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Sievers TOC 800 User Manual

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800 Series Total Organic Carbon Analyzer
Operation and Maintenance Manual
Minimum Firmware Version:
TOC Firmware Versions 3.52 (CAS) with or without
DataPro Autosampler Software, or
TOC Firmware Versions 3.62 (CAS) with
DataGuard and with or without DataPro Autosampler Software, or
TOC Firmware Versions 3.15 (CMS), or
TOC Firmware Versions 2.12 (CTB) Turbo, or
TOC Firmware Version 2.11 (CBI)
Instrument Business Group
6060 Spine Road
Boulder, CO 80301 USA
phone 800.255.6964 303.444.2009 fax 303.444.9543 DLM 30007-08 Rev. A
www.IonicsInstruments.com Printed in USA 2004

Table of Contents

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Sievers TOC 800 Specifications

General IconGeneral
Power Supply100-240 VAC, 50/60 Hz
TypeTotal Organic Carbon Analyzer
TechnologyUV-Persulfate Oxidation
Data StorageInternal Memory
Data OutputAnalog, digital
DisplayTouch screen
Sample TypeLiquid

Summary

Identification Records

Default Administrator Password

Specifies the default password for administrator access.

Instrument Serial Number

Field to record the unique serial number of the instrument.

Installation Date

Field to record the date of instrument receipt and installation.

Revision History

Revision Details

Lists manual revisions, dates, and brief descriptions of changes.

Trademarks and Patents

Trademarks

Lists registered trademarks and their owners.

Patents

Mentions patents covering the analyzer.

Confidentiality

Information Disclosure

Outlines conditions for proprietary and confidential information.

Standard Limited Warranty

Warranty Term

Specifies the duration and conditions of the limited warranty.

Warranty Service Procedures

Details procedures for obtaining warranty service and support.

Parts and Consumables Warranty

Covers warranty terms for replacement parts and consumables.

Shipping and Warranty Voiding Conditions

Outlines shipping requirements and conditions that void the warranty.

Limitation of Remedies and Liability

Defines customer remedies and limits the manufacturer's liability.

Declaration of Conformity

Compliance Statement

Declares conformity with relevant council directives and standards.

Introduction to Sievers 800 TOC Analyzer

Analyzer Overview and Principle

General description of the analyzer and its measurement principle.

Analyzer Capabilities and Specifications

Details sample range, maintenance, calibration stability, and operation.

Safety Warnings and Precautions

Lists critical safety precautions and warnings for operation and maintenance.

System Specifications

Detection and Performance Specifications

Lists detection limit, precision, accuracy, interferences, and linear range.

Environmental and Physical Specifications

Details sample/ambient temperature, altitude, size, and weight.

Power Requirements

Specifies power voltage, frequency, and wattage for different models.

System Description

Analyzer Components Overview

Lists the nine main components of the Sievers 800 TOC Analyzer.

Analyzer Schematic and Fluidics

Diagram and description of sample inlet, reagents, sensors, and DI water loop.

Control and Data Systems

Microprocessor, data storage, and output interfaces.

Major Accessories and Configurations

Details optional modules like IC Removal, Autosampler, Multistream, Turbo, Flow Switch.

Front Panel Interface

Explanation of the front panel display and control buttons.

Installation Procedures

Site Preparation and Initial Setup

Unpacking, inspection, equipment, site, power, environment, sample port, and plumbing.

Electrical and Reagent Installation

Wiring outputs, installing reagent cartridges, and setting dates.

Operational Mode and Flow Rate Configuration

Selecting sample mode, setting flow rates, and configuring presets.

System Configuration and Maintenance Setup

Setting passwords, printer, print intervals, constants, and reagent flush.

Analog and Digital Outputs

Baud Rate Configuration

Setting the communication speed for the RS-232 port.

RS-232 Data Output Configuration

Enabling and configuring data transmission via RS-232.

Serial Commands

How to send commands to the analyzer via RS-232.

Alarms Configuration

Setting trigger levels and types for analyzer alarms.

Analog Outputs Configuration

Setting the range and type (TOC, TC, IC) for analog outputs.

Display Mode Selection

Changing the measurement displayed (TOC, IC, TC) on the screen.

Warning 42 Message Configuration

Configuring the warning for low TOC/IC ratio.

Operation and Display Menus

Menu Map Overview

Visual guide to the analyzer's menu structure.

Main Menu Options

Description of the six primary options accessible from the MAIN menu.

Power-Up and Initialization

Steps for starting the analyzer and its initial sequence.

Measurement Display

How results are shown on the main measurement screen.

RunTime Menu Operations

Menu accessible during analysis for monitoring and control.

History Data Review

Viewing past TOC, TC, and IC measurement data.

Error and Warning Message Handling

Accessing and interpreting error and warning messages.

Stopping TOC Measurements

Procedure to safely stop the analyzer's measurement cycle.

Consumables Status Check

Viewing the status of reagents, lamps, and tubing.

UV Lamp Status

Checking the operational status and remaining life of the UV lamp.

Reagent Status Monitoring

Monitoring the status of acid and oxidizer reagent reservoirs.

Fatal Error Display and Handling

Handling and interpreting fatal error messages that halt operation.

Analyzer Power Down Procedures

Safe procedures for powering down the instrument.

Grab Sample Measurement Procedures

How to perform TOC analysis on discrete samples.

Sample Mode Configuration

Steps to configure the analyzer for grab or on-line sampling.

Grab Sample Parameter Setup

Configuring repetitions, rejections, and printout settings for grab samples.

Password Management Procedures

Steps to change the analyzer's password for access control.

Disabling Password Protection

How to turn off password prompts for analyzer access.

Service Menu Operations

Accessing diagnostic tests for analyzer subsystems.

DataGuard Operation

DataGuard Feature Overview

Explains DataGuard's role in 21 CFR Part 11 compliance.

DataGuard Menu Map

Visual representation of the DataGuard menu structure.

DataGuard Main and RunTime Menus

Primary menu options and RunTime menu with DataGuard enabled.

Stop TOC and Setup Menus with DataGuard

Stop TOC and Setup menu options with DataGuard enabled.

Admin Menu for User Management

Tools for managing user passwords and logout timers.

Password and Login Timeout Management

Changing passwords and setting the idle period before logout.

Audit Trail Management

Viewing, printing, exporting, and resetting the audit trail.

Maintenance Procedures

Replacement and Maintenance Schedule

Recommended intervals for replacing reagents, lamps, filters, and tubing.

RAM Card and Battery Information

Details on RAM card sizes, capacities, and battery life.

Replacing In-line Filter

Step-by-step guide for replacing the sample inlet line filter.

Replacing Reagents

Instructions for safely replacing acid and oxidizer reagent cartridges.

Replacing UV Lamp

Procedure for changing the UV lamp to maintain performance.

Replacing Pump Tubing

Guide for replacing sample pump tubing to ensure proper flow rates.

Setting Installation Dates for Replaced Components

Entering dates after replacement in the CONSUMABLES menu.

DI Water Reservoir Check and Refill

How to check and replenish the deionized water supply.

Analyzer Cleaning Procedures

Instructions for cleaning the external surfaces of the analyzer.

Calibration Procedures

Calibration Overview and Standards

Explains calibration importance, standards, and procedures.

TC Zero Offset Calibration

Procedure to adjust the TC zero offset for low TOC water analysis.

TC Calibration Constant Adjustment

Steps to calibrate the TC channel constant using standards.

IC Calibration Constant Adjustment

Steps to calibrate the IC channel constant using standards.

TC and IC Calibration Verification

How to verify the accuracy of the calibrated TC and IC channels.

Troubleshooting

Error Management and Diagnostics

Checking error stack, understanding messages, printing logs, and running diagnostics.

Flow and Reagent System Issues

Troubleshooting no power, no flow, pH, oxidizer flow, DI reservoir, and gas bubbles.

Measurement Accuracy and TOC Readings

Diagnosing negative/zero TOC, IC impact, and TC zero offset adjustments.

Analyzer Logistics and Preparation for Shipment

Procedures for returning the analyzer and preparing it for shipment.

RAM Cards, Card Reader, and RAMReader Software

Card Reader Hardware and Software Installation

Steps for installing a RAM card reader and its software.

RAM Card Handling and Installation

Procedures for safely removing, inserting, and protecting the RAM card.

RAM Card Battery Maintenance

How to change the battery that maintains data on the RAM card.

Downloading RAM Card Data

Using the GD command to transfer data from RAM card to PC.

Appendix A – 810/810AS Analyzer Operating Frequency

Selecting Operating Frequency

How to set the analyzer's operating frequency (50/60 Hz).

Calibration Frequency Settings

Adjusting calibration constants based on operating frequency.

Appendix B – 820/820AS Analyzer Operating Frequency

Checking Operating Frequency

Verifying the factory-configured operating frequency setting.

CE Mark Compliance Requirements

Required additional equipment for CE mark compliance.

Printer Cable Specifications

Specifications for printer cables to meet CE mark standards.

Appendix C - Turbo TOC Analyzers

Turbo Mode Introduction

Overview of the Turbo mode for rapid response analysis.

Setting Turbo Sampling Mode

How to activate the Turbo sampling mode on the analyzer.

Setting Turbo Reagent Flow Rates

Configuring reagent flow rates specific to Turbo mode.

Turbo Mode Alarm and Calibration Settings

Alarms and calibration notes for Turbo mode operation.

Turbo Mode TC Zero Offset and Channel Calibration

TC zero offset and channel calibration procedures for Turbo mode.

Turbo Mode Accuracy Specifications

Performance specifications for the analyzer in Turbo mode.

Appendix D – Binary Input Module – Flow Switch

Flow Switch Warnings and Installation

Safety and mechanical installation warnings and steps for the flow switch.

Firmware and EEPROM Chip Replacement

Instructions for printing constants and replacing the EEPROM chip.

Software Configuration for Binary Inputs

Configuring binary inputs for pausing operation.

Appendix E – Calibration Standard Preparation

Equipment and Supplies for Standards

Lists necessary items for preparing calibration standards on-site.

Preparing TC Calibration Standard

Detailed steps for preparing TC calibration standards.

Preparing IC Calibration Standard

Detailed steps for preparing IC calibration standards.

Appendix F – Consumables and Accessories

Consumables List

Lists consumable items like lamps, tubing, filters, and reagents.

Calibration Standards Sets and Vials

Catalog numbers and descriptions for calibration standards.

Firmware/Software Part Numbers

Part numbers for software upgrades and firmware.

Optional Accessories List

Lists optional accessories like flow switches, autosamplers, etc.

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