Ionics Instruments 2004 Page 9-9 DLM 30007-08 Rev. A
5. From the SET DISPLAY MODE menu, use the arrows ( or ) to
select TC DISPLAY and press ENTER to save this setting. The
program will prompt for confirmation. Press ENTER and the
OUTPUTS menu will appear. Press CLEAR once to return to the
SETUP menu.
6. Ensure that the analyzer is in grab-sample mode. From the SETUP
menu, select SAMPLE MODE and press ENTER. Using the
arrows
( or ), scroll to GRAB SAMPLING and press ENTER. Press
CLEAR twice to return to the MAIN menu.
7. Use the
arrows ( or ) to scroll to START TOC and press ENTER.
The GRAB SAMPLE menu is displayed.
8. Use the
arrows ( or ) to scroll to SETUP and press ENTER. The
GRAB SAMPLE SETUP menu is displayed.
9. Scroll to REPETITIONS and press ENTER.
10. Set the number of Repetitions to 10. Press ENTER to save the
number. Press CLEAR to return to the GRAB SAMPLING SETUP
menu.
11. Use the
arrows ( or ) to scroll to REJECTIONS and press ENTER.
12. Set the number of Rejections to 7. Press ENTER to save the
number. Press CLEAR to return to the GRAB SAMPLING SETUP
menu.
13. Use the
arrows ( or ) to scroll to REAGENTS and press ENTER.
14. Select the ACID FLOW RATE option and enter 0.75 µL/min. Press
ENTER to save the number, and press ENTER again to confirm it.
Press CLEAR to return to the REAGENTS menu. Use the
arrows (
or ) to scroll to OXIDIZER FLOW RATE, and enter 0.01 µL/min.
Press ENTER to save the number, and press ENTER again to
confirm it. Press CLEAR twice to return to the GRAB SAMPLING
SETUP menu.
15. Use the
arrows ( or ) to scroll to STATISTICS, and press ENTER.
Use the
arrows ( or ) to toggle to the AVE/CV option and press
ENTER to save the setting. Press CLEAR twice to return to the
GRAB SAMPLING MODE menu.
16. Place the 1/16"-OD INLET Teflon tube in the flask or vial of Ionics
Instruments-prepared standard labeled "Reagent Water Blank".
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