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Varian Micro-GC 490-GC User Manual
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Varian BV
Herculesweg 8
4330 EA Middelburg
The Netherlands
Micro-GC
User Manual
North/South America
2700 Mitchell Drive
Walnut Creek
94598 California, USA
Tel: ++(1)9259
392400
Fax: ++(1)925945
2360 or
++(1)9259452344
Europe
P.O. Box 8033
4330 EA Middelburg
The Netherlands
Tel: ++(31)118
671000
Fax: ++(31)11862
3193
Australia/East Asia
679 Springvale Road
Mulgrave, Victoria 3171
Australia
Tel: ++(61)395
607133
Fax: ++(61)39560
7950
© 2009 Varian, Inc. All Rights Re
served
Printed in the Ne
therlands
CP501265490 Rev:1 Nov
ember 2009
2
Table of Contents
Varian Analytical Instrument Warranty
2
Hardware Products
2
Software Products
2
Remedies
2
Limitation of Warranty
2
Limitation of Remedies and Liability
2
Safety Information
3
Information
3
Operating Instructions
3
General Safety Precautions
5
Cautions
5
Spare Parts Availability
7
Service Availability
7
Table of Contents
9
Preparing for Installation
14
Gas Supply
14
Gas Samples
14
Micro-Gc Installation
15
Inspection
15
Unpacking
15
Packing List
16
Micro-GC
16
Accessories
17
Installation
18
Install Gas Regulators and Set Pressures
18
Carrier Gas
18
Connect Data Handling Peripherals
18
Sample
18
Heated Sample Line
18
Connect to Power
19
Turn Power on
19
Factory Default States and Settings
19
Instrument Overview
20
Front View
20
Back View
21
Inside View
22
Carrier Gas Connection
23
Sample Gas
24
Handling a Sample
24
Unheated Injector Systems
24
Heated Injector Systems
25
Heated Sample Line
26
Connect a Heated Sample Line
26
Power
28
Shut down Procedure
28
Long Storage Recovery Procedure
29
Initial Operation
30
Initial Run
30
Setting up the Test Method
30
Injecting the Sample
30
Column Cp-Sil 5 Cb 6 Meter Unheated
31
Column Cp-Sil 5 Cb 4 Meter Heated
32
Column Cp-Sil 5 Cb 8 Meter Heated
33
Column Cp Sil13Cb Tbm 12 Meter Heated
34
Column Hayesep 40Cm Heated
35
Column Molsieve 5Å 20 Meter Unheated
36
Conditioning of Molsieve Columns
37
Column Ppq 10 Meter Heated
38
Reference
39
Instrument Description
39
Carrier Gas
39
Micro Electronic Gas Control (Egc)
40
Injector
40
Column
41
Detector
42
Tcd
42
DMD
42
In/Outputs
43
External Digital I/O
44
Ready/Not Ready Signal
44
Communication Ports (Com)
45
External Analog I/O
46
The Differential Mobility Detector
47
General
47
General Functionality
47
Micro-GC DMD Channel
49
General Operation
50
Tuning the DMD
50
Protocols
51
Different Types of Protocols
51
The Internet Protocol Suite
51
IP Addresses
51
Micro-Gc and Networks
52
Network Requirements of the Micro-GC
52
Faq (Frequent Ask Questions)
52
Glossary of Network Terms
53
BNC Connector
53
Crossover Cable
53
Domain
53
Ethernet Address
53
Gateway
53
Host Name
53
Hub
53
IP Address
53
Patch Cable
54
RJ45 Connector
54
Tcp/Ip
54
Workstation Software
55
Ezchrom Elite
56
Control Instrument
56
Serial Communication
57
Ethernet Communication
58
Peer-To-Peer: Single Instrument
58
Multiple Instrument (Local Network)
59
Global Network: Multiple Instruments
60
Communication Setup
61
Serial Communication (Ezcrom Only)
61
Ethernet Communication (Galaxie)
61
Assign New Ip Address Via Ethernet Connection
62
Assign New Ip Address Via Serial Connection
63
Remote Access Instrument Status
64
General Error State
66
Varian Userlink Applications
68
External Relays
68
Instrument Status Including Analog Inputs
69
Userdatastore Addresses of Varian Userlink Applications
69
External Devices
71
Cycle with Static (Electronic) Pressure
73
Cycle with Electronic Pressure Control
74
Column Module Conditioning
75
Backflush Option
76
Description
77
Tuning
78
Shipping Instructions
79
Cleaning Instructions
79
Disposal Instructions
79
Error List
80
Error Handling
80
Error List
81
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Varian Micro-GC 490-GC Specifications
General
Brand
Varian
Model
Micro-GC 490-GC
Category
Laboratory Equipment
Language
English
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