What to do if the Teledyne Laboratory Equipment PurIon vacuum level is too low?
The Pirani pressure must be below 5.5E-3 mbar for the PurIon turbo pump to operate. This issue usually occurs if the roughing pump isn't turned on, especially after cleaning the capillary or changing the pump oil. Ensure the roughing pump is on.
What to do if no ion source is detected on Teledyne Laboratory Equipment PurIon?
The PurIon has reported that the ion source high voltage cable is not properly plugged into its socket. This is the cable with the round connector, located to the right and behind the ion source. This usually happens when changing or cleaning probes. Ensure the ion source high voltage cable is properly plugged into its socket.
Why Teledyne Laboratory Equipment PurIon has been shut down?
This message appears after the PurIon has been successfully shut down using the SHUTDOWN command. It's a reminder that an Rf reboot is needed for the PurIon to be enabled again by the Rf.
What to do if the ionization probe isn’t fully seated into the ion source housing of Teledyne Laboratory Equipment?
On PurIon systems (excluding PurIon S or PurIon L), if the ionization probe isn’t seated properly, loosen the thumbscrew on the front of the ion source housing, push down on the probe, and then tighten the thumbscrew.
What does error 310 mean for Teledyne Laboratory Equipment PurIon?
This error message is displayed if a plug is detected during a separation.
What does error 316 mean for Teledyne Laboratory Equipment PurIon?
This error occurs if the tubing is plugged while the method development screen is in use.
What causes the Teledyne Laboratory Equipment fluid interface pressure to be too low?
This could be due to lack of carrier fluid, loss of pump prime, or leakage.
Why Teledyne Laboratory Equipment PurIon temperatures are stabilizing?
The PurIon has several areas with heaters. The software uses a timer to allow temperatures to reach operating conditions. If the heaters aren't within an acceptable range after this time (default is 300 seconds after entering operate), a separate error is thrown. During standby, most heaters are OFF, except the inlet capillary, which is set to 50 C°.
General| Brand | Teledyne |
|---|---|
| Model | CombiFlash Rf |
| Category | Laboratory Equipment |
| Language | English |
Provides information on safety, unpacking, installation, certification, and warranty.
Describes the Teledyne Isco CombiFlash Rf chromatography system's features and applications.
Details various CombiFlash system configurations like Rf 150, Rf+, Lumen, PurIon, EZ Prep, and 4x.
Lists physical, electrical, and performance specifications for Rf 150 and Rf+ systems.
Identifies front, side, and back panel controls and features of the CombiFlash Rf system.
Provides general warnings about hazardous practices, material classification, and ventilation.
Provides contact information for technical assistance from Teledyne Isco.
Instructions for unpacking the CombiFlash Rf+, Rf+ Lumen, and optional 4x module.
Details connecting the system to mains power using the supplied IEC cord.
Explains connecting solvent lines, including warnings about static discharge and tubing.
Explains connecting waste lines to diverter and inject valve outlets, with safety warnings.
Covers pre-assembled EZ Prep plumbing, removing clamps, and placing lines in reservoirs.
Guides testing and routing drain tubes for fraction collector and top shelf drains.
Lists available tube racks and instructions for loading tubes into racks.
Details turning the system on, monitoring startup, and checking for operation readiness.
Guides system configuration via the PeakTrak menu, covering various settings.
Explains managing solvents, adding names, and enabling solvent level sensing.
Explains the vapor sensor, limit settings, and troubleshooting alarms.
Guides priming solvent lines using the Auto Prime menu command.
Recommends system verification using pre-packaged test kits.
Instructions for unpacking the CombiFlash Rf 150 system.
Details connecting the CombiFlash Rf 150 to mains power using the IEC power cord.
Explains connecting solvent lines to the Rf 150 system's two solvent inlet ports.
Explains connecting waste lines to the Diverter Valve Waste port on the Rf 150 system.
Details turning the Rf 150 system on, monitoring startup, and checking for operation readiness.
Guides Rf 150 system configuration via the PeakTrak menu.
Explains managing solvents for the Rf 150 system, adding names.
Explains the vapor sensor and limit settings for the Rf 150 system.
Guides priming solvent lines for the Rf 150 system using Auto Prime.
Instructions for unpacking the CombiFlash Rf 4x module.
Details connecting the CombiFlash Rf 4x module to mains power.
Explains connecting solvent lines to the Rf 4x module's ports.
Explains connecting waste lines to the six liquid waste ports on the Rf 4x module.
Guides removing shipping hardware from the injection valve assemblies.
Guides priming solvent lines for the Rf 4x module using Manual Control.
Discusses methods for sample preparation: liquid injection, solid cartridges, and pre-loading.
Details preparing empty solid sample cartridges and mixing media with sample.
Provides instructions for loading a RediSep Rf column, including warnings and column selection.
Guides starting a run using default methods, including sample name and loading type selection.
Allows system operation monitoring and gradient parameter modification during a run.
Explains Play, Pause, and Stop buttons for controlling the run.
Explains bypassing the solid load cartridge to relieve back pressure, with CAUTION.
Covers EZ Prep operation, including column mounting and sample preparation.
Guides mounting HPLC columns and guard columns on the EZ Prep system.
Details HPLC sample preparation, injection loop volume, and solvent considerations.
Guides starting HPLC separations on the EZ Prep system, selecting columns and loading techniques.
Provides an overview of the PeakTrak control software and its interface.
Explains the role of Method files in controlling runs and their basic/advanced settings.
Lists PeakTrak menu options including File, Method Editor, MS, Tools, and Help.
Explains the Method Editor window, button bar, and sections.
Details MS options for PurIon systems, including method development and manual control.
Lists tools options: Edit Defaults, Configuration, Set Admin Password, User Management.
Describes various PeakTrak windows like Main Window, Method Editor, and Gradient Optimizer.
Explains the Method Editor window layout and its various settings.
Guides generating gradients from TLC data using the Gradient Optimizer.
Allows tailoring system operation by editing basic and advanced method settings.
Explains bypassing the solid load cartridge to relieve back pressure, with CAUTION.
Guides configuring the system for corporate network use, including IP address settings.
Lists PC recommendations for accessing a networked CombiFlash Rf system.
Explains configuring the system to print to a network printer.
Details instructions for direct connection setup for Windows 7, Vista, XP, and 2000.
Explains setting up a USB printer for direct printing from the CombiFlash Rf system.
Explains placing the system in Standby to conserve power and safe shutdown procedures.
Outlines preventive maintenance schedules: As Needed, Every Run, Monthly, Annually.
Guides cleaning exterior surfaces using detergent, water, and isopropyl alcohol.
Guides monthly inspection of tubing, fittings, and drains for damage or leaks.
Explains post-separation flush and quick cleaning procedures for the flow cell.
Covers maintenance for PurIon systems, including probe removal and cleaning.
Guides checking line cord and fuses for electrical issues and touch panel display problems.
Lists PurIon error codes and their corresponding solutions for troubleshooting.
Lists general troubleshooting steps for common system errors.
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