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860 KF Thermoprep
Metrohm 860 KF Thermoprep User Manual
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860 KF Thermopr
ep
Manual
8.860.8003EN / 2019-
12-02
2
Table of Contents
Default Chapter
5
Table of Contents
5
1 Introduction
9
Instrument Description
9
Instrument Components
9
Intended Use
10
About the Documentation
10
Symbols and Conventions
10
Safety Instructions
11
General Notes on Safety
11
Electrical Safety
11
Personnel Safety
12
Flammable Samples and Solvents
13
Recycling and Disposal
13
2 Overview of the Instrument
14
Figure 1 Front 860 KF Thermoprep
14
Figure 2 Rear 860 KF Thermoprep
15
Checks
16
Connecting the Instrument to the Power Grid
16
Location
16
Packaging
16
Setting up the Instrument
16
Figure 3 Loosening the Adapter
17
Mounting the Support Rod
17
Figure 4 Mounting the Support Rod
18
Figure 5 Mounting the Tubing
19
Figure 6 Attaching the Adapter
19
Figure 7 Mounted Support Rod
20
Figure 8 Mounting the Sample Holder
20
Mounting the Sample Holder
20
Mounting the Needles
21
Figure 9 Mounting the Needles
22
Figure 10 Mounting the Heating Tubing (Rear View)
23
Mounting the Heating Tubing
23
Figure 11 Connecting the Heating Tubing
24
Figure 12 Mounting the Dust Filter
24
Mounting the Dust Filter
24
Assembling Drying Flasks
25
Figure 13 Preparing the Drying Flasks
25
Figure 14 Mounting the Tubings
26
Assembling the Air/Nitrogen Connector
27
Figure 15 External Gas Connector
27
Inserting the Heating Tube into the KF Titration Cell
27
Figure 16 Coulometric KF Titration Cell
28
Figure 17 Volumetric KF Titration Cell
29
Figure 18 Power Switch
30
Figure 19 Keypad of the Operating Unit
30
Switching the Instrument on and off
30
The Keypad
30
Display Elements
31
Figure 20 Main Dialog
31
Status Display
31
The Display
31
Error Messages
32
Modifying Numerical Values and Settings
32
Modifying Numerical Values
33
Parameters
33
Selecting from a Selection List
33
Configuration
35
5 Performing a Determination
36
Conditioning the System
36
Preparing the KF Titration Cell
36
Preparing the 860 KF Thermoprep
37
Figure 21 Insert the Sample Vessel into the Oven
38
Figure 22 Move the Guide Head down
38
Figure 23 Insert the Needle
39
Determining the Blank Value
40
Determining Samples
41
6 Operation and Maintenance
43
General
43
Care
43
7 Troubleshooting
44
Problems and Their Solutions
44
8 Appendix
45
Practical Notes
45
Literature
46
9 Technical Specifications
47
Oven
47
Gas Flow
47
Outlet Heater
47
Power Connection
48
Ambient Temperature
48
Reference Conditions
48
Dimensions
48
10 Accessories
49
Index
50
5
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Metrohm 860 KF Thermoprep Specifications
General
Brand
Metrohm
Model
860 KF Thermoprep
Category
Laboratory Equipment
Language
English
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