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PerkinElmer PINAACLE 900 Series User Manual

PerkinElmer PINAACLE 900 Series
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PINAACLE 900 SERIES
Customer Hardware and
Service Guide
ATOMIC SPECTROSCOPY

Table of Contents

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PerkinElmer PINAACLE 900 Series Specifications

General IconGeneral
Wavelength Range190 - 900 nm
CategoryAtomic Absorption Spectrometer
ModelPINAACLE 900 Series
TypeLaboratory Equipment
Optical SystemDouble Beam
AtomizationFlame, Graphite Furnace
Flame TypesAir-Acetylene, Nitrous Oxide-Acetylene
Correction SystemDeuterium Background Correction
Bandwidth0.1, 0.2, 0.5, 1.0, 2.0 nm

Summary

Safety Practices

General Safety Precautions

Key safety information and general precautions for operating the instrument.

Environmental and Electrical Safety

Lab conditions for instrument operation and electrical safety practices to prevent hazards.

Hazardous Materials and Disposal

Precautions for safe handling of chemicals, gases, and proper waste disposal procedures.

Specific Hazards (UV, Magnetic, Temperature)

Awareness and precautions for UV radiation, magnetic fields, and high temperatures.

Preparing Your Laboratory

Laboratory Environment and Space

Requirements for installation location, temperature, humidity, and physical space.

Power and Ventilation Requirements

Specifications for line power, noise, conditioners, UPS, and fume ventilation.

Gas System Setup and Safety

Requirements for gas supplies, connections, cylinders, and safety.

Gas Specifications

Purity and pressure specifications for furnace and flame gases.

System Description

PinAAcle 900 Series System Overview

Introduction to the spectrometer system, concept, features, and components.

System Components and Control

Major components, control methods, and accessories of the PinAAcle 900 system.

Gas, Cooling, and Burner Systems

Description of burner assembly, gas connections, and cooling system details.

Technical Specifications

Detailed specifications for atomizers, background correction, and data handling.

Installation

Unpacking and Initial Setup

Safely unpacking the instrument, inspecting shipment, and preparing the site.

Connecting System Components

Instructions for connecting gas supplies, electrical power, computer, and printer.

Installing System Modules

Procedures for installing cooling, drain systems, nebulizer, autosampler, and sample capillary.

Moving and Reinstalling the Spectrometer

Procedures for safely relocating and reinstalling the instrument.

Preparing the System

System Startup and Lamp Installation

Procedures for powering on the system and installing lamps.

Flame Analysis Preparation

Configuring the system for flame atomization, including burner setup and safety checks.

Furnace Analysis Preparation

Configuring the system for furnace atomization, including cover locking and analysis setup.

Maintenance

General and Instrument Maintenance

General procedures, cleaning, periodic checks, and safety guidelines.

Burner System Maintenance

Procedures for burner head, drain system, and O-ring maintenance.

Spectrometer and Component Maintenance

Changing filters, fuses, and servicing optical components.

Graphite Furnace Maintenance

Procedures for maintaining graphite tubes, contacts, windows, and furnace components.

Autosampler System Care and Parts

Routine autosampler care and ordering replacement parts.

Troubleshooting

Spectrometer and Computer Issues

Solutions for problems with spectrometer, lamps, and computer communication.

Burner System Troubleshooting

Troubleshooting flame ignition, stability, and burner head issues.

Furnace and Autosampler Problems

Solutions for furnace operation, autosampler functionality, and graphite tube issues.

Analysis Technique Specific Issues

Troubleshooting for flame, furnace, and flow injection techniques, including sensitivity and signal problems.

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