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Metrohm 761 Compact IC User Manual

Metrohm 761 Compact IC
228 pages
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761 Compact IC
METROHM Ltd.
CH-9101 Herisau
Switzerland
Phone ++41 71 353 85 85
Fax ++41 71 353 89 01
8.761.1063
Instructions for Use

Table of Contents

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Metrohm 761 Compact IC Specifications

General IconGeneral
BrandMetrohm
Model761 Compact IC
CategoryLaboratory Equipment
LanguageEnglish

Summary

1 Introduction

1.1 Instrument Description

Provides an overview of the 761 Compact IC system and its components for ion chromatography analysis.

1.2 Parts and Controls

Details the various components and controls of the 761 Compact IC instrument, including front and rear panel elements.

1.3 Information on the Instructions for Use

Explains the organization and notation conventions used within the 761 Compact IC Instructions for Use manual.

1.4 Safety Notes

Covers essential safety precautions for electrical safety, handling of solvents, and general precautionary rules.

2 Installation

2.1 Overview

Presents a flow chart of the installation process and details internal connections within the 761 Compact IC.

2.2 Setting Up the Instrument

Guides on proper packaging, checking, and locating the instrument for optimal operation.

2.3 Attaching the Accessories

Provides step-by-step instructions for connecting various accessories like the detector block and tubing.

2.4 Mains Connection

Details the procedure for connecting the instrument to the power supply, including setting voltage and fuses.

2.5 Connection to the PC

Explains how to connect the 761 Compact IC to a PC, including software installation and basic settings.

2.6 High-Pressure Pump

Describes the installation and operation of the high-pressure pump, including the pulsation dampener.

2.7 Precolumns and Separating Columns

Covers the installation and selection of precolumns and separating columns for optimal separation.

2.8 Suppressor Module

Provides general information on the suppressor module, its preparation, and connection for chemical suppression.

2.9 Putting into Operation

Guides users through the initial setup and operation procedures for the instrument, with and without a suppressor.

2.10 Connection of External Devices

Details how to connect external devices such as autosamplers to the 761 Compact IC.

3 Operating Tutorial

3.1 Requirements

Lists the necessary instruments, accessories, and solutions for performing the operating tutorial.

3.2 Preparations

Outlines the key installation steps and preparations required before starting the operating tutorial.

3.3 Calibration

Guides users through the process of calibrating the IC system using a standard solution.

3.4 Sample Determination

Explains how to inject and analyze sample solutions after the system has been calibrated.

4 Operation

4.1 Fundamentals of the Operation

Describes basic operations like starting/closing the program, glossary of terms, and program windows.

4.2 Instrument and Software Settings

Covers settings for fonts, security system, global preferences, and COM port configuration.

4.3 Systems

Explains how to manage and configure systems, including system functions and settings.

4.4 Methods

Details how to create, manage, and use methods for data acquisition, integration, and calibration.

4.5 Chromatograms

Covers viewing, handling, printing, and graphical representation of chromatograms.

4.6 Sample Queue

Explains how to manage sample queues for automated analysis and use the queue editor.

4.7 Batch Reprocessing

Guides users on reprocessing chromatograms in batches, including setting options and performing reprocessing.

5 Notes – Maintenance – Faults

5.1 Practical Notes on Ion Chromatography

Offers tips on column handling, protection, and practical considerations for ion chromatography analysis.

5.2 Maintenance and Servicing

Provides instructions for general care, passivation, and routine maintenance of the instrument.

5.3 Faults and Malfunctions

Helps identify and rectify common malfunctions and errors encountered during instrument operation.

5.4 Diagnostic Tests / Validation / GLP

Outlines procedures for testing instrument functionality, validation, and adhering to GLP requirements.

6 Appendix

6.1 Technical Data

Provides detailed specifications for conductivity measurement, detector, injection valve, and pumps.

6.2 Standard Equipment

Lists the standard parts and accessories included with the 761 Compact IC instrument.

6.3 Optional Accessories

Details various optional accessories available for enhancing the functionality of the 761 Compact IC.

6.4 Warranty and Conformity

Covers warranty information, EU declaration of conformity, and system validation.

6.5 Index

An alphabetical listing of topics and their corresponding page numbers for quick reference.

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