VP-ITC MicroCalorimeter User’s Manual
Section 5: Instrument Maintenance
Section 5: Instrument Maintenance
The maintenance requirements of the VP-ITC are simple, but essential for quality experiments.
• The cells, injection and filling syringes must be kept clean.
• The Plunger Tips for the Pipette Injection Syringe must be replaced regularly to prevent
excess wear that would allow the titrant to leak from the syringe.
• Y-axis calibration is usually not a problem, but it is good practice to confirm the
calibration every 3 months.
• The Injection Syringe needle must be straight.
• The Plunger Screw must be kept straight.
• The syringe height (i.e. position of the stir paddle from the bottom of the cell) should be
approximately 3 mm. Once the syringe height adjustment is set, it is not usually a
problem, but this distance is custom for each instrument. This means that the user must
set the height position of newly purchased replacement syringes.
This section is arranged as follows:
............................................................................................64
5.1 Cleaning The Cells and Pipette ...........................................................................................................65
5.2 Replacing Pipette Plunger Tips ...........................................................................................................68
5.3 Y-axis Calibration ...............................................................................................................................72
5.4 Replacing Injection Syringes & Height Adjustment ...........................................................................74
64
To Next Page
Loading...