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ThermoFisher Scientific iCAP 7000 Plus Series User Manual

ThermoFisher Scientific iCAP 7000 Plus Series
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iCAP 7000 Plus Series ICP-OES
Operating Manual
BRE0004150 Revision C January 2018

Table of Contents

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ThermoFisher Scientific iCAP 7000 Plus Series Specifications

General IconGeneral
BrandThermoFisher Scientific
ModeliCAP 7000 Plus Series
CategoryLaboratory Equipment
LanguageEnglish

Summary

Legal Notices

Legal Notices

Information regarding legal notices and copyright.

Using this Manual

About this Manual

Introduction to the manual's content and purpose.

Typographical Conventions

Explains formatting conventions used in the manual.

Signal Words

Defines safety signal words like CAUTION, WARNING, DANGER.

Viewpoint Orientation

Defines terms like 'left' and 'right' from the operator's perspective.

Data Input

Describes conventions for data input and computer interaction.

Topic Headings

Explains the structure of headings within chapters.

Reference Documentation

Lists other relevant documents for the ICP-OES system.

Contacting Us

Provides contact information for Thermo Fisher Scientific.

Assistance

Details how to get help and support for the instrument.

Suggestions to the Manual

Provides information on how to submit feedback or suggest changes.

System Accessories

Required Accessories

Lists mandatory accessories for the ICP-OES system.

Optional Accessories

Lists optional accessories that can enhance system functionality.

Functional Description

Introduction

Provides an overview of the ICP-OES system and its components.

Instrument Specification

Details the technical specifications of different iCAP models.

Optical System

Describes the echelle optical design and its components.

Detector Specifications

Details the specifications of the CID detector.

Detector Mode

Explains the Random Access Integration (RAI) detector mode.

Plasma Viewing Specifications

Describes the dedicated radial and duo view plasma configurations.

Plasma Source Specification

Details the RF generator and plasma source specifications.

Sample Introduction Specifications

Covers nebulizer, spray chamber, sample pump, and torch details.

Center Tube Options

Lists different center tube options for the torch.

Nebulizer Options

Discusses various nebulizer options available for the system.

Pump Tubing Options

Describes the requirements and considerations for peristaltic pump tubing.

Internal Standards Kit

Explains the use and function of the Internal Standards Kit.

Organic Solvent Analysis

Discusses specific considerations for analyzing organic solvents.

Light Organic Samples

Details sample introduction for light organic samples.

Heavy Organic Samples

Details sample introduction for heavy organic samples.

Volatile Organic Samples

Discusses controlling sample loading for volatile organic samples.

High Dissolved Solid Samples

Addresses challenges and accessories for samples with high dissolved solids.

Argon Humidifier Accessory

Explains the function of the Argon Humidifier accessory.

Aerosalt Nebulizer

Describes the Aerosalt Nebulizer for high dissolved solids.

Parallel Path Nebulizer

Details the Parallel Path Nebulizer for high dissolved solids.

Sheath Gas Adaptor

Explains the use of the Sheath Gas Adaptor for analytical stability.

HF Samples

Discusses specific components and procedures for analyzing HF samples.

Safety

Safety Symbols and Signal Words in this Manual

Explains safety symbols, signal words, and general guidelines.

Observing this Manual

Emphasizes reading and understanding safety information before operation.

Safety Symbols on the Instrument

Describes warning labels found on the instrument itself.

Rating Plate

Explains the importance of the instrument's rating plate for identification.

Intended Use

Defines the proper usage guidelines and limitations of the ICP-OES system.

Intended User

Identifies the primary audience and required knowledge for using the manual.

Permitted Materials

Lists materials and gases compatible with the ICP-OES system.

Electric Safety Precautions

Details critical safety measures related to high voltage and electrical hazards.

Impaired Safety Protection

Addresses actions to take when safety features are compromised.

In Case of Emergency

Provides procedures for safely shutting down the system in an emergency.

Residual Hazards

Warns about potential hazards like toxic gases, suffocation, and hot surfaces.

Personal Protective Equipment

Recommends appropriate PPE for handling hazardous materials.

Installation

Safety Guidelines for Installation

Outlines essential safety precautions during system installation.

Spectrometer Dimensions

Provides physical dimensions and weight of the ICP-OES spectrometer.

Installation Requirements

Details the environmental and resource prerequisites for installation.

Before Installation

Lists preparatory steps and considerations before beginning the installation.

Location Requirements

Specifies ideal placement and space requirements for the instrument.

Environmental Requirements

Defines acceptable temperature, humidity, and pressure for operation.

Electrical Requirements

Details the necessary electrical supply specifications and connections.

Gas Requirements

Specifies the type, purity, and pressure of gases required for operation.

Recirculating Chiller

Describes the requirements and specifications for the cooling system.

Waste Storage

Discusses proper procedures and containers for waste disposal.

Spectrometer Fume Extraction

Emphasizes the critical need for and setup of fume extraction.

Sample Fume Extraction

Addresses additional extraction needs for volatile or acidic samples.

Communications Interface

Explains the Ethernet connection for data station communication.

Spectrometer Communication Requirements

Details firewall and IP address settings for instrument communication.

Data Station Requirements

Lists the hardware and software specifications for the data station PC.

Installation Checklist

Provides a summary of site requirements for installation.

System Operation

Safety Guidelines for Operation

Lists safety precautions to follow during instrument operation.

Preparing the System for Use

Describes initial steps to power up and prepare the ICP-OES for operation.

LED Indicators

Explains the meaning of various LED indicators on the instrument.

Instrument Optimization

Discusses the importance and process of optimizing instrument performance.

Method Optimization

Details parameters affecting data and the need for method-specific optimization.

Setting the Pump Tension

Explains how to adjust pump tension for optimal operation and tubing life.

Standard Sample Introduction Glassware Assembly

Guides the assembly and installation of glassware for sample introduction.

Duo Torch Assembly

Provides instructions for assembling and installing the Duo Torch.

Radial Torch Assembly

Provides instructions for assembling and installing the Radial Torch.

Connection of Pump Tubing

Details how to connect pump tubing for sample introduction.

Radial View Interfaces on a Duo Instrument

Explains the radial view interfaces for Duo instruments.

Radial Glass Window

Describes the cleaning procedure for the radial glass window.

Radial POP Interface

Details the Radial POP interface and its alignment procedure.

Example Standard Operating Procedures

Provides a sample procedure for setting up and running analyses.

Preparing the System

Outlines steps for preparing the system before starting operations.

Lighting the Plasma

Describes the procedure for igniting the plasma and checking interlocks.

Setting Up Analyses

Guides users through creating LabBooks and setting up analytical methods.

Running the Analysis

Details how to schedule and run analyses using the Qtegra software.

Reporting Results

Explains how to generate and customize reports for acquired data.

Exporting LabBooks

Describes how to export LabBooks and other data files.

Auto Peak Adjust

Explains the Auto Peak Adjust procedure for wavelength accuracy.

Shutting Down the System

Provides step-by-step instructions for safely shutting down the instrument.

Troubleshooting

Safety Guidelines for Troubleshooting

Lists safety precautions to observe during troubleshooting activities.

Problems with Plasma Ignition

Addresses common issues related to starting and maintaining plasma ignition.

Ignition Spark

Describes checks for the ignition spark mechanism.

RF Power to the Coil from the RF Generator

Explains how to check RF power delivery to the induction coil.

Problems with Plasma Going out Unexpectedly

Discusses potential causes for the plasma extinguishing during operation.

Resolving Problems with Analytical Results

Addresses issues with plasma going out and resolving analytical result problems.

To check sample introduction

Provides steps to verify the sample introduction system's condition.

Resolving Specific Analytical Problems

Addresses specific issues like poor precision, accuracy, and detection limits.

Poor Precision

Discusses causes and solutions for inconsistent analytical results.

Poor Accuracy/Feedback

Details how to resolve issues related to inaccurate or delayed feedback.

Poor Detection Limits

Explains how to improve detection limits, often related to precision issues.

Suggested Maintenance in Case of Poor Precision and Detection Limits

Offers maintenance steps to address precision and detection limit problems.

Replacing the Pump Tubing

Guides on selecting and replacing pump tubing for optimal performance.

Preventing Blockage of the Nebulizer

Provides suggestions to prevent nebulizer tip blockage.

Removing Solids from the Nebulizer

Describes procedures for cleaning solids from the nebulizer.

Maintenance

Safety Guidelines for Maintenance

Lists safety precautions to follow when performing maintenance tasks.

Cleaning the Instrument

Provides general guidelines for cleaning the instrument and accessories.

Cleaning and Decontaminating the Sample Introduction System

Details procedures for cleaning sample introduction components.

Cleaning the Torch

Explains methods for cleaning the torch, including carbon deposit removal.

Cleaning the Spray Chamber

Describes procedures for cleaning the spray chamber.

Cleaning the Nebulizer

Provides instructions for cleaning the nebulizer.

Cleaning the Purged Optical Path Window

Details the process for cleaning the POP window.

Cleaning the Radial View Interfaces

Explains how to clean radial view interfaces on Duo instruments.

Preventive Maintenance

Covers periodic checks for maintaining optimal performance.

Water Chiller

Highlights critical maintenance aspects of the water chiller.

Water Filter

Advises on checking and maintaining the water filter.

Gas Filters

Advises on checking and maintaining gas filters.

Torch Alignment

Guides on performing torch alignment for optimal results.

Thermo Fisher Scientific Service

Outlines services provided by Thermo Fisher Scientific and safety advice for returns.

Safety Advice for Possible Contamination

Provides safety recommendations for returning contaminated parts.

Returning Parts

Gives instructions and precautions for returning parts for exchange or repair.

Services to be Performed by Thermo Fisher Scientific Service Only

Specifies maintenance tasks exclusively handled by service engineers.

Advanced Hardware

Sprint Valve

Describes the Sprint Valve rapid sample introduction system.

Supported Autosamplers

Lists autosamplers compatible with the Sprint Valve system.

Functional Description

Details the construction and material properties of the Sprint Valve.

Plumbing Connections

Guides on establishing plumbing connections for the Sprint Valve.

Connecting the Tubing

Provides specific instructions for connecting tubing to the Sprint Valve.

Sprint Valve Plugin in Qtegra ISDS Software

Explains how to configure the Sprint Valve using the Qtegra plugin.

Description of Timings

Details the timing parameters for Sprint Valve operation.

Manual Control Features

Describes manual control options for the Sprint Valve.

External Sprint Valve Configurator

Explains how to access manual control features via the external configurator.

Sprint Valve Plugin in Qtegra ISDS Software

Explains how to configure the Sprint Valve using the Qtegra plugin.

Manual Sampling Using the Sprint Valve

Guides on performing manual sampling with the Sprint Valve.

Routine Maintenance

Outlines daily and weekly maintenance tasks for the Sprint Valve system.

Regular Inspection of Components

Advises on visually inspecting Sprint Valve system components.

Checking for Leaks

Details procedures for checking and replacing tubing for leaks.

Cleaning the System

Emphasizes the importance of cleaning the Sprint Valve system.

Daily External Cleaning

Provides guidance for daily external cleaning of the Sprint Valve.

Cleaning the 6-Port/7-Port Valve

Details the periodic disassembly and cleaning of the 6/7-port valve.

Re-Homing the 6-Port/7-Port Valve

Explains the procedure for re-homing the valve after removal.

Replacing or Reorienting the 6-Port/7-Port Valve

Guides on replacing or reorienting the valve.

Additional Gas Accessory

Installing the Additional Gas Accessory

Provides instructions for installing the additional gas accessory.

Optional Accessories

Autosampler

Describes the autosampler and its configuration for ICP-OES.

Autosampler Setup

Guides on setting up the autosampler tubing connection.

Ultrasonic Nebulizer

Details the use and setup of the ultrasonic nebulizer for increased sensitivity.

To set up the ultrasonic nebulizer

Provides instructions for connecting and setting up the ultrasonic nebulizer.

Hydride Generation

Explains hydride generation techniques for enhanced detection capabilities.

On-line Hydride Generation Kit

Describes the on-line hydride generation kit and its components.

Setup

Outlines setup procedures for hydride generation accessories.

Gas Liquid Separator (GLS)

Explains the function and assembly of the Gas Liquid Separator.

To prepare the Gas Liquid Separator

Provides instructions for preparing the Gas Liquid Separator before use.

Pump Tubing

Details the color-coded pump tubing for the GLS unit.

Legal Documents

Regulatory Compliance and Forms

Covers WEEE compliance, RoHS, and the Declaration of Conformity.

Health and Safety Form

Provides the Health and Safety Declaration form for material returns.

Glossary

Glossary of Terms

Defines technical terms, acronyms, and abbreviations used in the manual.

Index

Index

Provides an alphabetical index for quick reference to topics and page numbers.

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