Merck Spectroquant Prove 100 - Operating Manual

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Main Page

Contents3
Photometry8
Photometric Test Kits10
Cell Tests10
Additional Reagents10
Reagent Tests11
Notes for Practical Use12
Measuring Range12
Influence of Ph13
Influence of Temperature13
Time Stability14
Influence of Foreign Substances14
Suitability for Use in Seawater14
Dosing the Reagents15
Shelf-Life of the Reagents15
Sample Preparation16
Taking Samples16
Preliminary Tests16
Dilution16
Filtration17
Homogenization18
Decomposition18
Pipetting System20
Analytical Quality Assurance (AQA)22
Quality Control at the Manufacturer22
Quality Control for the User24
Checking the Spectrometer25
Checking the Overall System26
Checking the Pipettes27
Checking Thermoreactors27
Determination of Sample Influences (Matrix Effects)28
Definition of Errors28
Testing for Handling Errors28
Overview30
Scope of Delivery30
Product View30
Display and User Interface31
Main Menu Navigation32
Screen Layout Concentration Measurement Overview33
Screen Layout Method List Overview33
Screen Layout Results Overview34
Main Menu Buttons35
Safety40
Intended Use40
Function and Operational Safety41
Target Group and User Qualification41
Handling Hazardous Substances41
General Notes on Handling42
Initial Setup42
Connecting the Power Supply42
Connecting the Power Adapter42
First Power-On43
Language Setup43
Date, Time and Country-Specific Settings43
Self-Test44
Connecting Optional Peripheral Devices45
Communication Ports45
Printer45
USB Memory Device/Barcode Reader45
Operation46
Switching the Spectrometer on or off46
Energy-Saving Mode - Display47
Switching off47
System Setup48
Information49
Interface (Setup 1)49
Region (Setup 2)50
Country Zone EU/US, Decimal Separator51
Quality (Setup 3)52
Automation (Setup 4)53
User Management54
Edit User, E.g. Change Password54
Create User54
Delete User54
Service55
Backup/Restore55
Exporting Log And/Or System Files55
Importing User-Defined Methods55
Updates56
Firmware and Method Update Spectrophotometer56
Measurements57
Performing a Measurement58
Measuring with a Round Cell with a Round Cell with Closed Lid58
Measuring with Rectangular Cells with Open Lid58
Zero Adjustment60
When to Repeat the Zero Adjustment61
Zero Adjustment for User-Defined Concentration Methods62
Zero Adjustment Procedure for Pre-Programmed Concentration Methods62
Zero Adjustment for Ad Hoc Absorbance/Transmission Measurements63
Zero Adjustment for Ad Hoc Kinetic Measurements64
Zero Adjustment for Ad Hoc Spectra65
Zero Adjustment (Baseline) Procedure for Ad Hoc Spectrum Measurement65
Zero Adjustment for User-Defined Kinetic Methods66
Zero Adjustment for User-Defined Spectrum Methods67
Method List68
Selecting a Method Manually68
Searching and Filtering the Method List68
Programmng a User-Defined Method69
User-Defined Concentration Methods70
Calibration Data/Calibration Function for Single-Wavelength Methods70
Programming/Mofifying User-Defined Methods (Single Wavelength)71
Enter Value Pairs72
Measure Value Pairs72
Enter a Function73
Calculated Calibration Function73
Entering Coefficients73
Calibration Data and Calibration Function of Multi-Wavelength Methods74
Programming/Modifying User-Defined Methods (Multi-Wavelength)74
Programming a User-Defined Spectrum Method78
Programming a User-Defined Kinetic Method80
Copying/Duplicating a User-Defined Method82
Modifying a User-Defined Method from the Method List83
Deleting a User-Defined Method from the Method List84
Export User-Defined Method to a USB Memory Device85
Measuring in Concentration Mode86
Measuring Cell Tests with a Barcode86
Measuring Reagent Tests with Autoselector88
Measuring Reagent-Free Tests and User-Defined Methods88
Exceeding the Upper or Lower Limits of the Measuring Range89
Method-Specific Settings for Concentration Mode90
Measuring Diluted Samples91
Sample Blank Value92
Reagent Blank Value93
Automatic Turbidity Correction95
User Recalibration (Standard Adjustment)96
Calibration of Value Pairs for User-Defined Methods96
Value Pair Calibration97
Matrixcheck99
If Spiking Is Active101
If Diluting Is Active101
Ad Hoc Measurement102
Ad Hoc ABS/TRANS Measurement103
Ad Hoc Spectrum Measurement104
Ad Hoc Kinetic Measurement105
Spectrum - General Information106
Recording the Spectrum106
Baseline106
Content of the Information Bar in Spectrum Measurements107
Evaluating a Spectrum108
Kinetics110
Recording Kinetics110
Evaluating a Kinetic111
AQA (Analytical Quality Assurance)112
Spectrophotometer Monitoring (AQA1)112
Photometric Accuracy112
Total System Monitoring (AQA2)113
Wavelength Accuracy113
Stray Light Test113
Spectral Resolution113
AQA Overview114
Perform AQA1 Status Check115
Perform AQA2 Status Check116
AQA1 Selection List117
Activating and Deactivating an AQA1 Test118
Editing an AQA1 Test118
Performing an AQA1 Test120
Creating a User-Defined AQA1 Test122
AQA2 Selection List123
Activating and Deactivating an AQA2 Test124
Editing an AQA2 Test124
Performing an AQA2 Test126
Perform Pipecheck128
Timer130
Results and Measurement Datasets131
Displaying the Results132
Show Details of One Result133
Filtering Results to Further Process Measurement Datasets134
Panorama - Value Control Card135
Print Results and Measurement Datasets136
Export Results and Measurement Datasets137
User Groups138
User Rights in Detail138
Activating/Deactivating the User Management Function139
Create an Administrator/User Account140
Edit or Delete a User141
Login/Logout142
Change Password with User Rights Only143
To Logout as User or Administrator143
Maintenance and Cleaning144
Exchanging the Buffer Battery144
Exchanging the Halogen Lamp (Prove 100)144
Disposal of Batteries144
Cleaning the Housing and Display146
Cleaning the Cell Compartment146
Cleaning the Cell Compartment Cover and the Rear Cavity148
Cleaning the Detector Lens149
Error Causes and Troubleshooting150
Technical Data152
Accessories and Test Media158
Glossary160
List of Smart Icons on Display162

Merck Spectroquant Prove 100 - Operating Manual

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