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Metrohm Titrando 851 User Manual

Metrohm Titrando 851
63 pages
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851 Titrando
Manual
8.851.8004EN / 2020-02-11

Table of Contents

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Metrohm Titrando 851 Specifications

General IconGeneral
TypeTitrator
Model851
ManufacturerMetrohm
pH MeasurementYes
Conductivity MeasurementYes
Temperature MeasurementYes
Potentiometric MeasurementYes
Voltammetric MeasurementYes
Amperometric MeasurementYes
ConnectivityUSB, Ethernet
Communication InterfaceRS-232, USB
Measuring ResolutionpH: 0.001
Polarization CurrentVaries by method
Titration ModesVolumetric
Measuring InputspH, Temperature
Stirrer Connections2
Dosing DevicesBurettes, Pumps
Dosing SpeedAdjustable
DisplayTouchscreen
Power Supply100-240 V AC

Summary

Introduction

1.1 The Titrando System

Overview of the modular Titrando system and its peripheral devices.

1.2 Instrument Description

Details the characteristics and connectivity options of the 851 Titrando.

1.3 Titration Modes and Commands

Lists the supported titration modes, measuring modes, and dosing commands for the 851 Titrando.

1.4 Documentation Overview

Provides information on documentation content, warnings, and symbols used.

Safety Instructions

1.5.1 General Safety Notes

Outlines general safety precautions for operating the instrument.

1.5.2 Electrical Safety

Details electrical safety standards and warnings for qualified personnel.

1.5.3 Working with Liquids

Provides safety precautions and cautions when working with liquids, including leak checks.

1.5.4 Flammable Solvents and Chemicals

Lists safety measures for working with flammable solvents and chemicals.

Overview of the Instrument

Installation

3.1 Setting Up the Instrument

Covers packaging, checks, and selecting a suitable location for the instrument.

3.2 Connecting a Controller

Instructions for connecting the Touch Control or a computer for instrument operation.

3.3 Connecting MSB Devices

Information on connecting peripheral devices via the Metrohm Serial Bus (MSB).

3.4 Connecting USB Devices

Overview of connecting USB devices such as printers, keyboards, and readers.

3.5 Connecting to the Power Grid

Safety warnings and instructions for connecting the instrument to the power supply.

3.6 Titration Vessel Setup

Guidance on setting up the titration vessel for coulometric KF titration.

3.7 Connecting Sensors

Instructions for connecting generator electrodes, indicator electrodes, and temperature sensors.

Coulometric Titration

4.1 Principle of Coulometry

Explains the chemical principle and endpoint detection of coulometric Karl Fischer titration.

4.2 Working with Water Standards

Guidance on using certified water standards for instrument validation.

4.3 Sample Addition

Notes on sample addition for coulometric titration, including application bulletins.

4.4 Optimum Working Conditions

Discusses general conditions and specific parameters for optimal titration performance.

Operation and Maintenance

5.1 General Notes on Care

General considerations for instrument care to prevent disruptions and ensure longevity.

5.2 Generator Electrode

Details on generator electrodes, including types, reagents, and cleaning procedures.

Troubleshooting

6.1 General Troubleshooting

Guide to identifying and resolving common general issues with the 851 Titrando.

6.2 Karl Fischer Titration Issues

Specific troubleshooting steps for problems encountered during Karl Fischer titration.

Appendix

7.1 Remote Interface

Information about the Remote Box, its connectors, and pin assignments.

Technical Specifications

8.1 Measuring Interface

Details the galvanically isolated measuring interface specifications.

8.2 Power Connection

Technical details regarding power supply voltage, frequency, and consumption.

8.4 Interfaces

Overview of available interfaces: USB, Controller, and MSB.

Accessories

Downloading Accessories List

Step-by-step guide to downloading the accessories list from the Metrohm website.

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