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930 Compact IC Flex
Metrohm 930 Compact IC Flex User Manual
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930 Compact IC Flex
930 Compact IC Flex Oven/SeS/PP
Manual
8.930.8019EN / v3 / 2023-03-31
2
Table of Contents
Table of Contents
5
Introduction
9
Instrument Description
9
Accessories and Additional Information
11
Symbols and Conventions
11
Intended Use
13
Responsibility of the Operator
13
Requirements for Operating Personnel
14
Safety Instructions
14
General Notes on Safety
14
Electrical Safety
14
Tubing and Capillary Connections
15
Flammable Solvents and Chemicals
16
Recycling and Disposal
16
Overview of the Device
17
Front
17
Figure 1 Front
17
Rear
18
Figure 2 Rear
18
Feed-Throughs for Capillaries and Cables
20
Figure 3 Feed-Throughs on the Door
20
Figure 4 Openings for Capillaries and Cables
21
Figure 5 Ducts for Capillaries
22
Setting up the Instrument
23
Packaging
23
Checks
23
Location
23
Capillary Connections in the IC System
23
Removing Transport Locking Screws
26
Figure 6 Removing the Transport Locking Screws
26
Connecting the Drainage Tubing and Leak Sensor
27
Installing the Drainage Tubing
27
Connecting the Leak Sensor
29
Column Oven
29
Connecting the Eluent Bottle
30
Figure 7 Installing the Eluent Bottle Cap
30
Figure 8 Installing the Tubing Weighting and Aspiration Filter
32
Installing the High-Pressure Pump
34
Figure 9 High-Pressure Pump with Purge Valve
34
Installing an Inline Filter
35
Installing the Pulsation Absorber
35
Figure 10 Inline Filter
35
Injection Valve
36
Figure 11 Pulsation Absorber
36
Figure 12 Exchanging the Sample Loop
37
Metrohm Suppressor Module (MSM)
38
Inserting the Rotors
39
Connecting the Metrohm Suppressor Module (MSM)
41
Figure 13 Metrohm Suppressor Module (MSM) - Connection Capillaries
42
Peristaltic Pump
46
Installing the Peristaltic Pump
46
Mode of Operation for the Peristaltic Pump
50
Figure 14 Peristaltic Pump
50
Metrohm CO Suppressor (MCS)
51
General Information on the MCS
51
Connecting the MCS
51
Figure 15 Connecting the MCS
52
Installing the Adsorber Cartridge
53
Installing the Conductivity Detector
55
Installing the Amperometric Detector
56
Connecting the Instrument to a Computer
56
Connecting the Instrument to the Power Grid
57
Initial Start-Up
58
Connecting and Rinsing the Guard Column
60
Connecting and Rinsing the Separation Column
62
Conditioning
65
Operation
67
Operation and Maintenance
68
IC System
68
Operation
68
Care
68
Maintenance by Metrohm Service
68
Shutting down and Recommissioning
69
Capillary Connections
70
Servicing the Door
70
Column Oven - Replacing the Capillaries
70
Figure 16 Column Oven
71
Handling the Eluent
72
Manufacturing Eluent
72
Changing the Eluent
73
Notes on Operating the High-Pressure Pump
73
Servicing the High-Pressure Pump
74
Figure 17 High-Pressure Pump - Parts
74
Figure 18 High-Pressure Pump - Cross-Section
81
Figure 19 Tool for Piston Seal (6.2617.010)
82
Figure 20 Removing the Piston Cartridge from the Pump Head
82
Figure 21 Inserting the Piston Seal into the Tool
83
Figure 22 Parts of the Piston Cartridge
84
Servicing the Inline Filter
87
Figure 23 Inline Filter - Removing the Filter
88
Servicing the Pulsation Absorber
90
Injection Valve
90
Metrohm Suppressor Module (MSM)
90
Notes for Operating the Metrohm Suppressor Module (MSM)
90
Taking Care of the Suppressor Housing
91
Servicing the Metrohm Suppressor Module (MSM)
91
Figure 24 Parts of the Metrohm Suppressor Module (MSM)
91
Peristaltic Pump
99
Notes on Operating the Peristaltic Pump
99
Servicing the Peristaltic Pump
99
Figure 25 Pump Tubing Connection - Replacing the Filter
100
Maintenance on the Metrohm CO
101
Replacing the CO 2 Adsorption Cartridge CW
101
Detector Maintenance
102
Rinsing the Sample Path
102
Separation Column
103
Separating Efficiency
103
Protecting the Separation Column
104
Storing the Separation Column
104
Regenerating the Separation Column
104
Troubleshooting
105
Technical Specifications
110
Reference Conditions
110
Instrument
110
Ambient Conditions
110
Housing
111
Weight
111
Leak Sensor
111
Column Oven
111
High-Pressure Pump
112
Injection Valve
113
Metrohm Suppressor Module (MSM)
113
Peristaltic Pump
113
Metrohm CO Suppressor (MCS)
113
Detector
114
Power Connection
114
Interfaces
114
Index
115
Other manuals for Metrohm 930 Compact IC Flex
Short Instructions
49 pages
Manual - Short Instructions
48 pages
4
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Metrohm 930 Compact IC Flex Specifications
General
Brand
Metrohm
Model
930 Compact IC Flex
Category
Laboratory Equipment
Language
English
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