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Thermo Scientific Orion 2230XP User Manual

Thermo Scientific Orion 2230XP
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Thermo Scientific Orion
2230XP Silica Analyzer
271539-001 Revision A March 2016
User Manual

Table of Contents

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Thermo Scientific Orion 2230XP Specifications

General IconGeneral
BrandThermo Scientific
ModelOrion 2230XP
CategoryMeasuring Instruments
LanguageEnglish

Summary

General Information

Safety Precautions

Guidelines and warnings for safe operation and handling of the analyzer.

Symbols Used in this Manual

Specifications

Electrical

Details on power requirements, connection types, safety class, and fuses.

Environmental

Specifies operating and storage temperature ranges, humidity, and altitude limits.

Sample Requirements

Defines parameters for sample inlet pressure, flow rate, temperature, and fittings.

Introduction

Unpacking the Instrument

Instructions for removing the analyzer from its packaging and inspecting for damage.

Startup Procedure

Step-by-step guide for initial setup and powering on the analyzer.

General Product Description

Overview of the analyzer's capabilities, design, and intended use.

User Interface

Description of the analyzer's control panel, keypad, and display.

Display Fields

Explanation of the information shown on the analyzer's display fields.

Menus Display

Details on navigating menus, including item indicators and key functions.

Measurement Mode Display

How the analyzer displays current readings, units, date, and time in measurement mode.

Analysis Reaction Principle

Explanation of the colorimetric method used for silica analysis.

Fluids Storage

Recommendations for storing reagents and standards safely.

Calibration Standard

Information about the specific calibration standard used for this analyzer.

Reagents Required

Details on the reagents needed for operation and their installation.

Reagent Consumption

Estimates for reagent usage and lifespan based on analysis frequency.

Installation Environmental Considerations

Mounting the Instrument

Guidelines for physically installing the analyzer, including weight and clearance.

Plumbing Connections

Instructions for connecting sample inlet, return, and drain lines.

Installing Peristaltic Pump Head Tubing

Procedure for replacing or installing the pump head tubing.

Installing the Reagents

Steps for correctly inserting reagent bottles into the analyzer.

Connecting Power to the Analyzer

Safety precautions and procedures for connecting the analyzer to electrical power.

Analog Outputs Connections

Details on configuring and connecting the analog output signals.

Alarm Connections

Information on connecting alarm inputs and understanding relay outputs.

Inputs Signal Connections

Wiring details for external control inputs and sensor connections.

Communication Signal Connections

Instructions for establishing communication links with the analyzer.

Startup and Operation

Executing a manual calibration

Procedure for performing a manual calibration cycle and accepting results.

In Auto- Calibration mode

How the analyzer handles calibration results outside specified tolerances.

Placing the Analyzer into Service

Steps to activate the analyzer for routine, unattended operation.

Validating a Calibration Standard

How to check calibration accuracy using a validation function.

Running an Analysis (Analyze Once)

Procedure to perform a single or multiple sample analyses on demand.

Instrument Operation Modes

Description of the different operational modes like sample analysis and calibration.

Sample Analysis and Validation

Comparison of sample analysis and validation cycles and their data handling.

Calibration

Methods for executing manual or automatic calibration cycles.

Cleaning

Procedures for performing automatic or manual cleaning of the reaction cell.

Post Wash

Configuration of post-measurement wash cycles to clean the reaction cell.

Priming

Steps for priming instrument lines to fill tubing and purge air.

Analyzer Hardware Configuration and Calibration

Optics Calibration

Overview of the analyzer's optical components and calibration process.

Optics Calibration Steps

Detailed steps for performing optics calibration, including prerequisites.

Reaction Cell Temperature Calibration

Procedure for calibrating the reaction cell's temperature control system.

Heater Temperature Calibration

Instructions for tuning and calibrating the thermistor and heater assembly.

Pumps Calibration

Explanation of peristaltic pump function and the need for calibration.

Pumps Calibration Method

Step-by-step guide for calibrating the individual pumps for accurate dosing.

Analog Outputs Calibration

Procedure for calibrating the analog output channels for signal accuracy.

Calibration of the Instrument for Measurement Analysis

Theory of Calibration

Fundamental principles behind calibration using standards and calibration curves.

Methods of Calibration

Description of available calibration methods: Single Point and Base Line.

Single Point Calibration

Details on performing single point calibration and its formula.

Base Line Calibration

Explanation of base line calibration for improved low-level measurement accuracy.

High Range Dilution-Factor Calibration

Procedure for calibrating the dilution factor for high concentration samples.

Theory of Measurement

Principles of measuring sample concentration based on absorbance.

Mode of Measurement

Explanation of the AUTO restart and MANUAL restart modes of operation.

Auto Restart Mode

How the analyzer automatically restarts measurements after idle periods.

Manual Restart Mode

Procedure for initiating measurements manually and standby operation.

Measurement Cycle

Sequence of events performed during a single analysis cycle.

Cell Wash

Details on the cell wash step, including volume adjustment.

Sample Capture

Description of the sample capture step and settling time.

Optics Testing

Procedure for checking the optical path and LED source status.

Checking Reaction Temperature

Testing the reaction cell temperature against the set point.

Blank Measurement

Recording the blank absorbance reading before reagent addition.

Add Reagents

Procedure for adding reagents and editing reagent volumes.

Collect Data

Final reading and absorbance measurement for concentration calculation.

Post Wash

Configuring post-measurement wash cycles to clean the reaction cell.

Priming

Steps for priming instrument lines to fill tubing and purge air.

Measurement Data

How measurement and calibration results are stored and retrieved.

Printing Results

Instructions for printing stored measurement results via RS-232 port.

Menu Overview

Setup

Configuring instrument functionality, operational parameters, and display settings.

Measurement

Performing manual analysis, calibration, validation, and cleaning cycles.

View Data and Alarms

Reviewing collected data, alarms, and faults from recent cycles.

Services

System administration, hardware setup, fluidics priming, and diagnostics.

Alarms Menu

Configuration of alarm parameters and assignment of alarms to faults.

Relays Mapping Menu

Mapping multiple alarms to individual output relays.

Analog Outputs Menu

Configuration and settings for the instrument's analog output signals.

Inputs Menu

Configuration of internal and external inputs for sensors and control.

Display Parameters Menu

Adjusting display settings like contrast, backlight, and font size.

Calibration Parameters Menu

Setting calibration parameters, including reference and current values.

Validation Parameters Menu

Configuration of validation parameters, sources, and repetition counts.

Analysis Parameters Menu

Setting instrument mode, frequency, units, and wash cycle parameters.

Cleaner Parameters Menu

Configuration of parameters for manual or periodic cleaning cycles.

Temperature Units Menu

Selection of temperature display units (Fahrenheit or Celsius).

Method Parameters Menu

Configuring method parameters and the order of analysis events.

Date and Time Menu

Setting and editing the instrument's current date and time.

Daylight Saving

Configuration for daylight saving time adjustments.

Recovery After Power Failure Menu

Settings for instrument behavior after a power interruption.

Ethernet Parameters Menu

Configuration settings for network connectivity via Ethernet.

RS-232 Parameters Menu

Setting the baud rate for serial communication.

Language Menu

Selection of the instrument's operating language.

Analyze Once

Initiates a single manual analysis cycle.

Calibrate

Initiates a manual calibration cycle using standard solutions.

Validate

Performs manual validation of the instrument with a known sample or standard.

Clean

Initiates manual cleaning of the reaction cell.

Review / Reset Alarms

Review and reset instrument faults and alarms.

Review Calibration Results

Review and print stored calibration results from the database.

Review Analysis Results

Review and print stored analysis results from the database.

Delete All Calibration Results

Deletes the entire calibration results database.

Delete All Analysis Results

Deletes the entire analysis results database.

Service Menu

System Administration Menu

Manage user access, passwords, and permissions for the instrument.

Hardware Setup Menu

Access to hardware calibration and configuration settings.

Prime Fluidics Menu

Procedure for priming the analyzer's fluidic lines.

Diagnostics Menu

Tools for testing individual components like pumps, valves, and optics.

Edit User Menu

Allows editing of user names, passwords, and permissions.

Delete User Menu

Allows deletion of user accounts from the system.

Add User Menu

Allows adding new user accounts with specific permissions.

Factory Settings Menu

Restore factory defaults or update instrument settings.

Instrument Details Menu

View instrument details like software version, serial, and model numbers.

Analysis Label Change Menu

Allows modification of the analysis label displayed on the instrument.

Printing Options Menu

Configure settings for printing system and parameter reports.

Calibrate Thermistor

Calibrating the thermistor for accurate reaction cell temperature measurement.

Calibrate Pumps

Calibrating the flow rate of the peristaltic pumps.

Calibrate Optics

Calibrating the analyzer's optical system for accurate readings.

Calibrate Analog Outputs

Calibrating the analog output signals for proper data transmission.

Edit Calibrated Values

Fine-tuning previously calibrated hardware values.

Auto Prime All

Runs an automatic priming sequence for all fluid lines.

Prime Input Source (Sample/Reagent/...)

Selectively prime specific fluid sources like sample or reagents.

Priming Volume

Adjusting the volume of fluid used during the priming process.

Set NEW reagents BLANK

Setting the blank value for newly installed reagents.

Pumps, Valves and Stirrer

Checking the functionality of pumps, valves, and the stirrer.

Inputs Status

Checking the status of external inputs and assigned functions.

External Control

Directing analyzer operation via external controller using digital inputs.

Validate Grab Sample

Validates a sample without sending results to analog outputs.

Relays

Checking the functionality of the instrument's relays.

Analog Output

Checking the functionality of the two analog output channels.

LED and Detector Control

Testing optics functionality, adjusting LED intensity and detector gain.

Default and Lost or Forgotten Passwords

Information on default passwords and procedures for forgotten ones.

User Interface Tree

Hierarchical overview of the analyzer's menu structure and navigation.

Terms Definition

ALARM

Definitions for alarm types, values, and hysteresis.

RELAY

Definitions for relay modes and capabilities.

ANALOG OUTPUT

Definitions for analog output types, low, and high concentration values.

EXTERNAL INPUT

Definitions for external input labels, events, and actions.

DISPLAY PARAMETERS

Definitions for display settings like contrast and backlight time.

CALIBRATION PARAMETERS

Definitions for calibration parameters like standard, mode, and slope.

VALIDATION PARAMETERS

Definitions for validation parameters like source and number of repeats.

ANALYSIS PARAMETERS

Definitions for analysis parameters like mode, frequency, and units.

CLEANER PARAMETERS

Definitions for cleaner parameters like source, volume, and flow rate.

TEMPERATURE UNITS

Definitions for temperature unit selection.

METHOD PARAMETERS

Definitions for method parameters like cell wash and wavelength.

DATE

Definitions for selectable date formats.

TIME

Definitions for selectable time formats.

RECOVERY AFTER POWER FAILURE

Definitions for power failure duration and clean cycle settings.

ETHERNET PARAMETERS

Definitions for IP address and server settings.

RS-232 PARAMETERS

Definitions for baud rate settings.

LANGUAGE

Definitions for instrument language selection.

REVIEW/RESET ALARMS

Definitions for reviewing and resetting alarms and faults.

REVIEW CALIBRATION RESULTS

Definitions for displaying and printing calibration results.

REVIEW ANALYSIS RESULTS

Definitions for displaying and printing analysis results.

DELETE ALL CALIBRATION RESULTS

Definition for deleting the entire calibration database.

DELETE ALL ANALYSIS RESULTS

Definition for deleting the entire analysis database.

EDIT USER

Definitions for editing user names, passwords, and permissions.

DELETE USER

Definition for deleting a user account.

ADD USER

Definition for adding a new user account.

INSTRUMENT DETAILS

Definitions for instrument details like software version and serial number.

UNIT LABEL CHANGE

Definition for changing the instrument's label name.

PRINTING OPTIONS

Definitions for printing system and parameter configurations.

EDIT CALIBRATED VALUES

Definitions for adjusting calibrated values for pumps, optics, and gain.

PRIME FLUIDICS

Definitions for priming volume settings.

PUMPS, VALVES & STIRRER

Definitions for checking functionality of pumps, valves, and stirrer.

RELAYS

Definition for checking the functionality of relays.

ANALOG OUTPUTS

Definitions for testing analog output channels.

LED & ADC

Definitions for testing LEDs, intensity, and amplifier gain.

Maintenance Schedule

Changing Reagents

Procedure for safely changing reagent bottles and entering new blank values.

Installing Tubing Maintenance Kit

Instructions for replacing pump head tubing using the maintenance kit.

Cleaning the Reaction Cell

Steps for cleaning the reaction cell to maintain performance and accuracy.

Preparing the Cleaning solution

Recipes for preparing standard and extra strength cleaning solutions.

Cleaning the Sample Flow Chamber

Procedure for inspecting and cleaning the sample flow chamber.

Stand-By Mode and Extended Shutdown

How to put the system into standby or perform an extended shutdown.

Standby and On-Demand Modes

Overview

Introduction to the analyzer's modes of operation for power plant applications.

AUTO RESTART mode

Analyzer automatically restarts measurements after idle time.

MANUAL mode

Analyzer waits for operator command to start or resume measurements.

STAND-BY

Analyzer performs periodic house-keeping routines while in standby mode.

Factory Setup Recommendations When Operating In “ON-DEMAND" Mode

Recommended setup for operating the analyzer in an on-demand mode.

Customer Services

Notice of Compliance

Statements regarding radio frequency energy and compliance with FCC rules.

Declaration of Conformity

Manufacturer's declaration of compliance with safety and EMC standards.

Warranty Information

Details on warranty periods, exclusions, and limitations for the instrument.

Warranty Shipments/ Returns/Adjustments

Procedures for making warranty claims, returns, and adjustments.

Consumables

Information on ordering consumables and recommended product usage.

Assistance

Contact information for technical support and authorized dealers.

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