SCIEX 3200 Series User Manual

Name: SCIEX 3200 Series
Brand: SCIEX
Rating: 4 (1 reviews)

114 pages

To Next Page

SCIEX 3200 Systems

System User Guide

RUO-IDV-05-6475-C February 2022

Table of Contents3
Operational Precautions and Limitations7
General Safety Information7
Documentation Symbols and Conventions7
Regulatory Compliance8
Australia and New Zealand8
Canada8
Europe8
United States9
International9
Electrical Precautions10
Mains Supply10
Protective Earth Conductor10
Chemical Precautions11
System Safe Fluids12
Ventilation Precautions13
Physical Precautions14
Environmental Precautions14
Electromagnetic Environment14
Decommissioning and Disposal16
Qualified Personnel16
Laboratory Conditions17
Safe Environmental Conditions17
Performance Specifications17
Equipment Use and Modification17
Principles of Operation19
System Overview19
Hardware Overview20
Ion Source Overview26
Theory of Operation32
Ion Source Installation34
Prepare for Installation34
Install the Probe35
Connect the Ion Source Tubing36
Install the Ion Source on the Mass Spectrometer36
Inspect for Leaks38
Ion Source Optimization39
Sample Introduction39
Method39
Flow Rate40
Turboionspray Probe Optimization40
Flow Rate and Ion Source Temperature41
Set up the System41
Prepare the System41
Set the Starting Conditions42
Optimize the Turboionspray Probe Position42
Optimize Source and Gas Parameters and Voltage44
Optimize the Turbo Heater Temperature44
APCI Probe Optimization45
Optimization Tips45
Operating Instructions47
Start up the System47
Syringe Pump48
Adjust the Integrated Syringe Pump Position48
Diverter Valve48
Plumb the Diverter Valve in Injector Mode49
Plumb the Diverter Valve in Diverter Mode50
Shut down and Vent the System52
Operating Instructions - User Workflows53
Service and Maintenance Information - Mass Spectrometer55
Recommended Maintenance Schedule55
Clean the Surfaces57
Clean the Front-End58
Symptoms of Contamination58
Required Materials58
Cleaning Best Practices59
Prepare the Mass Spectrometer61
Clean the Curtain Plate62
Clean the Front of the Orifice Plate63
Put the Mass Spectrometer Back in Service63
Empty the Source Exhaust Drain Bottle63
Inspect the Roughing Pump Oil Level66
Storage and Handling67
Service and Maintenance - Ion Source68
Ion Source Handling69
Remove the Ion Source70
Clean the Ion Source Surfaces71
Clean the Probe71
Remove the Probe72
Replace the Electrode72
Replace the Corona Discharge Needle74
Replace the Sample Tubing76
Storage and Handling76
Mass Spectrometer Troubleshooting77
A Calibration Ions and Solutions82
B Principles of Operation - Ion Source84
Electrospray Ionization Mode84
APCI Mode85
APCI Ionization Region88
C Ion Source Optimization90
Turboionspray Probe Optimization90
Set up the System91
Prepare the System91
APCI Probe Optimization91
Set up the System92
Prepare the System92
Set the Starting Conditions93
Optimize Source and Gas Parameters93
Adjust the Position of the Corona Discharge Needle94
Optimize the APCI Probe Position94
Optimize the Nebulizer Current96
Optimize the APCI Probe Temperature96
D Source Parameters and Voltages98
Turboionspray Probe Parameters98
APCI Probe Parameters99
Parameter Descriptions100
Probe Position102
Solvent Composition102
E Glossary of Symbols104
F Glossary of Warnings110
Contact Us113
Customer Training113
Online Learning Center113
SCIEX Support113
Cybersecurity113
Documentation113

Questions and Answers:

Need help?

Do you have a question about the SCIEX 3200 Series and is the answer not in the manual?

SCIEX 3200 Series Specifications

General

Brand	SCIEX
Model	3200 Series
Category	Laboratory Equipment
Language	English

Related product manuals

SCIEX TripleTOF 5600 Plus

131 pages

SCIEX CESI 8000 Plus

376 pages

SCIEX Triple Quad 6500 Series

195 pages

SCIEX NanoSpray

92 pages

SCIEX 3200 Series User Manual

Table of Contents

Questions and Answers:

SCIEX 3200 Series Specifications

Related product manuals