 14-15
97
6400 Air Can Assembly, Cutaway Front
98
Figure 14-16
98
A1450DD Bomb Head Assembly, View 1
99
Figure 14-17
99
A1450DD Bomb Head Assembly, View 2
100
Figure 14-18
100
A1050DD Rinse Collection Assembly
101
Figure 14-19
101
Figure 14-20
102
Wiring Diagram
102
Figure 14-21
103
Wiring Diagram
103
Figure 14-22
104
Fuse Diagram
104
Figure 14-12
94
A1251DD Oxygen Solenoid Assembly
90
A1447DD Water Solenoid Assembly
90
Figure
90
Figure
91
6400 Internal Plumbing Diagram
92
Figure
92
6400 Water Tank and Jacket Cooling Solenoid
93
Figure 14-7
90
A1456DD Rinse Valve Assembly
91
Tables
106
Factory Default Settings
106
Table
106
Table
107
Settings for ISO & BSI Methods
108
5
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Parr Instrument 6400 Specifications
General
Brand
Parr Instrument
Model
6400
Category
Measuring Instruments
Language
English
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