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ACCQPrep HP125
Teledyne ACCQPrep HP125 User Manual
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A
CCQPr
ep HP125
Installation and Operation Guide
60-5233-81
2
Copyright © 2017 T
eledyne T
echnologies
Incorporated. All rights reserved.
Rev
. C
, J
anuary 2019
2
Table of Contents
Default Chapter
7
Table of Contents
7
Section 1 Introduction
11
Overview
11
Product Overview
11
Operating Overview
13
Multiple Control Possibilities
13
File Storage
13
Safety Components
13
Specification
14
Section 2 Installation
17
Accqprep Installation
17
Setting up the System
17
Pump Installation
18
Solvent Line Installation
20
Fluid Line Installation
21
Accqprep Equipped with Optional ELSD
22
Priming Steps
24
Installing the Manual Injection Port
25
Installing the Autosampler
26
Establishing the Fluid Connections
32
Column Installation
35
Column Mounting
35
Column Configuration
37
Column Select Valve (Optional)
37
Installation Troubleshooting
38
Section 3 Configuration
41
Configuration of the Accqprep
41
Network Configuration
42
User Preferences
42
Prep HPLC
43
Define a Column
44
Delete a Column
44
Creating Other Methods
45
Creating Focused Gradients
46
Section 4 Operation
47
Introduction
47
Method Selection
47
Starting a Separation
48
Separation with an Autoinjector
48
Autoinjection Operating Steps
51
Separation Using an Autosampler Module
53
Using the Queue Tab
53
Autosampler Injection Techniques
55
Fraction Collection with the Autosampler
58
Operation Troubleshooting
59
Section 5 Peaktrak
65
Overview
65
Peaktrak Window Elements
65
Method File
65
Run File
66
Peaktrak Menu Options
66
File
68
Method Editor
68
Tools
70
Help
71
Peaktrak Windows
72
Method Editor
76
Column Data
82
Files
82
Set Data Path
83
MS Method Development
84
MS Manual Control
85
Ionization Settings
86
Manual Control
88
Configuration
88
Set Administrator Password
89
Examples of Peaktrak Actions
90
Editing a Method
90
Alternative Ways to Create Method Files
94
Defining a Gradient
94
Real-Time Gradient Editing
95
Bypassing the Injection Loop
95
Monitoring the Purity Measure
96
Viewing Runs
96
Manual Control of the Accqprep
99
Section 6 Maintenance
101
Introduction
101
Cleaning
101
Collection Rack and Tray Cleaning
101
System Standby and Shut down
101
Tubing Inspection
102
Preventive Maintenance
103
Flow Cell Cleaning
104
Post Separation
104
Quick Cleaning When Recommended
105
Monthly Flow Cell Cleaning
106
Accqprep HP125 Maintenance
107
Injection Valve Rotor Replacement
107
Pump Seal Replacement
109
Seal Conditioning
114
Check Valve Replacement
114
Autosampler Maintenance
118
ELSD Maintenance
119
Cleaning the ELSD Detector
119
Purion Maintenance
122
ESI and APCI Removal from Purion S and Purion L
122
ESI and APCI Replacement Purion S and Purion L
122
Cleaning the Ionization Source Capillary
122
Replacement of Ion Source Housing
123
Overpressure Error
123
Check Valve Cleaning
123
Replacing Check Valves
124
Purion Cone Cleaning
124
Capillary Inlet Cone Removal
125
Capillary Inlet Cone Cleaning
125
Capillary Inlet Cone Installation
126
Purion Troubleshooting
126
Appendix A
129
Diagrams for the Autosampler and Accqprep
129
4
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Teledyne ACCQPrep HP125 Specifications
General
Brand
Teledyne
Model
ACCQPrep HP125
Category
Laboratory Equipment
Language
English
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