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Thermo Scientific Vanquish VH-P10 User Manual

Thermo Scientific Vanquish VH-P10
228 pages
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Vanquish
Pumps
VH-P10
OperatingManual
4820.4401ENRevision2.0a September2017
thermoscientific

Table of Contents

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Thermo Scientific Vanquish VH-P10 Specifications

General IconGeneral
Flow Rate0.001 to 10.000 mL/min
Pulsation<1%
Flow Rate Accuracy< 1.0 % at 1 mL/min using 100 % methanol
Flow Rate Precision<0.07% RSD
pH Range1 to 12

Summary

Using this Manual

About this Manual

Describes the manual's content, structure, and purpose for users.

Conventions

Explains typographical conventions, safety messages, and notices used in the manual.

Reference Documentation

Lists additional hardware and software documentation available for reference.

Safety

Safety Symbols and Signal Words

Explains safety symbols and signal words used to convey hazard information.

Intended Use

Specifies the intended use of the pump within the Vanquish system for research.

Safety Precautions

Provides general and specific safety guidelines for operating the pump.

Electrical Safety Precautions

Covers electrical safety measures to prevent shock and device damage.

General Residual Hazards

Warns about general hazards from substances and biohazards encountered.

In Case of Emergency

Provides instructions on actions to take in emergency situations.

Solvent and Additive Information

Details recommendations for using compatible solvents and additives for optimal performance.

Compliance Information

Outlines compliance with domestic and international EMC and safety standards.

Pump Overview

Pump Features

Highlights the main features of the Vanquish pump, such as dual-piston design and seal wash.

Operating Principle

Explains the pump's operating principle, including dual-piston design and flow path.

Interior Components

Identifies and describes the user-accessible interior components of the pump.

Piston Seal Wash System

Details the function and components of the active piston seal wash system.

Purge Unit

Explains the function of the purge unit and its connections.

Leak Detection

Describes the leak detection system and how it alerts users to leaks.

Operation

Explains how to operate the pump, primarily via computer software.

Unpacking and Transport

Unpacking and Moving

Provides instructions on inspecting packaging, unpacking the pump, and safe handling.

Scope of Delivery

Lists the items included in the pump's delivery package.

Installation

Safety Guidelines for Installation

Provides safety guidelines specifically for the installation process.

Installing the Pump

Outlines the steps for installing the pump hardware and software.

Site Requirements

Specifies environmental and power requirements for pump installation.

Accessing the Interior Components

Explains how to open the pump doors to access interior components.

Setting Up the Hardware

Describes how to set up the pump hardware and its connectors.

Connecting the Pump

Details how to connect the pump to the system via electrical and device connectors.

Setting Up the Flow Connections

Provides general rules and recommendations for setting up flow connections safely.

Guiding Capillaries and Tubing Through the System

Explains how to route capillaries and tubing using the system's tubing chase.

Connecting Fittings, Capillaries, and Tubing

Provides guidelines and steps for connecting fittings, capillaries, and tubing, including Viper capillaries.

Guiding Liquids to Waste

Explains how liquids from the leak tray and purge unit are guided to waste.

Connecting the Solvent Lines

Provides instructions on connecting solvent lines between reservoirs and the degasser.

Setting Up the Seal Wash System

Details setup, liquid choice, and flushing procedures for the seal wash system.

Connecting the Pump and Autosampler

Details how to connect the pump to the autosampler using a capillary.

Turning On the Pump

Provides step-by-step instructions for turning on the pump.

Setting Up the Pump in the Software

Explains how to configure the pump within the chromatography software.

Operation

Introduction to this Chapter

Introduces the chapter on pump operation and assumes initial setup is complete.

Safety Guidelines for Operation

Provides critical safety guidelines to follow during pump operation.

Control Elements

Describes the pump's interface elements like keypad and status indicators.

Power On/Off Control

Details how to control the pump's power using the system base button and main switch.

Use of Solvents and Additives

Provides guidelines for selecting and using solvents and additives for optimal performance.

Preparing the Pump for Operation

Details pre-operation steps, including first-time use and sample analysis preparation.

Important Operating Parameters

Details parameters like Flow ramps, Leak detection, Pressure limits, etc.

Purging the Pump

Explains the purpose, items required, and settings for purging the pump.

Optimizing the Performance of the Pump

General guidelines to optimize pump performance, including solvent use and maintenance.

Gradient Delay Volume, Dwell Volume, and Ripple

Explains gradient delay volume, dwell volume, and ripple in HPLC systems.

Installing Solvent Shut Off Valves

Details how to install optional solvent shut-off valves for flow control.

Shutting Down the Pump

Instructions for short-term and long-term shutdown of the pump.

Maintenance and Service

Introduction to Maintenance and Service

Introduces routine maintenance, service, and repair procedures.

Safety Guidelines for Maintenance and Service

Provides essential safety guidelines for performing maintenance and service.

General Rules for Maintenance and Service

General rules and recommendations for successful maintenance and service procedures.

Routine and Preventive Maintenance

A suggested maintenance plan with daily and regular tasks.

Flushing the Pump

Procedures for flushing the pump to avoid contamination or remove persistent issues.

Cleaning or Decontaminating the Pump

Instructions for cleaning and decontaminating the pump, with safety precautions.

Predictive Performance

Explains software functions for estimating consumable lifetime and scheduling maintenance.

Seal Wash System

Procedures for testing, replacing lines, and replacing the seal wash detector.

Pump Head

Covers maintenance tasks for the pump head, pistons, and seals.

Check Valves

Procedures for replacing and cleaning inlet and outlet check valves.

Inline Filter

Instructions for testing and replacing the inline filter or capillary mixer.

Mixing System

Procedures for testing and replacing static or capillary mixers.

Solvent Lines and Solvent Line Filters

Instructions for emptying, replacing solvent lines, and replacing solvent line filters.

Testing the Pump for Leakage

Method to test the pump for leaks after maintenance.

Replacing the Main Power Fuses

Instructions for replacing blown main power fuses.

Updating the Pump Firmware

Guide on how to update the pump firmware using Chromeleon.

Replacing the Doors

Instructions for removing and installing the pump doors.

Transporting or Shipping the Pump

Steps to prepare the pump for transport, including shutdown and disconnection.

Replacing the Slide-In Module

Step-by-step guide for removing and installing the slide-in module.

Troubleshooting

General Information about Troubleshooting

General information to help identify and eliminate operational problems.

Chromeleon Audit Trail Messages

Explains how messages in the Audit Trail indicate problem severity and types.

Messages

Information about common messages in the Chromeleon Audit Trail and their causes.

Resolving Leakage

Steps to locate and resolve leaks detected by the sensor.

Checking the Compression Values

How to check pump head compression values for troubleshooting.

Performing Pressure Recalibration

Procedure for recalibrating the pump's pressure sensor.

Testing the Inline Filter/Static Mixer for Permeability

How to test inline filters and static mixers for permeability.

Specifications

Performance Specifications

Details the performance specifications of the Vanquish pump.

Physical Specifications

Lists the physical specifications of the pump, including dimensions and weight.

Accessories, Consumables and Replacement Parts

General Information

General information on using authorized replacement parts and components.

Ship Kit

Lists the items included in the pump's ship kit.

Optional Accessories

Details optional accessories available for the Vanquish system.

Consumables and Replacement Parts

Lists parts for pump heads, filters, lines, reservoirs, and kits with part numbers.

Appendix

Compliance Information

States CE, cTUVus, WEEE, and FCC compliance declarations for the device.

Digital I/O

Explains the function and use of the pump's digital I/O ports for external signals.

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