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Varian Micro-GC 490-GC User Manual

Varian Micro-GC 490-GC
83 pages
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Varian BV
Herculesweg 8
4330 EA Middelburg
The Netherlands
Micro-GC
User Manual
North/South America
2700 Mitchell Drive
Walnut Creek
94598 California, USA
Tel: ++(1)9259392400
Fax: ++(1)9259452360 or
++(1)9259452344
Europe
P.O. Box 8033
4330 EA Middelburg
The Netherlands
Tel: ++(31)118671000
Fax: ++(31)118623193
Australia/East Asia
679 Springvale Road
Mulgrave, Victoria 3171
Australia
Tel: ++(61)395607133
Fax: ++(61)395607950
© 2009 Varian, Inc. All Rights Reserved Printed in the Netherlands CP501265490 Rev:1 November 2009

Table of Contents

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Varian Micro-GC 490-GC Specifications

General IconGeneral
BrandVarian
ModelMicro-GC 490-GC
CategoryLaboratory Equipment
LanguageEnglish

Summary

Varian Analytical Instrument Warranty

Hardware Products Warranty

Warranty terms for physical analytical instruments and their components.

Software Products Warranty

Warranty conditions for software provided under license agreements.

Warranty Remedies

Describes exclusive remedies for hardware warranty claims, including repair or replacement.

Warranty Limitations

Outlines exclusions from warranty coverage, including consumables and misuse.

Remedy and Liability Limitations

States provided remedies are exclusive and limits liability for damages.

Safety Information

Information and Compliance

Details CE specifications, safety requirements, and regulatory compliance.

Operating Instructions Overview

Guidance on using the manual and understanding safety precautions.

Warning Symbols and Descriptions

Explains common warning symbols (caution, danger, burn hazard) and their meanings.

General Safety Precautions

Practices for safe operation, including handling gases and waste.

Cautions and Warnings

Specific safety advice, including electrical hazards and proper cord usage.

Spare Parts and Service Availability

Information on obtaining spare parts and available post-warranty service options.

Introduction to Micro-GC

Product Overview and Features

Welcome to the Varian Micro-GC, highlighting EGC technology and its benefits.

Preparing for Installation

Gas Supply and Sample Requirements

Specifications for carrier gas quality and sample preparation.

Gas Samples Handling

Guidelines for preparing and introducing gaseous samples to the instrument.

Micro-GC Installation

Inspection and Unpacking Procedures

Steps for inspecting the instrument upon arrival and unpacking it safely.

Packing List

A detailed list of all items included in the Micro-GC package.

Accessories

List of optional accessories available for the Micro-GC system.

Installation Procedures

Gas Regulators and Pressure Setup

Instructions for installing and setting gas regulators for optimal pressure.

Carrier Gas Connection

Details on connecting the carrier gas supply to the instrument.

Data Handling Peripherals Connection

Connecting workstations and other data acquisition devices.

Sample Connection

How to connect the sample inlet to the instrument.

Heated Sample Line Connection

Guide for connecting heated sample lines for specific analyses.

Connecting to Power and Initial Power-On

Steps for electrical hookup and turning the instrument on for the first time.

Factory Default States and Settings

Information on the instrument's default configuration upon shipment.

Instrument Overview

Front View Description

Identifies and explains the indicators and controls on the front panel.

Back View Description

Details the connectors, vents, and ports located on the rear of the instrument.

Inside View Description

Shows internal connectors and ports accessible after opening the cover.

Carrier Gas Connection Details

Specifics on connecting carrier gas, including tubing and filter recommendations.

Sample Handling

Sample Gas Preparation and Filtering

Advice on preparing gaseous samples and using external filters.

Heated Injector Systems Setup

Configuration for analyzing samples using heated injectors.

Heated Sample Line

Connecting a Heated Sample Line

Procedure for connecting the heated sample line, including safety warnings.

Power and Shutdown Procedures

Power Requirements and Safety

Details on the instrument's power needs and safety during operation.

Shut Down Procedure

Steps for safely powering down the instrument for short or long periods.

Long Storage Recovery Procedure

Steps to follow when recovering the instrument after extended storage.

Initial Operation and Run

Setting Up Test Methods

Guide to entering method parameters and sending them to the instrument.

Injecting the Sample

How to connect and introduce samples for analysis.

Column Performance Examples

CP-SIL 5 CB 6m Unheated Chromatogram

Chromatogram and parameters for the CP-SIL 5 CB 6m unheated column.

CP-SIL 5 CB 4m Heated Chromatogram

Chromatogram and parameters for the CP-SIL 5 CB 4m heated column.

CP-SIL 5 CB 8m Heated Chromatogram

Chromatogram and parameters for the CP-SIL 5 CB 8m heated column.

CP SIL13CB TBM 12m Heated Chromatogram

Chromatogram and parameters for the CP SIL13CB TBM 12m heated column.

HayeSep 40cm Heated Chromatogram

Chromatogram and parameters for the HayeSep 40cm heated column.

Molsieve 5Å 20m Unheated Chromatogram

Chromatogram and parameters for the Molsieve 5Å 20m unheated column.

Molsieve Column Conditioning Procedure

Method to restore Molsieve column efficiency by heating and purging.

PPQ 10m Heated Chromatogram

Chromatogram and parameters for the PPQ 10m heated column.

Reference Information

Instrument Description Overview

General description of the Micro-GC's components and modules.

Carrier Gas Specifications

Details on carrier gas types, purity, and pressure requirements.

Micro Electronic Gas Control (EGC)

Explanation of the EGC system for precise pressure and flow control.

Column Configurations and Applications

Overview of different column types and their suitability for various analyses.

Detector Types (TCD and DMD)

Description of the Thermal Conductivity Detector (TCD) and DMD.

In/Outputs and Ports

Information on the instrument's input and output connection ports.

External Digital I/O

Details on digital input and output connections for external devices.

Communication Ports (COM)

Overview of serial (RS232/RS485) and Ethernet communication ports.

External Analog I/O

Details on external analog input and output connections.

Shipping Instructions

Guidelines for preparing the instrument for return shipment to the factory.

Cleaning Instructions

Recommendations for safely cleaning the exterior of the Micro-GC.

Disposal Instructions

Information on proper disposal of the instrument according to regulations.

Differential Mobility Detector (DMD)

General Information and Safety

Introduction to the DMD, including safety precautions related to its radioactive source.

General Functionality

Explanation of how the DMD operates using ion mobility spectroscopy principles.

Micro-GC DMD Channel Specifics

Location and recognition of the DMD channel within the Micro-GC system.

General Operation of DMD

How the DMD is managed by workstation software and its specific settings.

Tuning the DMD

Procedure for optimizing DMD performance through tuning runs.

Protocols and Networking

Protocol Types Overview

Lists various communication protocols used in networking.

Internet Protocol Suite Details

Information on TCP/IP, its development, and related services.

IP Address Structure and Usage

Explains IP addresses, their format, and range for network identification.

Micro-GC Network Connectivity

Network Requirements

Specifies cable types, network compliance, and hardware for Micro-GC networking.

Frequently Asked Questions (FAQ)

Answers common queries regarding connecting the Micro-GC to a network.

Glossary of Network Terms

Definitions of essential networking vocabulary for clear understanding.

Network Cables and Protocols

Details on patch cables, RJ45 connectors, and the TCP/IP protocol.

Workstation Software Integration

Software Communication and IP Settings

Configuration for EZChrom Elite and Galaxie, including COM ports and IP setup.

Analog and Digital I/O Configuration

Settings for integrating analog and digital I/O with workstation software.

Relay Control Setup

How to configure relay control functions within the software.

EZChrom Elite Software

Controlling the Instrument

Methods for controlling the Micro-GC via serial or Ethernet connections.

Serial Communication Setup

Instructions for establishing a serial connection to the instrument.

Ethernet Communication

Peer-to-Peer Instrument Connection

Setting up a direct Ethernet connection between a computer and the Micro-GC.

Local Network Instrument Connection

Connecting multiple instruments to a local network via a switch.

Global Network Instrument Connection

Connecting instruments across multiple networks using routers.

Communication Setup Configuration

Detailed steps for configuring communication parameters for control.

Assigning New IP Address via Ethernet

Procedure to assign a new IP address to the Micro-GC over Ethernet.

Assigning New IP Address via Serial

Procedure to assign a new IP address using a serial connection.

Remote Instrument Status Access

How to access instrument status and parameters remotely.

Instrument Status and Analog Inputs

UserDataStore addresses for instrument parameters and analog inputs.

Error Handling and States

General Error State Classification

Classification of error classes (diagnostic, advisory, critical, fatal).

Error List and Handling

Error Handling Overview

How the Micro-GC reacts to events and error messages.

Error List Part 1 (Codes 1-28)

Detailed error codes, descriptions, and actions for errors 1-28.

Error List Part 2 (Codes 29-60)

Detailed error codes, descriptions, and actions for errors 29-60.

Error List Part 3 (Codes 61-999)

Detailed error codes, descriptions, and actions for errors 61-999.

Backflush Option

Backflush Functionality and Diagrams

Explanation and diagrams of backflush to vent technique for column maintenance.

Tuning the Backflush Time

Method for adjusting backflush time to optimize analysis and column condition.

Special Backflush Time Values

Explanation of special values for backflush time, including FOREFLUSH mode.

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