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General| Type | Triple Quadrupole Mass Spectrometer |
|---|---|
| Dynamic Range | > 5 orders of magnitude |
| Mass Analyzer | Triple Quadrupole |
| Polarity | Positive and Negative |
| Scan Modes | Multiple Reaction Monitoring (MRM), Precursor Ion Scan, Product Ion Scan, Neutral Loss Scan |
| Ion Source | Turbo V Ion Source |
| Power Requirements | 200 – 240 VAC |
| Resolution | Unit resolution (0.7 Da FWHM) |
Provides essential safety guidelines and warnings for operating the system.
Explains symbols and conventions used throughout the user guide.
Details compliance with various regional and international standards and regulations.
Outlines critical safety measures related to electrical hazards and system power.
Details safety measures for handling chemicals and hazardous materials.
Lists fluids approved for use with the system and guidelines for their use.
Specifies requirements for proper ventilation and exhaust systems for safe operation.
Covers safety measures related to the physical handling and movement of the equipment.
Addresses safe handling, disposal, and environmental conditions for the system.
Discusses electromagnetic compatibility and interference considerations for system operation.
Provides instructions for safely retiring and disposing of the system components.
Defines the qualifications required for personnel operating and maintaining the system.
Specifies the environmental conditions required for safe and optimal system operation.
Details the safe operating environmental conditions for the system.
Lists the performance parameters and conditions under which the system meets specifications.
Outlines guidelines for proper equipment usage and restrictions on modifications.
Provides a general overview of the components within the 3200 series instruments.
Details the front and back views of the instrument hardware with component identification.
Explains the different types of ion sources and their ionization modes (ESI, APCI).
Identifies and describes the components of the ion source assembly.
Compares specifications and describes the TurboIonSpray and APCI probes.
Explains the fundamental principles of mass spectrometry and the 3200 system's ion optics.
Outlines preparatory steps and required materials for installing the ion source.
Provides step-by-step instructions for installing the ion source probe.
Details the procedure for connecting the sample tubing to the ion source.
Guides the user through the process of mounting the ion source onto the mass spectrometer.
Describes how to check for leaks after installation to ensure system integrity.
Discusses methods and flow rates for introducing samples into the ion source.
Specifies the flow rate ranges supported by the TurboIonSpray and APCI probes.
Provides detailed steps for optimizing the TurboIonSpray probe for best performance.
Explains how flow rate and solvent composition affect optimal probe temperature.
Steps to configure the LC pump and autosampler for system setup.
Steps to prepare the system using control software for optimization.
Defines initial parameter settings for ion source optimization.
Guides on adjusting probe position for optimal signal-to-noise ratio.
Adjusting gas flows and voltages for optimal signal stability and sensitivity.
Details how to adjust the turbo heater temperature for optimal performance.
Steps to optimize the APCI probe for optimal signal and stability.
Offers general advice for optimizing ion source performance and minimizing maintenance.
Outlines the prerequisites and steps for safely powering on and starting the system.
Explains how to adjust and use the integrated syringe pump for sample infusion.
Describes how to configure and use the integrated diverter valve.
Details the tubing connections for the diverter valve in injector mode.
Details the tubing connections for the diverter valve in diverter mode.
Provides instructions for safely shutting down and venting the system.
Provides a schedule and guidelines for routine cleaning and maintenance tasks.
Details methods for cleaning the external surfaces of the mass spectrometer.
Explains how to perform routine cleaning of the mass spectrometer's front-end components.
Lists signs indicating system contamination and the need for cleaning.
Lists the necessary tools and supplies for cleaning and maintenance procedures.
Offers recommended practices for effective and safe cleaning of the instrument.
Outlines steps to prepare the mass spectrometer before performing cleaning procedures.
Provides instructions for cleaning the curtain plate component of the ion source.
Details the procedure for cleaning the front of the orifice plate.
Guides the user on reassembling and returning the mass spectrometer to operation.
Explains how to safely empty the source exhaust drain bottle.
Details how to check the oil level in the roughing pump.
Provides guidelines for storing and handling the mass spectrometer system.
Describes how to safely handle the ion source, noting hot surfaces.
Step-by-step guide for safely removing the ion source from the mass spectrometer.
Instructions for cleaning the exterior surfaces of the ion source.
Details the procedure for flushing and cleaning the ion source probes.
Step-by-step guide for safely removing the probe from the ion source.
Instructions for replacing the electrode within the ion source probe.
Guide for replacing the corona discharge needle in the ion source.
Instructions for replacing the sample tubing of the ion source.
Provides guidelines for storing and handling the ion source component.
Lists calibration ions, solutions, and tuning frequencies for the system.
Explains the principles of Electrospray Ionization (ESI) and APCI modes.
Describes how Electrospray Ionization (ESI) works to generate ions.
Explains the process and suitability of Atmospheric Pressure Chemical Ionization (APCI).
Details the location and process within the APCI ionization region.
Provides detailed steps for optimizing ion source parameters for performance.
Steps to optimize the TurboIonSpray probe for best signal-to-noise.
Steps to optimize the APCI probe for best signal-to-noise.
Guide for adjusting the corona discharge needle position for optimal ionization.
Steps to optimize the APCI probe position for sensitivity and stability.
How to adjust nebulizer current for optimal signal in APCI.
Guide for setting the optimal temperature for the APCI probe.
Details recommended operating parameters and voltages for ion sources.
Recommended operating conditions for the TurboIonSpray probe at different flow rates.
Recommended operating parameters for the APCI probe.
Explains source-dependent parameters like gases, temperature, and voltage.
Discusses how probe position affects analysis sensitivity.
Lists commonly used solvents and modifiers for the ion source.
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