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Thermo Scientific Nicolet FT-IR User Manual

Thermo Scientific Nicolet FT-IR
31 pages
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Thermo Scientific Nicolet FT-IR Specifications

General IconGeneral
Spectral Range7, 800 to 350 cm-1
Detector TypeDTGS detector
BeamsplitterKBr
SourceIR Source
Wavenumber Accuracy0.01 cm-1
Interferometer TypeDynaScan™ interferometer
SoftwareOmnic™ software suite
InterferometerDynaScan™ interferometer with dynamic alignment

Summary

Introduction

TGA-IR Module Overview

Explains the features and components of the TGA-IR Module and experiment procedures.

Safety Information

Highlights the importance of reading safety guides and following precautions for safe operation.

Questions and Concerns

Contacting Support and Assistance

Provides contact information for emergency procedures and operational assistance.

Manual Conventions

Understanding Manual Symbols and Warnings

Explains symbols like Note, Important, Caution, Warning, and Danger for user guidance.

Safety Precautions

High Temperature and Burn Hazard Warning

Warns about high temperatures of the gas cell and transfer line and associated burn hazards.

Electrical Shock and Fire Hazard Warning

Warns against contact with liquids and accessing internal components to prevent shock and fire.

Module Components

Overview of TGA-IR Module Components

Illustrations and descriptions of the TGA-IR Module and its internal components.

The Front Panel

Front Panel Indicator Lights

Explains the function of the four indicator lights on the front panel of the TGA-IR Module.

The Rear Panel

Rear Panel Connectors and Controls

Details the components and their functions on the rear panel of the TGA-IR Module.

Using the TGA-IR Module

Principles of Operation

Explains how Thermogravimetric Analysis (TGA) works and its combination with FT-IR.

Setting Up the Module

Outlines the procedures for setting up the TGA-IR Module for data collection.

Connecting the Purge Line

Procedure for connecting the purge gas supply to the TGA-IR Module.

Connecting the Transfer and Exhaust Gas Lines

Procedure for connecting the transfer and exhaust gas lines for TGA-IR experiments.

Verifying the Installation

Steps to verify the successful installation of the TGA-IR Module.

Setting the Temperature

Instructions on setting the temperature for the TGA-IR Module using OMNIC software.

Using the Remote Start Option

Details on how to use the remote start option with a TGA furnace.

Cooling the Detector

Procedure for cooling the MCT detector with liquid nitrogen.

Operating Tips

Tips for obtaining the best results when using the TGA-IR Module.

Maintenance

Checking and Replacing Fuses

Procedure for checking and replacing fuses in the TGA-IR Module.

Fuse Replacement Specifications

Specifications for replacement fuses for different AC voltage systems.

Troubleshooting

Addressing Low Infrared Throughput

Identifies causes and solutions for low infrared throughput issues.

Specifications

Electrical Specifications

Details maximum power consumption, AC voltage, and current ratings for the module.

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