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Oxford Instruments Cryojet User Manual
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Operator’s Handbook
Cryojet
Issue 4
January 2001
File reference: CJ
250101.DOC
Part number UMC0001
Oxford Instruments
Superconductivity
Tubney Woods, Abingdon,
Oxon, OX13 5QX, England
Tel: +44 (0)1865 393 200
Fax: +44 (0)1865 393 333
E-mail:superconductivity@oxinst.co.uk
www.oxford
-instrume
nts.com
2
Table of Contents
Table of Contents
2
Quick User Guide
4
Description of the System
7
Sample Flow Unit
8
Shield Unit
8
Stand
8
Storage Dewar
8
Controller
8
Unpacking and Preparation
9
Unpacking the System
9
Preparing the System for Operation
9
Controller
13
Control of Flow Rates
13
Control of Jet Temperature
13
Default Conditions on Start-Up
14
Low Nitrogen Level Cut-Out
14
Operation
15
Suggested Operating Conditions
15
Alignment of Nozzle and Use of Alignment Tip
15
Filling the Dewar
16
Using the Dipstick to Measure the Level of Liquid Nitrogen
16
Warming up the System
17
Evacuating the Outer Vacuum Chamber (OVC)
18
Calibration of Sample Temperature
19
Stability
19
Icing of Crystal Support and Goniometer
19
Control from a Computer
20
RS232 Connection Hardware
20
GPIB (IEEE-488) Connection Hardware
20
Control Using the Oxford Instruments Objectbench Software Package
21
Installation of Cryojet Driver in Objectbench
21
Setting up the Cryojet Driver
22
Control of the Cryojet
22
Restoring Standard Calibration Parameters
23
Setting of P, I and D Control Terms
24
Liquid Nitrogen Autofill System
26
Setting up the Autofill System
27
The Solenoid Valve
28
Fault Finding
29
Wiring Information
32
Shield Unit
32
4
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Oxford Instruments Cryojet Specifications
General
Brand
Oxford Instruments
Model
Cryojet
Category
Laboratory Equipment
Language
English
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