395411000: Rev. 5 12 of 14 Pre-installation Instructions
Materials and Solvents
The Varian Representative will prepare solutions to tune and evaluate the LC/MS. Please
supply the materials Table 13 and the solvents on Table 14.
Table 13 M
aterials
Materials
Quantity
(each)
Item
2 50 mL clean and new volumetric flasks
2 1 L clean and new bottles for mobile phase reservoirs
1 1 L or larger bottle for LC/MS waste
2 10 mL clean and new volumetric flask
2 100 mL clean and new volumetric flask
1 Pipette 100 to 1000 µL and tips
1 Pipette 20 to 200 µL and tips
1 50 mL clean and new volumetric flask (for optional APCI)
1 500 clean and new volumetric flask (for optional APCI)
1
310-MS ONLY: Syringe pump similar to the Harvard syringe pump
(Varian part number 2732070100).
Table 14 Solvents for ESI or APCI
Solvents for ESI or APCI
Quantity
(each)
Solvent
2 4-liter bottles HPLC grade or better water, new and unopened
2 4-liter bottles HPLC grade or better, acetonitrile, new and unopened
Additional tubing is required to complete installation. Most of this tubing is included in the
accessory kits of the LC modules. Additional tubing (PEEK® or stainless steel) may be required
for installation of special valves or modules. For most analytical HPLC systems, use 1/16 in.
tubing with an ID of 0.005 in. Use 0.005 in. ID or smaller tubing downstream of the sample
injector and autosampler to prevent peak broadening. Keep tubing as short as possible to
prevent peak broadening and to minimize run time.
;
Check the checklist box: Materials and solvents of specified grade are on site.
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