3.3.2 Installing the fused silica transfer line insert ........................................................... 16
3.3.3 Connecting the transfer line to UNITY-xr .................................................................. 18
3.4 Installing the cold trap ............................................................................................................ 22
3.5 Check for gas leaks ................................................................................................................. 24
4. Installing Markes Instrument Control (MIC) software ............................................................... 26
4.1 System Configuration .............................................................................................................. 26
4.2 Running the software .............................................................................................................. 26
4.2.1 Configuring the software ........................................................................................... 26
4.2.2 Detecting the UNITY-xr ............................................................................................... 30
5. Installation qualification ............................................................................................................. 31
5.1 Leak Testing ............................................................................................................................ 31
5.2 Conditioning the cold trap ...................................................................................................... 31
5.3 System checkout ..................................................................................................................... 33
6. Appendix ...................................................................................................................................... 34
6.1 UNITY-xr Electronic Gas Control with the Agilent 6890GC.................................................... 34
6.1.1 Procedure ................................................................................................................... 34
6.1.2 6890 inlet settings .................................................................................................... 35
6.2 UNITY-xr Electronic Gas Control with the Agilent 7890GC.................................................... 36
6.2.1 Procedure ................................................................................................................... 36
6.2.2 7890 Inlet Setup ........................................................................................................ 37
6.2.3 7890 Inlet Settings .................................................................................................... 37
6.3 UNITY-xr Electronic Gas Control with the Shimadzu QP 2010 (Plus) GCMS fitted
with AFC ................................................................................................................................... 38
6.3.1 Gas connections between UNITY-xr and the Shimadzu AFC................................... 38
6.3.2 Configuring the Shimadzu GC software ................................................................... 39
6.3.3 Flow stability ............................................................................................................... 40
6.3.4 Ready / Start connections between UNITY-xr and Shimadzu GC........................... 41
6.4 UNITY-xr Electronic Gas Control with the Thermo DPFC ....................................................... 42
6.4.1 Procedure ................................................................................................................... 42
6.4.2 Configuring the Thermo GC software ....................................................................... 42
6.5 UNITY-xr Electronic Gas Control with the Thermo 1300 Series GC ...................................... 43
6.5.1 Installing the Markes TD to the Thermo Scientific TRACE Series 1300 GC .......... 43
6.6 Testing the ECC setup ............................................................................................................. 46
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