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Metrohm Professional IC Vario 940 User Manual

Metrohm Professional IC Vario 940
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940 Professional IC Vario
940 Professional IC Vario ONE/Prep 2
Manual
8.940.8003EN / 2017-07-31

Table of Contents

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Metrohm Professional IC Vario 940 Specifications

General IconGeneral
BrandMetrohm
ModelProfessional IC Vario 940
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction

Instrument Description

Detailed description of the 940 Professional IC Vario instrument and its features.

Intended Use

Specifies the intended application of the 940 Professional IC Vario ONE/Prep 2 for ion chromatography.

Safety Instructions

Provides essential safety guidelines for operating the instrument, covering general, electrical, and chemical hazards.

Symbols and Conventions

Explains symbols, formatting, and warnings used throughout the documentation for clarity.

Overview of the Instrument

Front Panel Overview

Details the components and features visible on the front panel of the instrument.

Rear Panel Overview

Illustrates and describes the connections and ports located on the rear panel of the instrument.

Feed-throughs for Capillaries and Cables

Explains the openings and pathways for routing capillaries and cables into and out of the instrument.

Installation

Setting Up the Instrument

Covers the initial steps for setting up the instrument, including packaging, checks, and location.

Capillary Connections in the IC System

Explains how to make proper capillary connections within the IC system for optimal performance.

Removing the Handle

Instructions on how to remove the instrument's handle for installation purposes.

Removing Transport Locking Screws

Guidance on removing transport locking screws before the initial start-up of the instrument.

Connecting the Drainage Tubing and Leak Sensor

Details on connecting the drainage tubing and leak sensor for safety and leak detection.

Column Thermostat

Information on the column thermostat, which regulates separation column temperature.

Connecting the Eluent Bottle

Step-by-step guide for connecting the eluent bottle to the instrument for analysis.

Connecting the Eluent Degasser

Instructions for connecting the eluent degasser to ensure proper eluent quality.

Installing the High-Pressure Pump

Details on installing the high-pressure pump, a key component for eluent delivery.

Installing an Inline Filter

Procedure for installing an inline filter to protect the separation column from contamination.

Installing the Pulsation Absorber

Guidance on installing the pulsation absorber to protect the separation column from pressure fluctuations.

Injection Valve

Description of the injection valve's function and installation for sample introduction.

Installing the Conductivity Detector

Steps for installing the conductivity detector, a primary detection method.

Installing the Amperometric Detector

Instructions for installing the amperometric detector, an alternative detection method.

Connecting the Sample Degasser (Optional)

Details on connecting the optional sample degasser for improved sample reproducibility.

Peristaltic Pump

Information on installing and operating the peristaltic pump for fluid transfer.

Installing the 6-Port Valve

Procedure for installing the 6-port valve, used for sample preparation.

Connecting the Instrument to a Computer

Steps to connect the instrument to a computer for control and data management.

Connecting the Instrument to the Power Grid

Instructions for safely connecting the instrument to the electrical power supply.

Initial Start-Up

Comprehensive guide for the initial start-up sequence of the instrument and system.

Connecting and Rinsing the Guard Column

Procedure for connecting and rinsing the guard column to protect the separation column.

Connecting the Separation Column

Detailed steps for connecting the separation column, the heart of the analysis.

Conditioning

Guidance on conditioning the system with eluent to achieve a stable baseline.

Operation

Operation and Maintenance

IC System Operation and Maintenance

Covers the operation and maintenance of the overall IC system, including care and troubleshooting.

Capillary Connections Maintenance

Guidelines for maintaining capillary connections to ensure leak-tightness and low dead volume.

Servicing the Door

Instructions for servicing the instrument door, including cleaning precautions.

Column Thermostat - Replacing Capillaries

Procedure for replacing capillaries within the column thermostat for maintenance.

Handling the Eluent

Essential measures for handling eluents correctly to ensure stable analysis results.

Servicing the Eluent Degasser

Steps for loosening and reconnecting connection tubing at the eluent degasser.

Operating the High-Pressure Pump

Important recommendations for operating the high-pressure pump to prevent damage and ensure performance.

Servicing the High-Pressure Pump

Detailed procedures for servicing the high-pressure pump, including valve and piston maintenance.

Servicing the Inline Filter

Instructions for replacing the filter in the inline filter unit.

Servicing the Pulsation Absorber

Note that the pulsation absorber is maintenance-free and should not be opened.

Injection Valve Maintenance

Best practices for injection valve maintenance, typically during annual service.

Detector Servicing

Guidance to follow maintenance instructions provided in the detector's specific manual.

Rinsing the Sample Path

Procedure for rinsing the sample path to prevent carry-over and ensure accurate measurements.

Peristaltic Pump Operation and Servicing

Notes on operating the peristaltic pump and procedures for servicing it, including tubing replacement.

Separation Column Care

Information on separation column efficiency, protection, storage, and regeneration.

Quality Management and Qualification with Metrohm

Details on Metrohm's support for quality management and instrument qualification services.

Troubleshooting

Technical Specifications

Reference Conditions

Defines the reference conditions under which the technical specifications are valid.

Instrument Specifications

Lists the general specifications for the instrument, including IC system and materials.

Ambient Conditions

Specifies the ambient temperature and humidity requirements for operation, storage, and transport.

Housing Specifications

Provides the physical dimensions and control indicators of the instrument housing.

Weight

States the weight of the instrument, including its article number.

Leak Sensor Specifications

Technical details for the electronic leak sensor, noting no calibration is necessary.

Column Thermostat Specifications

Specifications for the column thermostat, including temperature range, heating/cooling, and reproducibility.

Eluent Degasser Specifications

Technical specifications for the eluent degasser, including material and vacuum establishment time.

High-Pressure Pump Specifications

Detailed specifications for the high-pressure pump, covering type, flow rate, pressure, and safety features.

Injection Valve Specifications

Specifications for the injection valve, including actuator switching time, pressure, and material.

Detector Specifications

Indicates that detector specifications are found in the detector's manual.

Sample Degasser Specifications

Technical specifications for the sample degasser, including material and vacuum establishment time.

Peristaltic Pump Specifications

Specifications for the peristaltic pump, covering type, speed, and pumping characteristics.

6-Port Valve Specifications

Specifications for the 6-port valve, including switching time, pressure, and material.

Power Connection Specifications

Details on power requirements, consumption, and the power supply unit.

Interface Specifications

Lists the available interfaces for connecting peripherals like USB, MSB, and detectors.

Accessories

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