Table of contents
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IV
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930 Compact IC Flex Oven/SeS/PP (2.930.2500)
4.10 Injection valve ..................................................................... 28
4.11 Metrohm Suppressor Module (MSM) ............................... 30
4.11.1 Inserting the rotors ................................................................ 31
4.11.2 Connecting the Metrohm Suppressor Module (MSM) ............. 33
4.12 Peristaltic pump .................................................................. 38
4.12.1 Installing the peristaltic pump ................................................ 38
4.12.2 Mode of operation for the peristaltic pump ........................... 42
4.13 Metrohm CO
2
Suppressor (MCS) ....................................... 43
4.13.1 General information on the MCS ........................................... 43
4.13.2 Connecting the MCS ............................................................. 43
4.13.3 Installing the adsorber cartridge ............................................. 45
4.14 Installing the conductivity detector .................................. 47
4.15 Installing the amperometric detector ............................... 48
4.16 Connecting the instrument to a computer ....................... 48
4.17 Connecting the instrument to the power grid ................. 49
4.18 Initial start-up ..................................................................... 50
4.19 Connecting and rinsing the guard column ....................... 52
4.20 Connecting and rinsing the separation column ............... 54
4.21 Conditioning ........................................................................ 57
5 Operation 59
6 Operation and maintenance 60
6.1 IC system ............................................................................. 60
6.1.1 Operation .............................................................................. 60
6.1.2 Care ...................................................................................... 60
6.1.3 Maintenance by Metrohm Service .......................................... 60
6.1.4 Shutting down and recommissioning ..................................... 61
6.2 Capillary connections ......................................................... 62
6.3 Servicing the door .............................................................. 62
6.4 Column oven – Replacing the capillaries .......................... 62
6.5 Handling the eluent ............................................................ 64
6.5.1 Manufacturing eluent ............................................................ 64
6.5.2 Changing the eluent .............................................................. 65
6.6 Notes on operating the high-pressure pump ................... 65
6.7 Servicing the high-pressure pump .................................... 66
6.8 Servicing the inline filter .................................................... 79
6.9 Servicing the pulsation absorber ...................................... 82
6.10 Injection valve ..................................................................... 82